Fabrication electro-spun Poly(vinyl alcohol)-Melamine nonwoven membrane composite separator for high-power lithium-ion batteries

Current commercial separators used in lithium-ion batteries have inherent flaws, especially poor thermal stability, which pose substantial safety risks. This study introduces a high-safety composite membrane made from electrospun poly(vinyl alcohol)-melamine (PVAM) and polyvinylidene fluoride (PVDF)...

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Bibliographic Details
Main Authors: Wu, Xiao-Wei, Seenivasan, Manojkumar, Karuppiah, Chelladurai, Zhang, Bo-Rong, Shih, Jeng-Ywan, Hung, Tai-Feng, Chien, Wen-Chen, Ramaraj, Sayee Kannan, Rajan, Jose, Yang, Chun-Chen
Format: Article
Language:English
Published: Elsevier Ltd 2024
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Online Access:http://umpir.ump.edu.my/id/eprint/44102/
http://umpir.ump.edu.my/id/eprint/44102/1/Fabrication%20electro-spun%20Poly%28vinyl%20alcohol%29-Melamine%20nonwoven.pdf
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Summary:Current commercial separators used in lithium-ion batteries have inherent flaws, especially poor thermal stability, which pose substantial safety risks. This study introduces a high-safety composite membrane made from electrospun poly(vinyl alcohol)-melamine (PVAM) and polyvinylidene fluoride (PVDF) polymer solutions via a dip coating method, designed for high-voltage battery systems. The poly(vinyl alcohol) and melamine components enhance battery safety, while the PVDF coating improves lithium-ion conductivity. The dip-coated PVDF/Esp-PVAM composite separators were evaluated for electrolyte uptake, contact angle, thermal stability, porosity, electrochemical stability and ionic conductivity. Notably, our Dip 1 % PVDF@Esp-PVAM composite separator exhibited excellent wettability and a lithium-ion conductivity of approximately 7.75 × 10⁻⁴ S cm⁻ 1 at room temperature. These separators outperformed conventional PE separators in half-cells with Ni-rich NCM811 cathodes, showing exceptional cycling stability with 93.4 % capacity retention after 100 cycles at 1C/1C, as compared to 84.8 % for PE separators. Our Dip 1 % PVDF@Esp-PVAM composite separator demonstrates significant potential for enhancing the long-term durability and high-rate performance of lithium-ion batteries, making it a promising option for long-term energy storage applications.