Studies on H+ ions conducting bio-polymer blend electrolyte based on alginate-PVA doped with NH4NO3

This study provides insights into the protonation of bio-polymer blend electrolytes (BBEs) that are based on alginate (Alg)-PVA doped with various NH4NO3 compositions, which was prepared using the solution casting method. The physicochemical of BBEs were studied by using electrical impedance spectro...

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Main Authors: N. M., Ghazali, A. F., Fuzlin, M. A., Saadiah, Md. M., Hasan, Y., Nagao, A. S., Samsudin
Format: Article
Language:English
Published: Elsevier Ltd 2022
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/35552/
http://umpir.ump.edu.my/id/eprint/35552/1/Studies%20on%20H%2B%20ions%20conducting%20bio-polymer%20.pdf
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author N. M., Ghazali
A. F., Fuzlin
M. A., Saadiah
Md. M., Hasan
Y., Nagao
A. S., Samsudin
author_facet N. M., Ghazali
A. F., Fuzlin
M. A., Saadiah
Md. M., Hasan
Y., Nagao
A. S., Samsudin
author_sort N. M., Ghazali
building UMP Institutional Repository
collection Online Access
description This study provides insights into the protonation of bio-polymer blend electrolytes (BBEs) that are based on alginate (Alg)-PVA doped with various NH4NO3 compositions, which was prepared using the solution casting method. The physicochemical of BBEs were studied by using electrical impedance spectroscopy (EIS) analysis, thermogravimetric analysis (TGA), scanning electron microscope (SEM), x-ray diffraction (XRD) and Fourier transform infrared (FTIR) spectroscopy. The complexation had occurred between the Alg-PVA functional groups with the H+–NH3NO3 through the shifting and changes in the intensity of the bands. The BBEs films showed the enhancement of amorphous and the presence of globules when introduced NH4NO3, which enhanced the ionic conductivity. The addition of 35 wt.% of NH4NO3 resulted in the highest ionic conductivity value of 5.20×10–4 S cm-1 and demonstrated excellent thermal property. It was found that the system's ionic conductivity was generally influenced by the charge carriers based on evaluation of the Nyquist fitting approaches.
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publisher Elsevier Ltd
recordtype eprints
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spelling ump-355522022-11-08T04:45:49Z http://umpir.ump.edu.my/id/eprint/35552/ Studies on H+ ions conducting bio-polymer blend electrolyte based on alginate-PVA doped with NH4NO3 N. M., Ghazali A. F., Fuzlin M. A., Saadiah Md. M., Hasan Y., Nagao A. S., Samsudin Q Science (General) QC Physics QD Chemistry This study provides insights into the protonation of bio-polymer blend electrolytes (BBEs) that are based on alginate (Alg)-PVA doped with various NH4NO3 compositions, which was prepared using the solution casting method. The physicochemical of BBEs were studied by using electrical impedance spectroscopy (EIS) analysis, thermogravimetric analysis (TGA), scanning electron microscope (SEM), x-ray diffraction (XRD) and Fourier transform infrared (FTIR) spectroscopy. The complexation had occurred between the Alg-PVA functional groups with the H+–NH3NO3 through the shifting and changes in the intensity of the bands. The BBEs films showed the enhancement of amorphous and the presence of globules when introduced NH4NO3, which enhanced the ionic conductivity. The addition of 35 wt.% of NH4NO3 resulted in the highest ionic conductivity value of 5.20×10–4 S cm-1 and demonstrated excellent thermal property. It was found that the system's ionic conductivity was generally influenced by the charge carriers based on evaluation of the Nyquist fitting approaches. Elsevier Ltd 2022-12-15 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/35552/1/Studies%20on%20H%2B%20ions%20conducting%20bio-polymer%20.pdf N. M., Ghazali and A. F., Fuzlin and M. A., Saadiah and Md. M., Hasan and Y., Nagao and A. S., Samsudin (2022) Studies on H+ ions conducting bio-polymer blend electrolyte based on alginate-PVA doped with NH4NO3. Journal of Non-Crystalline Solids, 598 (121939). pp. 1-15. ISSN 0022-3093. (Published) https://doi.org/10.1016/j.jnoncrysol.2022.121939 https://doi.org/10.1016/j.jnoncrysol.2022.121939
spellingShingle Q Science (General)
QC Physics
QD Chemistry
N. M., Ghazali
A. F., Fuzlin
M. A., Saadiah
Md. M., Hasan
Y., Nagao
A. S., Samsudin
Studies on H+ ions conducting bio-polymer blend electrolyte based on alginate-PVA doped with NH4NO3
title Studies on H+ ions conducting bio-polymer blend electrolyte based on alginate-PVA doped with NH4NO3
title_full Studies on H+ ions conducting bio-polymer blend electrolyte based on alginate-PVA doped with NH4NO3
title_fullStr Studies on H+ ions conducting bio-polymer blend electrolyte based on alginate-PVA doped with NH4NO3
title_full_unstemmed Studies on H+ ions conducting bio-polymer blend electrolyte based on alginate-PVA doped with NH4NO3
title_short Studies on H+ ions conducting bio-polymer blend electrolyte based on alginate-PVA doped with NH4NO3
title_sort studies on h+ ions conducting bio-polymer blend electrolyte based on alginate-pva doped with nh4no3
topic Q Science (General)
QC Physics
QD Chemistry
url http://umpir.ump.edu.my/id/eprint/35552/
http://umpir.ump.edu.my/id/eprint/35552/
http://umpir.ump.edu.my/id/eprint/35552/
http://umpir.ump.edu.my/id/eprint/35552/1/Studies%20on%20H%2B%20ions%20conducting%20bio-polymer%20.pdf