Investigation on pre-treatment process in microcrystalline cellulose (MCC) from oil palm empty fruit bunch (EFB)

In this study, microcrystalline cellulose (MCC) was extracted from empty fruit bunch (EFB) with alkaline treatment, bleaching and acid hydrolysis treatment and its properties were compared with commercial MCC. Two conditions were optimized in this study which are fiber consistency and sodium hydroxi...

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Main Authors: Muhammad Arif Fahmi, Supian, Khairatun Najwa, Mohd Amin, Saidatul Shima, Jamari, Shahril, Mohamad
Format: Article
Language:English
Published: Universiti Malaysia Pahang 2018
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/24430/
http://umpir.ump.edu.my/id/eprint/24430/1/Investigation%20on%20pre-treatment%20process%20in%20microcrystalline%20cellulose%20%28MCC%29%20from%20oil%20palm%20empty%20fruit%20bunch%20%28EFB%29.pdf
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author Muhammad Arif Fahmi, Supian
Khairatun Najwa, Mohd Amin
Saidatul Shima, Jamari
Shahril, Mohamad
author_facet Muhammad Arif Fahmi, Supian
Khairatun Najwa, Mohd Amin
Saidatul Shima, Jamari
Shahril, Mohamad
author_sort Muhammad Arif Fahmi, Supian
building UMP Institutional Repository
collection Online Access
description In this study, microcrystalline cellulose (MCC) was extracted from empty fruit bunch (EFB) with alkaline treatment, bleaching and acid hydrolysis treatment and its properties were compared with commercial MCC. Two conditions were optimized in this study which are fiber consistency and sodium hydroxide (NaOH) concentration in alkaline pretreatment. The obtained optimum consistency and alkaline concentration are 5% and 20% respectively. The physicochemical and morphological characteristics, elemental composition and size distribution of the obtained alpha cellulose and MCC were analyzed in this work. Fourier transform infrared spectroscopy (FTIR) analysis provided clear evidence that the characteristic peak of lignin and hemicellulose were absent in the spectrum of the alpha cellulose and MCC. The difference in surface morphology and aggregation between alpha cellulose, MCC and commercialized MCC were observed by scanning electron microscopy (SEM). The mean length of approximately 251.3 μm, 41.4 μm and 138.6 μm were measured for alpha cellulose, MCC and commercialized MCC respectively. Thus, the isolated MCC from EFB has a good potential to be utilized as reinforcing agent in green composites and may be a precursor for future roselle derived nanocellulose, and thus a promising subject in nanocomposite research.
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spelling ump-244302019-03-19T04:10:48Z http://umpir.ump.edu.my/id/eprint/24430/ Investigation on pre-treatment process in microcrystalline cellulose (MCC) from oil palm empty fruit bunch (EFB) Muhammad Arif Fahmi, Supian Khairatun Najwa, Mohd Amin Saidatul Shima, Jamari Shahril, Mohamad TP Chemical technology In this study, microcrystalline cellulose (MCC) was extracted from empty fruit bunch (EFB) with alkaline treatment, bleaching and acid hydrolysis treatment and its properties were compared with commercial MCC. Two conditions were optimized in this study which are fiber consistency and sodium hydroxide (NaOH) concentration in alkaline pretreatment. The obtained optimum consistency and alkaline concentration are 5% and 20% respectively. The physicochemical and morphological characteristics, elemental composition and size distribution of the obtained alpha cellulose and MCC were analyzed in this work. Fourier transform infrared spectroscopy (FTIR) analysis provided clear evidence that the characteristic peak of lignin and hemicellulose were absent in the spectrum of the alpha cellulose and MCC. The difference in surface morphology and aggregation between alpha cellulose, MCC and commercialized MCC were observed by scanning electron microscopy (SEM). The mean length of approximately 251.3 μm, 41.4 μm and 138.6 μm were measured for alpha cellulose, MCC and commercialized MCC respectively. Thus, the isolated MCC from EFB has a good potential to be utilized as reinforcing agent in green composites and may be a precursor for future roselle derived nanocellulose, and thus a promising subject in nanocomposite research. Universiti Malaysia Pahang 2018 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/24430/1/Investigation%20on%20pre-treatment%20process%20in%20microcrystalline%20cellulose%20%28MCC%29%20from%20oil%20palm%20empty%20fruit%20bunch%20%28EFB%29.pdf Muhammad Arif Fahmi, Supian and Khairatun Najwa, Mohd Amin and Saidatul Shima, Jamari and Shahril, Mohamad (2018) Investigation on pre-treatment process in microcrystalline cellulose (MCC) from oil palm empty fruit bunch (EFB). Journal of Chemical Engineering and Industrial Biotechnology (JCEIB), 3. pp. 87-96. ISSN 0126-8139. (Published) http://jceib.ump.edu.my/index.php/en/volume-3-docman/89-investigation-on-pre-treatment-process-in-microcrystalline-cellulose-mcc-from-oil-palm-empty-fruit-bunch-efb https://doi.org/10.15282/JCEIB-V3-09.28/3/2018/3.3
spellingShingle TP Chemical technology
Muhammad Arif Fahmi, Supian
Khairatun Najwa, Mohd Amin
Saidatul Shima, Jamari
Shahril, Mohamad
Investigation on pre-treatment process in microcrystalline cellulose (MCC) from oil palm empty fruit bunch (EFB)
title Investigation on pre-treatment process in microcrystalline cellulose (MCC) from oil palm empty fruit bunch (EFB)
title_full Investigation on pre-treatment process in microcrystalline cellulose (MCC) from oil palm empty fruit bunch (EFB)
title_fullStr Investigation on pre-treatment process in microcrystalline cellulose (MCC) from oil palm empty fruit bunch (EFB)
title_full_unstemmed Investigation on pre-treatment process in microcrystalline cellulose (MCC) from oil palm empty fruit bunch (EFB)
title_short Investigation on pre-treatment process in microcrystalline cellulose (MCC) from oil palm empty fruit bunch (EFB)
title_sort investigation on pre-treatment process in microcrystalline cellulose (mcc) from oil palm empty fruit bunch (efb)
topic TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/24430/
http://umpir.ump.edu.my/id/eprint/24430/
http://umpir.ump.edu.my/id/eprint/24430/
http://umpir.ump.edu.my/id/eprint/24430/1/Investigation%20on%20pre-treatment%20process%20in%20microcrystalline%20cellulose%20%28MCC%29%20from%20oil%20palm%20empty%20fruit%20bunch%20%28EFB%29.pdf