A bioanalytical method for quantification of telmisartan in rat plasma; development, validation and application to pharmacokinetic study

The telmisartan was determined in a rat plasma using developed and validated a reversed-phase high performance liquid chromatographic (HPLC). The pre-treatment of the plasma sample involving liquid-liquid extraction using ethanol as the extracting solvent. The HPLC method validation has been shown a...

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Main Authors: AL-japairai, Khater Ahmed Saeed, Chatterjee, Bappaditya, Mahmood, Syed, Almurisi, Samah Hamed
Format: Article
Language:English
Published: A and V publication 2021
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/25861/
http://umpir.ump.edu.my/id/eprint/25861/1/A%20Bioanalytical%20Method%20for%20Quantification%20of%20Telmisartan%20in%20rat%20Plasma%20Development%20Validation%20and%20Application%20to%20Pharmacokinetic%20Study.pdf
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author AL-japairai, Khater Ahmed Saeed
Chatterjee, Bappaditya
Mahmood, Syed
Almurisi, Samah Hamed
author_facet AL-japairai, Khater Ahmed Saeed
Chatterjee, Bappaditya
Mahmood, Syed
Almurisi, Samah Hamed
author_sort AL-japairai, Khater Ahmed Saeed
building UMP Institutional Repository
collection Online Access
description The telmisartan was determined in a rat plasma using developed and validated a reversed-phase high performance liquid chromatographic (HPLC). The pre-treatment of the plasma sample involving liquid-liquid extraction using ethanol as the extracting solvent. The HPLC method validation has been shown a linear calibration curve over a plasma concentrations range of 0.7 to 10µg/mL with a correlation coefficient of 0.9979, the limit of detection and the limit of quantification were determined to be 0.025µg/ml and 0.07µg/ml, respectively. The precision and accuracy were in an acceptable limit. The pharmacokinetic parameters of telmisartan were adequately evaluated following a single oral dose (4mg/kg) in Sprague-Dawley rats. The results observed conclude that the developed bioanalytical HPLC method is appropriate and applicable as an analytical tool in the pharmacokinetic study of telmisartan.
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spelling ump-258612021-07-15T09:15:23Z http://umpir.ump.edu.my/id/eprint/25861/ A bioanalytical method for quantification of telmisartan in rat plasma; development, validation and application to pharmacokinetic study AL-japairai, Khater Ahmed Saeed Chatterjee, Bappaditya Mahmood, Syed Almurisi, Samah Hamed Q Science (General) The telmisartan was determined in a rat plasma using developed and validated a reversed-phase high performance liquid chromatographic (HPLC). The pre-treatment of the plasma sample involving liquid-liquid extraction using ethanol as the extracting solvent. The HPLC method validation has been shown a linear calibration curve over a plasma concentrations range of 0.7 to 10µg/mL with a correlation coefficient of 0.9979, the limit of detection and the limit of quantification were determined to be 0.025µg/ml and 0.07µg/ml, respectively. The precision and accuracy were in an acceptable limit. The pharmacokinetic parameters of telmisartan were adequately evaluated following a single oral dose (4mg/kg) in Sprague-Dawley rats. The results observed conclude that the developed bioanalytical HPLC method is appropriate and applicable as an analytical tool in the pharmacokinetic study of telmisartan. A and V publication 2021 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/25861/1/A%20Bioanalytical%20Method%20for%20Quantification%20of%20Telmisartan%20in%20rat%20Plasma%20Development%20Validation%20and%20Application%20to%20Pharmacokinetic%20Study.pdf AL-japairai, Khater Ahmed Saeed and Chatterjee, Bappaditya and Mahmood, Syed and Almurisi, Samah Hamed (2021) A bioanalytical method for quantification of telmisartan in rat plasma; development, validation and application to pharmacokinetic study. Research J. Pharm. and Tech, 14 (4). pp. 2139-2144. ISSN 0974-360X. (Published) https: //doi.org/10.52711/0974-360X.2021.00379
spellingShingle Q Science (General)
AL-japairai, Khater Ahmed Saeed
Chatterjee, Bappaditya
Mahmood, Syed
Almurisi, Samah Hamed
A bioanalytical method for quantification of telmisartan in rat plasma; development, validation and application to pharmacokinetic study
title A bioanalytical method for quantification of telmisartan in rat plasma; development, validation and application to pharmacokinetic study
title_full A bioanalytical method for quantification of telmisartan in rat plasma; development, validation and application to pharmacokinetic study
title_fullStr A bioanalytical method for quantification of telmisartan in rat plasma; development, validation and application to pharmacokinetic study
title_full_unstemmed A bioanalytical method for quantification of telmisartan in rat plasma; development, validation and application to pharmacokinetic study
title_short A bioanalytical method for quantification of telmisartan in rat plasma; development, validation and application to pharmacokinetic study
title_sort bioanalytical method for quantification of telmisartan in rat plasma; development, validation and application to pharmacokinetic study
topic Q Science (General)
url http://umpir.ump.edu.my/id/eprint/25861/
http://umpir.ump.edu.my/id/eprint/25861/
http://umpir.ump.edu.my/id/eprint/25861/1/A%20Bioanalytical%20Method%20for%20Quantification%20of%20Telmisartan%20in%20rat%20Plasma%20Development%20Validation%20and%20Application%20to%20Pharmacokinetic%20Study.pdf