Iron-based nanoparticles oxygen scavenger for suppressing heat-stable salts formation in amine

Heat-stable salts (HSS), which trigger excessing foaming in absorber, are formed when protonated methyl diethanolamine (MDEA) reacts with the more acidic degraded products in the presence of dissolved oxygen (DO). The aim is to suppress the HSS formation in MDEA solution inaugurally employing a hybr...

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Main Authors: Chin, Sim Yee, Lim, Soh Fong, Lau, Kok Keong, Thangavel, Mythili, Muhammad Ridzuan, Kamaruzaman
Format: Article
Language:English
Published: Wiley-VCH Verlag 2023
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/40365/
http://umpir.ump.edu.my/id/eprint/40365/1/Iron-based%20nanoparticles%20oxygen%20scavenger%20for%20suppressing%20heat-stable%20salts%20.pdf
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author Chin, Sim Yee
Lim, Soh Fong
Lau, Kok Keong
Thangavel, Mythili
Muhammad Ridzuan, Kamaruzaman
author_facet Chin, Sim Yee
Lim, Soh Fong
Lau, Kok Keong
Thangavel, Mythili
Muhammad Ridzuan, Kamaruzaman
author_sort Chin, Sim Yee
building UMP Institutional Repository
collection Online Access
description Heat-stable salts (HSS), which trigger excessing foaming in absorber, are formed when protonated methyl diethanolamine (MDEA) reacts with the more acidic degraded products in the presence of dissolved oxygen (DO). The aim is to suppress the HSS formation in MDEA solution inaugurally employing a hybrid iron-based nanoparticles (HINP) oxygen scavenger. It was discovered that the oxygen-scavenging performance of a more cost-effective 20 %Fe/HZSM5 was one-fold higher than the 20 %Fe/MCM-41. The former was verified for its superior structural properties. The Fe2+ on its surface first reacted with DO, preventing DO from oxidizing the MDEA. Consequently, the absence of hydroxyl radicals eliminated the potential of formic acid formation, hence suppressing the MDEA-acid HSS formation.
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institution Universiti Malaysia Pahang
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publishDate 2023
publisher Wiley-VCH Verlag
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spelling ump-403652024-02-15T01:46:56Z http://umpir.ump.edu.my/id/eprint/40365/ Iron-based nanoparticles oxygen scavenger for suppressing heat-stable salts formation in amine Chin, Sim Yee Lim, Soh Fong Lau, Kok Keong Thangavel, Mythili Muhammad Ridzuan, Kamaruzaman Q Science (General) QD Chemistry TP Chemical technology Heat-stable salts (HSS), which trigger excessing foaming in absorber, are formed when protonated methyl diethanolamine (MDEA) reacts with the more acidic degraded products in the presence of dissolved oxygen (DO). The aim is to suppress the HSS formation in MDEA solution inaugurally employing a hybrid iron-based nanoparticles (HINP) oxygen scavenger. It was discovered that the oxygen-scavenging performance of a more cost-effective 20 %Fe/HZSM5 was one-fold higher than the 20 %Fe/MCM-41. The former was verified for its superior structural properties. The Fe2+ on its surface first reacted with DO, preventing DO from oxidizing the MDEA. Consequently, the absence of hydroxyl radicals eliminated the potential of formic acid formation, hence suppressing the MDEA-acid HSS formation. Wiley-VCH Verlag 2023-12 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/40365/1/Iron-based%20nanoparticles%20oxygen%20scavenger%20for%20suppressing%20heat-stable%20salts%20.pdf Chin, Sim Yee and Lim, Soh Fong and Lau, Kok Keong and Thangavel, Mythili and Muhammad Ridzuan, Kamaruzaman (2023) Iron-based nanoparticles oxygen scavenger for suppressing heat-stable salts formation in amine. Chemical Engineering and Technology, 46 (12). 2670 -2675. ISSN 0930-7516. (Published) https://doi.org/10.1002/ceat.202300081 https://doi.org/10.1002/ceat.202300081
spellingShingle Q Science (General)
QD Chemistry
TP Chemical technology
Chin, Sim Yee
Lim, Soh Fong
Lau, Kok Keong
Thangavel, Mythili
Muhammad Ridzuan, Kamaruzaman
Iron-based nanoparticles oxygen scavenger for suppressing heat-stable salts formation in amine
title Iron-based nanoparticles oxygen scavenger for suppressing heat-stable salts formation in amine
title_full Iron-based nanoparticles oxygen scavenger for suppressing heat-stable salts formation in amine
title_fullStr Iron-based nanoparticles oxygen scavenger for suppressing heat-stable salts formation in amine
title_full_unstemmed Iron-based nanoparticles oxygen scavenger for suppressing heat-stable salts formation in amine
title_short Iron-based nanoparticles oxygen scavenger for suppressing heat-stable salts formation in amine
title_sort iron-based nanoparticles oxygen scavenger for suppressing heat-stable salts formation in amine
topic Q Science (General)
QD Chemistry
TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/40365/
http://umpir.ump.edu.my/id/eprint/40365/
http://umpir.ump.edu.my/id/eprint/40365/
http://umpir.ump.edu.my/id/eprint/40365/1/Iron-based%20nanoparticles%20oxygen%20scavenger%20for%20suppressing%20heat-stable%20salts%20.pdf