Factorial screening on the development of cellulose nanocrystal/ carboxylated multi-walled carbon nanotube polyethersulfone membrane for humic acid rejection

A two-level factorial experimental design was used to formulate the dope composition of cellulose nanocrystal (CNC) multi-walled carbon nanotube (MWCNT) polyethersulfone (PES) membrane for humic acid (HA) rejection. Four factors were screened, which are the composition of PES (1517 wt.%), polyvinylp...

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Bibliographic Details
Main Authors: Nor Azura, Che Mahmud, Mazrul Nizam, Abu Seman, Mohd Sobri, Takriff, Ang, Wei Lun, Saufia, Syed M.
Format: Conference or Workshop Item
Language:English
Published: 2022
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/37027/
http://umpir.ump.edu.my/id/eprint/37027/1/Factorial%20screening%20on%20the%20development%20of%20cellulose%20nanocrystal_carboxylated%20multi-walled%20carbon%20nanotube%20polyethersulfone%20membrane%20for%20humic%20acid%20rejection.pdf
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Summary:A two-level factorial experimental design was used to formulate the dope composition of cellulose nanocrystal (CNC) multi-walled carbon nanotube (MWCNT) polyethersulfone (PES) membrane for humic acid (HA) rejection. Four factors were screened, which are the composition of PES (1517 wt.%), polyvinylpyrrolidone (PVP, 1-4%), CNC (0.01-0.75%), and carboxylated MWCNT (00.025%). The membranes were evaluated based on HA rejection from a 10-ppm aqueous feed solution. The percentage of MWCNT was the most significant factor, accounting for 72.31 % of the contribution. The highest HA rejection of 90% was obtained from the membrane fabricated using 17 % PES, 1% PVP,0.01 % CNC, and 0.025% MWCNT. The predicted values generated from the model agreed reasonably with the experimental data, demonstrating the model's validity.