Synthesis of α-alumina developed from waste aluminium using precipitation technique

The heated aluminium containers were added to a solution of 8.0 M H2SO4 solution, which eventually yielded a solution of Al2(SO4)3 after a series of stepwise precipitation reactions. Al2(SO4)3 was presented in large quantities of H2SO4 in the white semi-fluid solution; there were some unreacted alum...

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Main Authors: Aiman A., Mokaizh, Jun Haslinda, Shariffuddin
Format: Conference or Workshop Item
Language:English
Published: IOP Publishing 2021
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/35396/
http://umpir.ump.edu.my/id/eprint/35396/1/Synthesis%20of%20%CE%B1-alumina%20developed%20from%20waste%20aluminium%20using%20precipitation%20technique.pdf
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author Aiman A., Mokaizh
Jun Haslinda, Shariffuddin
author_facet Aiman A., Mokaizh
Jun Haslinda, Shariffuddin
author_sort Aiman A., Mokaizh
building UMP Institutional Repository
collection Online Access
description The heated aluminium containers were added to a solution of 8.0 M H2SO4 solution, which eventually yielded a solution of Al2(SO4)3 after a series of stepwise precipitation reactions. Al2(SO4)3 was presented in large quantities of H2SO4 in the white semi-fluid solution; there were some unreacted aluminium parts. The solution was subjected to filtration and then mixed with anion in a ratio of 2:3, this resulted in the formation of a white layer Al2(SO4)3•18H2O. Thereafter, Al2(SO4)3•18H2O was calcined in an electric oven for 2 h at various calcination temperatures (500, 700, 900, 1100, and 1300°C). The mixtures were heated and cooled at a rate of 10°C/min. XRD was employed to investigate variations in temperature and determination of elemental accumulation of alumina produced. Ah(SO4)3•18H2O was due to a series of aluminium compositions produced from dehydration. All transitions from low temperatures to aluminium phases were converted to high-temperature α-Al2O3. The results obtained from X-ray disintegration showed that the α-Al2O3 phase was obtained at a reaction temperature of about 1150°C and above.
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format Conference or Workshop Item
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institution Universiti Malaysia Pahang
institution_category Local University
language English
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publishDate 2021
publisher IOP Publishing
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spelling ump-353962022-10-26T01:50:23Z http://umpir.ump.edu.my/id/eprint/35396/ Synthesis of α-alumina developed from waste aluminium using precipitation technique Aiman A., Mokaizh Jun Haslinda, Shariffuddin QD Chemistry TA Engineering (General). Civil engineering (General) TP Chemical technology The heated aluminium containers were added to a solution of 8.0 M H2SO4 solution, which eventually yielded a solution of Al2(SO4)3 after a series of stepwise precipitation reactions. Al2(SO4)3 was presented in large quantities of H2SO4 in the white semi-fluid solution; there were some unreacted aluminium parts. The solution was subjected to filtration and then mixed with anion in a ratio of 2:3, this resulted in the formation of a white layer Al2(SO4)3•18H2O. Thereafter, Al2(SO4)3•18H2O was calcined in an electric oven for 2 h at various calcination temperatures (500, 700, 900, 1100, and 1300°C). The mixtures were heated and cooled at a rate of 10°C/min. XRD was employed to investigate variations in temperature and determination of elemental accumulation of alumina produced. Ah(SO4)3•18H2O was due to a series of aluminium compositions produced from dehydration. All transitions from low temperatures to aluminium phases were converted to high-temperature α-Al2O3. The results obtained from X-ray disintegration showed that the α-Al2O3 phase was obtained at a reaction temperature of about 1150°C and above. IOP Publishing 2021-06-16 Conference or Workshop Item PeerReviewed pdf en cc_by http://umpir.ump.edu.my/id/eprint/35396/1/Synthesis%20of%20%CE%B1-alumina%20developed%20from%20waste%20aluminium%20using%20precipitation%20technique.pdf Aiman A., Mokaizh and Jun Haslinda, Shariffuddin (2021) Synthesis of α-alumina developed from waste aluminium using precipitation technique. In: Journal of Physics: Conference Series, The 1st International Conference on Fundamental, Applied Sciences and Technology (ICoFAST 2021) , 15-16 March 2021 , Perlis, Malaysia, & Hadhramout, Yemen. pp. 1-8., 1900 (012002). ISSN 1742-6588 (Published) https://doi.org/10.1088/1742-6596/1900/1/012002
spellingShingle QD Chemistry
TA Engineering (General). Civil engineering (General)
TP Chemical technology
Aiman A., Mokaizh
Jun Haslinda, Shariffuddin
Synthesis of α-alumina developed from waste aluminium using precipitation technique
title Synthesis of α-alumina developed from waste aluminium using precipitation technique
title_full Synthesis of α-alumina developed from waste aluminium using precipitation technique
title_fullStr Synthesis of α-alumina developed from waste aluminium using precipitation technique
title_full_unstemmed Synthesis of α-alumina developed from waste aluminium using precipitation technique
title_short Synthesis of α-alumina developed from waste aluminium using precipitation technique
title_sort synthesis of α-alumina developed from waste aluminium using precipitation technique
topic QD Chemistry
TA Engineering (General). Civil engineering (General)
TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/35396/
http://umpir.ump.edu.my/id/eprint/35396/
http://umpir.ump.edu.my/id/eprint/35396/1/Synthesis%20of%20%CE%B1-alumina%20developed%20from%20waste%20aluminium%20using%20precipitation%20technique.pdf