Tubular Carbon Membrane Prepared from PI/NCC: Effects of Pyrolysis Atmosphere

The performance of Tubular Carbon Membrane (TCMs)due to pyrolysis conditions was studied. Dip-coating technique was used to synthesize the P84 co- polyimide/Nanocrystalline cellulose-based TCM, and pure gas O2 and N2 were used to determine the permeation properties of the TCMs. Different atmosphere...

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Main Authors: Norazlianie, Sazali, Wan Norharyati, Wan Salleh, Ahmad Fauzi, Ismail, Nur Izwanne, Mahyon, K., Kadirgama, Mohd Shahrizan, Moslan
Format: Article
Language:English
Published: AIDIC Servizi 2019
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/25528/
http://umpir.ump.edu.my/id/eprint/25528/7/Tubular%20Carbon%20Membrane%20Prepared%20from.pdf
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author Norazlianie, Sazali
Wan Norharyati, Wan Salleh
Ahmad Fauzi, Ismail
Nur Izwanne, Mahyon
K., Kadirgama
Mohd Shahrizan, Moslan
author_facet Norazlianie, Sazali
Wan Norharyati, Wan Salleh
Ahmad Fauzi, Ismail
Nur Izwanne, Mahyon
K., Kadirgama
Mohd Shahrizan, Moslan
author_sort Norazlianie, Sazali
building UMP Institutional Repository
collection Online Access
description The performance of Tubular Carbon Membrane (TCMs)due to pyrolysis conditions was studied. Dip-coating technique was used to synthesize the P84 co- polyimide/Nanocrystalline cellulose-based TCM, and pure gas O2 and N2 were used to determine the permeation properties of the TCMs. Different atmosphere i.e Argon, Nitrogen and Helium were introduced during the heat treatment processes at a flow rate of 200 mL/min to enhance the membrane’s performance. The pyrolysis temperature and heating rate were set at 800 °C and 3°C/min. It was found that the best pyrolysis condition for the preparation of PI/NCC-based TCMs was conducted in Argon atmosphere with the permeance of 3.22±3.21 and 29.90±2.98 GPU for N2, and O2 gas. The membrane also demonstrated that the highest O2/N2 selectivity of 9.29±2.54. In comparisons to all other carbonization atmosphere, preparation of TCMs in Ar atmosphere showed the lowest weight loss and revealed the highest N2 selectivity in this study.
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institution Universiti Malaysia Pahang
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language English
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publisher AIDIC Servizi
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spelling ump-255282019-08-07T06:21:24Z http://umpir.ump.edu.my/id/eprint/25528/ Tubular Carbon Membrane Prepared from PI/NCC: Effects of Pyrolysis Atmosphere Norazlianie, Sazali Wan Norharyati, Wan Salleh Ahmad Fauzi, Ismail Nur Izwanne, Mahyon K., Kadirgama Mohd Shahrizan, Moslan QD Chemistry The performance of Tubular Carbon Membrane (TCMs)due to pyrolysis conditions was studied. Dip-coating technique was used to synthesize the P84 co- polyimide/Nanocrystalline cellulose-based TCM, and pure gas O2 and N2 were used to determine the permeation properties of the TCMs. Different atmosphere i.e Argon, Nitrogen and Helium were introduced during the heat treatment processes at a flow rate of 200 mL/min to enhance the membrane’s performance. The pyrolysis temperature and heating rate were set at 800 °C and 3°C/min. It was found that the best pyrolysis condition for the preparation of PI/NCC-based TCMs was conducted in Argon atmosphere with the permeance of 3.22±3.21 and 29.90±2.98 GPU for N2, and O2 gas. The membrane also demonstrated that the highest O2/N2 selectivity of 9.29±2.54. In comparisons to all other carbonization atmosphere, preparation of TCMs in Ar atmosphere showed the lowest weight loss and revealed the highest N2 selectivity in this study. AIDIC Servizi 2019 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/25528/7/Tubular%20Carbon%20Membrane%20Prepared%20from.pdf Norazlianie, Sazali and Wan Norharyati, Wan Salleh and Ahmad Fauzi, Ismail and Nur Izwanne, Mahyon and K., Kadirgama and Mohd Shahrizan, Moslan (2019) Tubular Carbon Membrane Prepared from PI/NCC: Effects of Pyrolysis Atmosphere. Chemical Engineering Transactions, 72. pp. 409-414. ISSN 2283-9216. (Published) https://doi.org/10.3303/CET1972069 https://doi.org/10.3303/CET1972069
spellingShingle QD Chemistry
Norazlianie, Sazali
Wan Norharyati, Wan Salleh
Ahmad Fauzi, Ismail
Nur Izwanne, Mahyon
K., Kadirgama
Mohd Shahrizan, Moslan
Tubular Carbon Membrane Prepared from PI/NCC: Effects of Pyrolysis Atmosphere
title Tubular Carbon Membrane Prepared from PI/NCC: Effects of Pyrolysis Atmosphere
title_full Tubular Carbon Membrane Prepared from PI/NCC: Effects of Pyrolysis Atmosphere
title_fullStr Tubular Carbon Membrane Prepared from PI/NCC: Effects of Pyrolysis Atmosphere
title_full_unstemmed Tubular Carbon Membrane Prepared from PI/NCC: Effects of Pyrolysis Atmosphere
title_short Tubular Carbon Membrane Prepared from PI/NCC: Effects of Pyrolysis Atmosphere
title_sort tubular carbon membrane prepared from pi/ncc: effects of pyrolysis atmosphere
topic QD Chemistry
url http://umpir.ump.edu.my/id/eprint/25528/
http://umpir.ump.edu.my/id/eprint/25528/
http://umpir.ump.edu.my/id/eprint/25528/
http://umpir.ump.edu.my/id/eprint/25528/7/Tubular%20Carbon%20Membrane%20Prepared%20from.pdf