Thermal Profile and Microstructure Analysis of Al-Si with the Magnesium Addition under Different Cooling Conditions
Thermal analysis is an effective approach for studying the characteristics of materials under different temperature situations. The study implemented cooling curve analysis (CCA), complemented by computational methods for precisely evaluating the temperature variation of the molten alloy by employin...
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Springer Nature
2024
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| Online Access: | http://umpir.ump.edu.my/id/eprint/41938/ http://umpir.ump.edu.my/id/eprint/41938/1/Thermal%20Profile%20and%20Microstructure%20Analysis%20of%20Al-Si%20with%20the%20Magnesium%20Addition.pdf http://umpir.ump.edu.my/id/eprint/41938/2/THERMAL%20PROFILE%20AND%20MICROSTRUCTURE%20ANALYSIS%20OF%20Al-Si%20WITH%20THE%20MAGNESIUM%20ADDITION%20UNDER%20DIFFERENT%20COOLING%20CONDITIONS.pdf |
| _version_ | 1848826474480533504 |
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| author | Muhammad Faez, Mohamad Tajudin Asnul Hadi, Ahmad Juliawati, Alias Nur Azhani, Abd Razak Naher, S. |
| author_facet | Muhammad Faez, Mohamad Tajudin Asnul Hadi, Ahmad Juliawati, Alias Nur Azhani, Abd Razak Naher, S. |
| author_sort | Muhammad Faez, Mohamad Tajudin |
| building | UMP Institutional Repository |
| collection | Online Access |
| description | Thermal analysis is an effective approach for studying the characteristics of materials under different temperature situations. The study implemented cooling curve analysis (CCA), complemented by computational methods for precisely evaluating the temperature variation of the molten alloy by employing two thermocouples. An aluminium alloy with 1 wt.% Mg addition was melted in graphite crucible and subjected to various cooling conditions, which included normal, slow, fast, and fastest cooling rate conditions. Normal cooling condition (A) was achieved when the crucible was allowed to cool down to room temperature. Meanwhile, the slow cooling condition (B) was achieved when the crucible was allowed to cool within the Kaowool insulator chamber. In addition, the fast (C) and fastest (D) cooling conditions were attained when the forced airflow was directed at the crucible at minimum and maximum speed, respectively. The temperature data were collected via K-type thermocouples connected to a Ni 9129 data acquisition system and DasyLab software. Cooling curves, cooling curves with baselines, dendritic coherency points, and solid fractions were then recorded using OriginPro 2019b software. The liquidus, eutectic, and solidus temperatures were determined. The microstructure of the alloy sample was characterised by optical microscopy (OM), scanning electron microscopy (SEM), combined with energy-dispersive X-ray spectroscopy (EDX), and X-ray diffraction (XRD) analysis. The results show that the high cooling rates produced smaller and more globular grain structures. The highest cooling rate condition produced smaller and globular microstructure formation at 944 µm2 and a circularity of 0.61, respectively. Meanwhile, the slow cooling condition produced the largest grain size at 1668 µm2 and a circularity of 0.46. The results show that higher cooling rates result in a smaller and more spherical grain structure than other cooling conditions. This underlines the significant influence of the cooling rate on the development of the microstructure during the solidification process. This comprehensive thermal analysis study has shed light on the significant influence of Mg addition and different cooling conditions on the Al-Si alloy's thermal properties and microstructure formation. The results contribute to understanding alloy solidification and may have practical implications for materials engineering and manufacturing. |
| first_indexed | 2025-11-15T03:45:24Z |
| format | Article |
| id | ump-41938 |
| institution | Universiti Malaysia Pahang |
| institution_category | Local University |
| language | English English |
| last_indexed | 2025-11-15T03:45:24Z |
| publishDate | 2024 |
| publisher | Springer Nature |
| recordtype | eprints |
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| spelling | ump-419382024-07-15T08:05:22Z http://umpir.ump.edu.my/id/eprint/41938/ Thermal Profile and Microstructure Analysis of Al-Si with the Magnesium Addition under Different Cooling Conditions Muhammad Faez, Mohamad Tajudin Asnul Hadi, Ahmad Juliawati, Alias Nur Azhani, Abd Razak Naher, S. T Technology (General) TJ Mechanical engineering and machinery TL Motor vehicles. Aeronautics. Astronautics Thermal analysis is an effective approach for studying the characteristics of materials under different temperature situations. The study implemented cooling curve analysis (CCA), complemented by computational methods for precisely evaluating the temperature variation of the molten alloy by employing two thermocouples. An aluminium alloy with 1 wt.% Mg addition was melted in graphite crucible and subjected to various cooling conditions, which included normal, slow, fast, and fastest cooling rate conditions. Normal cooling condition (A) was achieved when the crucible was allowed to cool down to room temperature. Meanwhile, the slow cooling condition (B) was achieved when the crucible was allowed to cool within the Kaowool insulator chamber. In addition, the fast (C) and fastest (D) cooling conditions were attained when the forced airflow was directed at the crucible at minimum and maximum speed, respectively. The temperature data were collected via K-type thermocouples connected to a Ni 9129 data acquisition system and DasyLab software. Cooling curves, cooling curves with baselines, dendritic coherency points, and solid fractions were then recorded using OriginPro 2019b software. The liquidus, eutectic, and solidus temperatures were determined. The microstructure of the alloy sample was characterised by optical microscopy (OM), scanning electron microscopy (SEM), combined with energy-dispersive X-ray spectroscopy (EDX), and X-ray diffraction (XRD) analysis. The results show that the high cooling rates produced smaller and more globular grain structures. The highest cooling rate condition produced smaller and globular microstructure formation at 944 µm2 and a circularity of 0.61, respectively. Meanwhile, the slow cooling condition produced the largest grain size at 1668 µm2 and a circularity of 0.46. The results show that higher cooling rates result in a smaller and more spherical grain structure than other cooling conditions. This underlines the significant influence of the cooling rate on the development of the microstructure during the solidification process. This comprehensive thermal analysis study has shed light on the significant influence of Mg addition and different cooling conditions on the Al-Si alloy's thermal properties and microstructure formation. The results contribute to understanding alloy solidification and may have practical implications for materials engineering and manufacturing. Springer Nature 2024 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/41938/1/Thermal%20Profile%20and%20Microstructure%20Analysis%20of%20Al-Si%20with%20the%20Magnesium%20Addition.pdf pdf en http://umpir.ump.edu.my/id/eprint/41938/2/THERMAL%20PROFILE%20AND%20MICROSTRUCTURE%20ANALYSIS%20OF%20Al-Si%20WITH%20THE%20MAGNESIUM%20ADDITION%20UNDER%20DIFFERENT%20COOLING%20CONDITIONS.pdf Muhammad Faez, Mohamad Tajudin and Asnul Hadi, Ahmad and Juliawati, Alias and Nur Azhani, Abd Razak and Naher, S. (2024) Thermal Profile and Microstructure Analysis of Al-Si with the Magnesium Addition under Different Cooling Conditions. International Journal of Metalcasting. pp. 1-14. ISSN 2163-3193. (In Press / Online First) (In Press / Online First) https://doi.org/10.1007/s40962-024-01388-4 10.1007/s40962-024-01388-4 |
| spellingShingle | T Technology (General) TJ Mechanical engineering and machinery TL Motor vehicles. Aeronautics. Astronautics Muhammad Faez, Mohamad Tajudin Asnul Hadi, Ahmad Juliawati, Alias Nur Azhani, Abd Razak Naher, S. Thermal Profile and Microstructure Analysis of Al-Si with the Magnesium Addition under Different Cooling Conditions |
| title | Thermal Profile and Microstructure Analysis of Al-Si with the Magnesium Addition under Different Cooling Conditions |
| title_full | Thermal Profile and Microstructure Analysis of Al-Si with the Magnesium Addition under Different Cooling Conditions |
| title_fullStr | Thermal Profile and Microstructure Analysis of Al-Si with the Magnesium Addition under Different Cooling Conditions |
| title_full_unstemmed | Thermal Profile and Microstructure Analysis of Al-Si with the Magnesium Addition under Different Cooling Conditions |
| title_short | Thermal Profile and Microstructure Analysis of Al-Si with the Magnesium Addition under Different Cooling Conditions |
| title_sort | thermal profile and microstructure analysis of al-si with the magnesium addition under different cooling conditions |
| topic | T Technology (General) TJ Mechanical engineering and machinery TL Motor vehicles. Aeronautics. Astronautics |
| url | http://umpir.ump.edu.my/id/eprint/41938/ http://umpir.ump.edu.my/id/eprint/41938/ http://umpir.ump.edu.my/id/eprint/41938/ http://umpir.ump.edu.my/id/eprint/41938/1/Thermal%20Profile%20and%20Microstructure%20Analysis%20of%20Al-Si%20with%20the%20Magnesium%20Addition.pdf http://umpir.ump.edu.my/id/eprint/41938/2/THERMAL%20PROFILE%20AND%20MICROSTRUCTURE%20ANALYSIS%20OF%20Al-Si%20WITH%20THE%20MAGNESIUM%20ADDITION%20UNDER%20DIFFERENT%20COOLING%20CONDITIONS.pdf |