Proximate characteristics and statistical optimization of ultrasound-assisted extraction of high-methoxyl-pectin from Hylocereus polyrhizus peels

Ultrasound-assisted-extraction (UAE) and statistical optimization of significant process parameters for high methoxy pectin (HMP) from Hylocereus polyrhizus peels (HPP) were examined and functional properties and proximate chemical characteristics were evaluated in the present study. Statistically,...

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Main Authors: Rubaiyi, M. Zaid, Mishra, Puranjan, Siti Noredyani, Abdul Rahman, Tabassum, Shabana, Zularisam, Ab Wahid, Mimi Sakinah, Abdul Munaim
Format: Article
Language:English
English
Published: Elsevier Ltd 2020
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/28719/
http://umpir.ump.edu.my/id/eprint/28719/1/Proximate%20characteristics%20and%20statistical%20optimization%20of%20ultrasound-assisted_FULL.pdf
http://umpir.ump.edu.my/id/eprint/28719/2/Proximate%20characteristics%20and%20statistical%20optimization%20of%20ultrasound-assisted%20.pdf
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author Rubaiyi, M. Zaid
Mishra, Puranjan
Siti Noredyani, Abdul Rahman
Tabassum, Shabana
Zularisam, Ab Wahid
Mimi Sakinah, Abdul Munaim
author_facet Rubaiyi, M. Zaid
Mishra, Puranjan
Siti Noredyani, Abdul Rahman
Tabassum, Shabana
Zularisam, Ab Wahid
Mimi Sakinah, Abdul Munaim
author_sort Rubaiyi, M. Zaid
building UMP Institutional Repository
collection Online Access
description Ultrasound-assisted-extraction (UAE) and statistical optimization of significant process parameters for high methoxy pectin (HMP) from Hylocereus polyrhizus peels (HPP) were examined and functional properties and proximate chemical characteristics were evaluated in the present study. Statistically, the maximum yield of HMP of 31.4% with a 56.10% degree of esterification (DE) was achieved by a quadratic polynomial equation and regression analysis of 88% and 86%, respectively. The optimal observed conditions for UAE of HMP were; agitation 250 rpm, extraction temperature 65ᵒC, extraction time at 70 min, extraction solvent with pH value of 2 and LSR of 12:1 (v/w). The proximate characteristics showed 17.93% of mannose, 7.65% of rhamnose, 44.34% of galacturonic acid, 2.8% of glucose, 27.32% of galactose with 79.8% purity of the total sugar extracted from HPP. Conclusively, that the extracted HMP from HPP using UAE possesses a high yield of pectin with a significant lower extraction temperature.
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spelling ump-287192025-05-21T01:29:24Z http://umpir.ump.edu.my/id/eprint/28719/ Proximate characteristics and statistical optimization of ultrasound-assisted extraction of high-methoxyl-pectin from Hylocereus polyrhizus peels Rubaiyi, M. Zaid Mishra, Puranjan Siti Noredyani, Abdul Rahman Tabassum, Shabana Zularisam, Ab Wahid Mimi Sakinah, Abdul Munaim TP Chemical technology Ultrasound-assisted-extraction (UAE) and statistical optimization of significant process parameters for high methoxy pectin (HMP) from Hylocereus polyrhizus peels (HPP) were examined and functional properties and proximate chemical characteristics were evaluated in the present study. Statistically, the maximum yield of HMP of 31.4% with a 56.10% degree of esterification (DE) was achieved by a quadratic polynomial equation and regression analysis of 88% and 86%, respectively. The optimal observed conditions for UAE of HMP were; agitation 250 rpm, extraction temperature 65ᵒC, extraction time at 70 min, extraction solvent with pH value of 2 and LSR of 12:1 (v/w). The proximate characteristics showed 17.93% of mannose, 7.65% of rhamnose, 44.34% of galacturonic acid, 2.8% of glucose, 27.32% of galactose with 79.8% purity of the total sugar extracted from HPP. Conclusively, that the extracted HMP from HPP using UAE possesses a high yield of pectin with a significant lower extraction temperature. Elsevier Ltd 2020-09 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/28719/1/Proximate%20characteristics%20and%20statistical%20optimization%20of%20ultrasound-assisted_FULL.pdf pdf en http://umpir.ump.edu.my/id/eprint/28719/2/Proximate%20characteristics%20and%20statistical%20optimization%20of%20ultrasound-assisted%20.pdf Rubaiyi, M. Zaid and Mishra, Puranjan and Siti Noredyani, Abdul Rahman and Tabassum, Shabana and Zularisam, Ab Wahid and Mimi Sakinah, Abdul Munaim (2020) Proximate characteristics and statistical optimization of ultrasound-assisted extraction of high-methoxyl-pectin from Hylocereus polyrhizus peels. Food and Bioproducts Processing, 123. pp. 134-149. ISSN 0960-3085. (Published) https://doi.org/10.1016/j.fbp.2020.06.011 https://doi.org/10.1016/j.fbp.2020.06.011
spellingShingle TP Chemical technology
Rubaiyi, M. Zaid
Mishra, Puranjan
Siti Noredyani, Abdul Rahman
Tabassum, Shabana
Zularisam, Ab Wahid
Mimi Sakinah, Abdul Munaim
Proximate characteristics and statistical optimization of ultrasound-assisted extraction of high-methoxyl-pectin from Hylocereus polyrhizus peels
title Proximate characteristics and statistical optimization of ultrasound-assisted extraction of high-methoxyl-pectin from Hylocereus polyrhizus peels
title_full Proximate characteristics and statistical optimization of ultrasound-assisted extraction of high-methoxyl-pectin from Hylocereus polyrhizus peels
title_fullStr Proximate characteristics and statistical optimization of ultrasound-assisted extraction of high-methoxyl-pectin from Hylocereus polyrhizus peels
title_full_unstemmed Proximate characteristics and statistical optimization of ultrasound-assisted extraction of high-methoxyl-pectin from Hylocereus polyrhizus peels
title_short Proximate characteristics and statistical optimization of ultrasound-assisted extraction of high-methoxyl-pectin from Hylocereus polyrhizus peels
title_sort proximate characteristics and statistical optimization of ultrasound-assisted extraction of high-methoxyl-pectin from hylocereus polyrhizus peels
topic TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/28719/
http://umpir.ump.edu.my/id/eprint/28719/
http://umpir.ump.edu.my/id/eprint/28719/
http://umpir.ump.edu.my/id/eprint/28719/1/Proximate%20characteristics%20and%20statistical%20optimization%20of%20ultrasound-assisted_FULL.pdf
http://umpir.ump.edu.my/id/eprint/28719/2/Proximate%20characteristics%20and%20statistical%20optimization%20of%20ultrasound-assisted%20.pdf