The effect of temperature on the hydrothermal synthesis of carbonated apatite from calcium carbonate obtained from green mussels shells
Hydroxyapatite (HAp) refers to a bioceramic broadly employed in bone tissue engineering since it has bioactive and osteoconductive properties. The synthesis of HAp will be more economically viable using waste materials because it is cheap, easy to find, and available in large quantities. Therefore,...
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| Format: | Article |
| Language: | English English |
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Asian Research Publishing Network
2023
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| Online Access: | http://umpir.ump.edu.my/id/eprint/40504/ http://umpir.ump.edu.my/id/eprint/40504/1/The%20effect%20of%20temperature%20on%20the%20hydrothermal.pdf http://umpir.ump.edu.my/id/eprint/40504/2/The%20effect%20of%20temperature%20on%20the%20hydrothermal%20synthesis%20of%20carbonated%20apatite%20from%20calcium%20carbonate%20obtained%20from%20green%20mussels%20shells_ABS.pdf |
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| author | Fitriyana, Deni Fajar Irawan, Agustinus Purna Bahatmaka, Aldias Ismail, Rifky Bayuseno, Athanasius Priharyoto Muhamadin, Rilo Chandra Cionita, Tezara Siregar, Januar Parlaungan Jehadus, Emilianus Baskara, Gregorius Dimas Laksmidewi, Dwinita da Silva Guterres, Natalino Fonseca |
| author_facet | Fitriyana, Deni Fajar Irawan, Agustinus Purna Bahatmaka, Aldias Ismail, Rifky Bayuseno, Athanasius Priharyoto Muhamadin, Rilo Chandra Cionita, Tezara Siregar, Januar Parlaungan Jehadus, Emilianus Baskara, Gregorius Dimas Laksmidewi, Dwinita da Silva Guterres, Natalino Fonseca |
| author_sort | Fitriyana, Deni Fajar |
| building | UMP Institutional Repository |
| collection | Online Access |
| description | Hydroxyapatite (HAp) refers to a bioceramic broadly employed in bone tissue engineering since it has bioactive and osteoconductive properties. The synthesis of HAp will be more economically viable using waste materials because it is cheap, easy to find, and available in large quantities. Therefore, this study aimed to synthesize and characterize HAp from green mussel shells by hydrothermal method at various temperatures. Precipitated calcium carbonate (PCC), made from green mussel shell powder, is employed in this study. Utilizing a hydrothermal reactor for 14 hours at 120°C, 140°C, as well as 160°C, a combination of PCC and (NH4)2HPO4 with a Ca/P molar ratio of 1.67 was synthesized to form HAp. Note that the synthesis findings were categorized using scanning electron microscopy (SEM), Fourier transforms infrared spectroscopy (FTIR), as well as X-ray diffraction (XRD) tests. Apart from that, the FTIR test showed the formation of HAp in all test variations because the results of –OH, and –PO4 were found. XRD results that have been analyzed using HighScore Plus software show the percentage of weight (%) and crystal size of HAp increases with increasing hydrothermal temperature. Other than that, HAp produced at hydrothermal temperature variations of 160°C has a hexagonal crystal system with a percentage of weight (%) as well as a crystal size of 46.43 nm and 99.3%, whilst the amount of impurity (%) produced is 0.7%. The higher the hydrothermal temperature, the weight percentage (%), and the crystallite size in HAp are getting bigger while the number of impurities gets smaller. |
| first_indexed | 2025-11-15T03:38:56Z |
| format | Article |
| id | ump-40504 |
| institution | Universiti Malaysia Pahang |
| institution_category | Local University |
| language | English English |
| last_indexed | 2025-11-15T03:38:56Z |
| publishDate | 2023 |
| publisher | Asian Research Publishing Network |
| recordtype | eprints |
| repository_type | Digital Repository |
| spelling | ump-405042024-04-30T06:25:30Z http://umpir.ump.edu.my/id/eprint/40504/ The effect of temperature on the hydrothermal synthesis of carbonated apatite from calcium carbonate obtained from green mussels shells Fitriyana, Deni Fajar Irawan, Agustinus Purna Bahatmaka, Aldias Ismail, Rifky Bayuseno, Athanasius Priharyoto Muhamadin, Rilo Chandra Cionita, Tezara Siregar, Januar Parlaungan Jehadus, Emilianus Baskara, Gregorius Dimas Laksmidewi, Dwinita da Silva Guterres, Natalino Fonseca T Technology (General) TA Engineering (General). Civil engineering (General) TJ Mechanical engineering and machinery TL Motor vehicles. Aeronautics. Astronautics Hydroxyapatite (HAp) refers to a bioceramic broadly employed in bone tissue engineering since it has bioactive and osteoconductive properties. The synthesis of HAp will be more economically viable using waste materials because it is cheap, easy to find, and available in large quantities. Therefore, this study aimed to synthesize and characterize HAp from green mussel shells by hydrothermal method at various temperatures. Precipitated calcium carbonate (PCC), made from green mussel shell powder, is employed in this study. Utilizing a hydrothermal reactor for 14 hours at 120°C, 140°C, as well as 160°C, a combination of PCC and (NH4)2HPO4 with a Ca/P molar ratio of 1.67 was synthesized to form HAp. Note that the synthesis findings were categorized using scanning electron microscopy (SEM), Fourier transforms infrared spectroscopy (FTIR), as well as X-ray diffraction (XRD) tests. Apart from that, the FTIR test showed the formation of HAp in all test variations because the results of –OH, and –PO4 were found. XRD results that have been analyzed using HighScore Plus software show the percentage of weight (%) and crystal size of HAp increases with increasing hydrothermal temperature. Other than that, HAp produced at hydrothermal temperature variations of 160°C has a hexagonal crystal system with a percentage of weight (%) as well as a crystal size of 46.43 nm and 99.3%, whilst the amount of impurity (%) produced is 0.7%. The higher the hydrothermal temperature, the weight percentage (%), and the crystallite size in HAp are getting bigger while the number of impurities gets smaller. Asian Research Publishing Network 2023 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/40504/1/The%20effect%20of%20temperature%20on%20the%20hydrothermal.pdf pdf en http://umpir.ump.edu.my/id/eprint/40504/2/The%20effect%20of%20temperature%20on%20the%20hydrothermal%20synthesis%20of%20carbonated%20apatite%20from%20calcium%20carbonate%20obtained%20from%20green%20mussels%20shells_ABS.pdf Fitriyana, Deni Fajar and Irawan, Agustinus Purna and Bahatmaka, Aldias and Ismail, Rifky and Bayuseno, Athanasius Priharyoto and Muhamadin, Rilo Chandra and Cionita, Tezara and Siregar, Januar Parlaungan and Jehadus, Emilianus and Baskara, Gregorius Dimas and Laksmidewi, Dwinita and da Silva Guterres, Natalino Fonseca (2023) The effect of temperature on the hydrothermal synthesis of carbonated apatite from calcium carbonate obtained from green mussels shells. ARPN Journal of Engineering and Applied Sciences, 18 (11). pp. 1215-1224. ISSN 1819-6608. (Published) https://doi.org/10.59018/0623158 https://doi.org/10.59018/0623158 |
| spellingShingle | T Technology (General) TA Engineering (General). Civil engineering (General) TJ Mechanical engineering and machinery TL Motor vehicles. Aeronautics. Astronautics Fitriyana, Deni Fajar Irawan, Agustinus Purna Bahatmaka, Aldias Ismail, Rifky Bayuseno, Athanasius Priharyoto Muhamadin, Rilo Chandra Cionita, Tezara Siregar, Januar Parlaungan Jehadus, Emilianus Baskara, Gregorius Dimas Laksmidewi, Dwinita da Silva Guterres, Natalino Fonseca The effect of temperature on the hydrothermal synthesis of carbonated apatite from calcium carbonate obtained from green mussels shells |
| title | The effect of temperature on the hydrothermal synthesis of carbonated apatite from calcium carbonate obtained from green mussels shells |
| title_full | The effect of temperature on the hydrothermal synthesis of carbonated apatite from calcium carbonate obtained from green mussels shells |
| title_fullStr | The effect of temperature on the hydrothermal synthesis of carbonated apatite from calcium carbonate obtained from green mussels shells |
| title_full_unstemmed | The effect of temperature on the hydrothermal synthesis of carbonated apatite from calcium carbonate obtained from green mussels shells |
| title_short | The effect of temperature on the hydrothermal synthesis of carbonated apatite from calcium carbonate obtained from green mussels shells |
| title_sort | effect of temperature on the hydrothermal synthesis of carbonated apatite from calcium carbonate obtained from green mussels shells |
| topic | T Technology (General) TA Engineering (General). Civil engineering (General) TJ Mechanical engineering and machinery TL Motor vehicles. Aeronautics. Astronautics |
| url | http://umpir.ump.edu.my/id/eprint/40504/ http://umpir.ump.edu.my/id/eprint/40504/ http://umpir.ump.edu.my/id/eprint/40504/ http://umpir.ump.edu.my/id/eprint/40504/1/The%20effect%20of%20temperature%20on%20the%20hydrothermal.pdf http://umpir.ump.edu.my/id/eprint/40504/2/The%20effect%20of%20temperature%20on%20the%20hydrothermal%20synthesis%20of%20carbonated%20apatite%20from%20calcium%20carbonate%20obtained%20from%20green%20mussels%20shells_ABS.pdf |