Studies on ionics conduction properties of modification CMC-PVA based polymer blend electrolytes via impedance approach

In this study, the modification of cellulose derivative namely carboxymethyl cellulose (CMC) blended with polyvinyl alcohol (PVA) and doped with different content of NH4Br based solid polymer electrolytes (SPEs) prepared via solution casting method is investigated. The FTIR analysis demonstrated the...

Full description

Bibliographic Details
Main Authors: Norfatihah, Mazuki, Anwar, P. P. Abdul Majeed, Nagao, Yuki, Ahmad Salihin, Samsudin
Format: Article
Language:English
English
Published: Elsevier Ltd 2020
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/27742/
http://umpir.ump.edu.my/id/eprint/27742/1/Studies%20on%20ionics%20conduction%20properties%20of%20modification%20CMC-PVA.pdf
http://umpir.ump.edu.my/id/eprint/27742/2/Studies%20on%20ionics%20conduction%20properties%20of%20modification%20CMC-PVA.pdf
_version_ 1848822872243437568
author Norfatihah, Mazuki
Anwar, P. P. Abdul Majeed
Nagao, Yuki
Ahmad Salihin, Samsudin
author_facet Norfatihah, Mazuki
Anwar, P. P. Abdul Majeed
Nagao, Yuki
Ahmad Salihin, Samsudin
author_sort Norfatihah, Mazuki
building UMP Institutional Repository
collection Online Access
description In this study, the modification of cellulose derivative namely carboxymethyl cellulose (CMC) blended with polyvinyl alcohol (PVA) and doped with different content of NH4Br based solid polymer electrolytes (SPEs) prepared via solution casting method is investigated. The FTIR analysis demonstrated the interaction between CMC-PVA and NH4Br via COO−. The optimum ionic conductivity at ambient temperature is found to be 3.21 × 10−4 S/cm for the sample containing 20 wt% NH4Br with the lowest percentage of crystallinity and total weight loss. The conductivity-temperature relationship for the entire SPEs system obeys Arrhenius behaviour. Besides that, based on the Nyquist fitting analysis, it is shown that the ionic conductivity of the SPEs is primarily influenced by the ionic mobility as well as the ions diffusion coefficient. The H+ transference number obtained using non-blocking reversible electrode is 0.31, which further indicates that the conduction species is predominantly due to the cationic conduction.
first_indexed 2025-11-15T02:48:08Z
format Article
id ump-27742
institution Universiti Malaysia Pahang
institution_category Local University
language English
English
last_indexed 2025-11-15T02:48:08Z
publishDate 2020
publisher Elsevier Ltd
recordtype eprints
repository_type Digital Repository
spelling ump-277422023-12-04T02:05:39Z http://umpir.ump.edu.my/id/eprint/27742/ Studies on ionics conduction properties of modification CMC-PVA based polymer blend electrolytes via impedance approach Norfatihah, Mazuki Anwar, P. P. Abdul Majeed Nagao, Yuki Ahmad Salihin, Samsudin TP Chemical technology In this study, the modification of cellulose derivative namely carboxymethyl cellulose (CMC) blended with polyvinyl alcohol (PVA) and doped with different content of NH4Br based solid polymer electrolytes (SPEs) prepared via solution casting method is investigated. The FTIR analysis demonstrated the interaction between CMC-PVA and NH4Br via COO−. The optimum ionic conductivity at ambient temperature is found to be 3.21 × 10−4 S/cm for the sample containing 20 wt% NH4Br with the lowest percentage of crystallinity and total weight loss. The conductivity-temperature relationship for the entire SPEs system obeys Arrhenius behaviour. Besides that, based on the Nyquist fitting analysis, it is shown that the ionic conductivity of the SPEs is primarily influenced by the ionic mobility as well as the ions diffusion coefficient. The H+ transference number obtained using non-blocking reversible electrode is 0.31, which further indicates that the conduction species is predominantly due to the cationic conduction. Elsevier Ltd 2020-01 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/27742/1/Studies%20on%20ionics%20conduction%20properties%20of%20modification%20CMC-PVA.pdf pdf en http://umpir.ump.edu.my/id/eprint/27742/2/Studies%20on%20ionics%20conduction%20properties%20of%20modification%20CMC-PVA.pdf Norfatihah, Mazuki and Anwar, P. P. Abdul Majeed and Nagao, Yuki and Ahmad Salihin, Samsudin (2020) Studies on ionics conduction properties of modification CMC-PVA based polymer blend electrolytes via impedance approach. Polymer Testing, 81 (106234). pp. 1-13. ISSN 0142-9418. (Published) https://doi.org/10.1016/j.polymertesting.2019.106234 https://doi.org/10.1016/j.polymertesting.2019.106234
spellingShingle TP Chemical technology
Norfatihah, Mazuki
Anwar, P. P. Abdul Majeed
Nagao, Yuki
Ahmad Salihin, Samsudin
Studies on ionics conduction properties of modification CMC-PVA based polymer blend electrolytes via impedance approach
title Studies on ionics conduction properties of modification CMC-PVA based polymer blend electrolytes via impedance approach
title_full Studies on ionics conduction properties of modification CMC-PVA based polymer blend electrolytes via impedance approach
title_fullStr Studies on ionics conduction properties of modification CMC-PVA based polymer blend electrolytes via impedance approach
title_full_unstemmed Studies on ionics conduction properties of modification CMC-PVA based polymer blend electrolytes via impedance approach
title_short Studies on ionics conduction properties of modification CMC-PVA based polymer blend electrolytes via impedance approach
title_sort studies on ionics conduction properties of modification cmc-pva based polymer blend electrolytes via impedance approach
topic TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/27742/
http://umpir.ump.edu.my/id/eprint/27742/
http://umpir.ump.edu.my/id/eprint/27742/
http://umpir.ump.edu.my/id/eprint/27742/1/Studies%20on%20ionics%20conduction%20properties%20of%20modification%20CMC-PVA.pdf
http://umpir.ump.edu.my/id/eprint/27742/2/Studies%20on%20ionics%20conduction%20properties%20of%20modification%20CMC-PVA.pdf