Green synthesis of stannic oxide nanoparticles for ciprofloxacin degradation: optimization and modelling using a Response Surface Methodology (RSM) based on the box–behnken design

In this work, stannic oxide (SnO2) nanoparticles were biologically synthesized utilizing the polysaccharide extract of gum acacia by performing the calcination of stannous chloride precursors at 450° centigrade. The confirmation of SnO2 nanoparticles was done through various characterizations. Makin...

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Main Authors: Dash, Archita Rani, Lakhani, Aadit J., Priya, Duraipandi Devi, Surendra, T. V., Khan, Md. Maksudur Rahman, Samuel, E. James Jebaseelan, Roopan, Selvaraj Mohana
Format: Article
Language:English
Published: Springer 2021
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/34396/
http://umpir.ump.edu.my/id/eprint/34396/1/Green%20synthesis%20of%20stannic%20oxide%20nanoparticles.pdf
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author Dash, Archita Rani
Lakhani, Aadit J.
Priya, Duraipandi Devi
Surendra, T. V.
Khan, Md. Maksudur Rahman
Samuel, E. James Jebaseelan
Roopan, Selvaraj Mohana
author_facet Dash, Archita Rani
Lakhani, Aadit J.
Priya, Duraipandi Devi
Surendra, T. V.
Khan, Md. Maksudur Rahman
Samuel, E. James Jebaseelan
Roopan, Selvaraj Mohana
author_sort Dash, Archita Rani
building UMP Institutional Repository
collection Online Access
description In this work, stannic oxide (SnO2) nanoparticles were biologically synthesized utilizing the polysaccharide extract of gum acacia by performing the calcination of stannous chloride precursors at 450° centigrade. The confirmation of SnO2 nanoparticles was done through various characterizations. Making use of the Scherer formula within the XRD analysis, the dimensions confirmed for the synthesized nanoparticles of SnO2 was obtained to be 4.66 nm. SnO2 NPs are 4.22 nm in size, according to TEM images. ciprofloxacin is a frequently utilized antibiotic as well as exclusive therapy for bacterial infections, and not viral pathogens. In this report, ciprofloxacin photocatalytic degradation in presence of stannic oxide was investigated, which was confirmed by the UV–Vis characterization. The results also optimized using RSM optimization and indicated that the efficiency of ciprofloxacin removal is 99.7% under the optimum conditions of experimental factors (catalyst concentration (R1) in 50 mg/L, ciprofloxacin dose (R2) in 0.5 g/L, and Reaction time (R3) in 120 min). These results suggest that these nanoparticles possess great potential for removing ciprofloxacin from aqueous solutions.
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spelling ump-343962022-11-15T07:52:28Z http://umpir.ump.edu.my/id/eprint/34396/ Green synthesis of stannic oxide nanoparticles for ciprofloxacin degradation: optimization and modelling using a Response Surface Methodology (RSM) based on the box–behnken design Dash, Archita Rani Lakhani, Aadit J. Priya, Duraipandi Devi Surendra, T. V. Khan, Md. Maksudur Rahman Samuel, E. James Jebaseelan Roopan, Selvaraj Mohana TP Chemical technology In this work, stannic oxide (SnO2) nanoparticles were biologically synthesized utilizing the polysaccharide extract of gum acacia by performing the calcination of stannous chloride precursors at 450° centigrade. The confirmation of SnO2 nanoparticles was done through various characterizations. Making use of the Scherer formula within the XRD analysis, the dimensions confirmed for the synthesized nanoparticles of SnO2 was obtained to be 4.66 nm. SnO2 NPs are 4.22 nm in size, according to TEM images. ciprofloxacin is a frequently utilized antibiotic as well as exclusive therapy for bacterial infections, and not viral pathogens. In this report, ciprofloxacin photocatalytic degradation in presence of stannic oxide was investigated, which was confirmed by the UV–Vis characterization. The results also optimized using RSM optimization and indicated that the efficiency of ciprofloxacin removal is 99.7% under the optimum conditions of experimental factors (catalyst concentration (R1) in 50 mg/L, ciprofloxacin dose (R2) in 0.5 g/L, and Reaction time (R3) in 120 min). These results suggest that these nanoparticles possess great potential for removing ciprofloxacin from aqueous solutions. Springer 2021 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/34396/1/Green%20synthesis%20of%20stannic%20oxide%20nanoparticles.pdf Dash, Archita Rani and Lakhani, Aadit J. and Priya, Duraipandi Devi and Surendra, T. V. and Khan, Md. Maksudur Rahman and Samuel, E. James Jebaseelan and Roopan, Selvaraj Mohana (2021) Green synthesis of stannic oxide nanoparticles for ciprofloxacin degradation: optimization and modelling using a Response Surface Methodology (RSM) based on the box–behnken design. Journal of Cluster Science. pp. 1-13. ISSN 1572-8862. (Published) https://doi.org/10.1007/s10876-021-02198-y https://doi.org/10.1007/s10876-021-02198-y
spellingShingle TP Chemical technology
Dash, Archita Rani
Lakhani, Aadit J.
Priya, Duraipandi Devi
Surendra, T. V.
Khan, Md. Maksudur Rahman
Samuel, E. James Jebaseelan
Roopan, Selvaraj Mohana
Green synthesis of stannic oxide nanoparticles for ciprofloxacin degradation: optimization and modelling using a Response Surface Methodology (RSM) based on the box–behnken design
title Green synthesis of stannic oxide nanoparticles for ciprofloxacin degradation: optimization and modelling using a Response Surface Methodology (RSM) based on the box–behnken design
title_full Green synthesis of stannic oxide nanoparticles for ciprofloxacin degradation: optimization and modelling using a Response Surface Methodology (RSM) based on the box–behnken design
title_fullStr Green synthesis of stannic oxide nanoparticles for ciprofloxacin degradation: optimization and modelling using a Response Surface Methodology (RSM) based on the box–behnken design
title_full_unstemmed Green synthesis of stannic oxide nanoparticles for ciprofloxacin degradation: optimization and modelling using a Response Surface Methodology (RSM) based on the box–behnken design
title_short Green synthesis of stannic oxide nanoparticles for ciprofloxacin degradation: optimization and modelling using a Response Surface Methodology (RSM) based on the box–behnken design
title_sort green synthesis of stannic oxide nanoparticles for ciprofloxacin degradation: optimization and modelling using a response surface methodology (rsm) based on the box–behnken design
topic TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/34396/
http://umpir.ump.edu.my/id/eprint/34396/
http://umpir.ump.edu.my/id/eprint/34396/
http://umpir.ump.edu.my/id/eprint/34396/1/Green%20synthesis%20of%20stannic%20oxide%20nanoparticles.pdf