Characterization of polyamide 6.10 composites incorporated with microcrystalline cellulose fiber: Effects of fiber loading and impact modifier

Microcrystalline cellulose (MCC) fiber‐reinforced polyamide 6.10 (PA) composites were prepared in the presence of an impact modifier (IM), exxelor VA1803 (VA), by melt compounding process. Fiber loading was considered from 20 to 30 wt.%, whereas IM was varied from 2.0 to 5.0 wt.%. Composites were ch...

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Main Authors: Beg, M. D. H., Islam, Muhammad Remanul, Al Mamun, Abdullah, Heim, Hans‐Peter, Feldmann, Maik, Akindoyo, John Olabode
Format: Article
Language:English
Published: Wiley 2018
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/23873/
http://umpir.ump.edu.my/id/eprint/23873/1/Characterization%20of%20polyamide%206.10%20composites%20incorporated1.pdf
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author Beg, M. D. H.
Islam, Muhammad Remanul
Al Mamun, Abdullah
Heim, Hans‐Peter
Feldmann, Maik
Akindoyo, John Olabode
author_facet Beg, M. D. H.
Islam, Muhammad Remanul
Al Mamun, Abdullah
Heim, Hans‐Peter
Feldmann, Maik
Akindoyo, John Olabode
author_sort Beg, M. D. H.
building UMP Institutional Repository
collection Online Access
description Microcrystalline cellulose (MCC) fiber‐reinforced polyamide 6.10 (PA) composites were prepared in the presence of an impact modifier (IM), exxelor VA1803 (VA), by melt compounding process. Fiber loading was considered from 20 to 30 wt.%, whereas IM was varied from 2.0 to 5.0 wt.%. Composites were characterized by tensile test, impact test, dynamic thermal mechanical analysis (DTMA), differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), and X‐ray diffraction (XRD). Composites’ fractured surfaces were examined by scanning electron microscope (SEM). In addition, fiber size distribution was also analyzed. Result analyses showed that the fiber incorporation changed the tensile strength (TS) slightly, but the tensile modulus (TM) significantly. The TM was found to be improved by 45% at the amount of fiber loading of 30 wt.%. Moreover, the thermomechanical properties revealed that the storage modulus (SM) and loss modulus (LM) were increased due to the incorporation of MCC, which was improved further by the uses of 5.0 wt.% of VA. The MCC possess high crystallinity index and high crystallite size along with enhanced mechanical and thermal properties. Therefore, the extraordinary benefit of using MCC in PA was evaluated in terms of thermomechanical, structural, and thermal properties in the presence of the impact modifier.
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spelling ump-238732019-10-09T07:12:25Z http://umpir.ump.edu.my/id/eprint/23873/ Characterization of polyamide 6.10 composites incorporated with microcrystalline cellulose fiber: Effects of fiber loading and impact modifier Beg, M. D. H. Islam, Muhammad Remanul Al Mamun, Abdullah Heim, Hans‐Peter Feldmann, Maik Akindoyo, John Olabode TP Chemical technology Microcrystalline cellulose (MCC) fiber‐reinforced polyamide 6.10 (PA) composites were prepared in the presence of an impact modifier (IM), exxelor VA1803 (VA), by melt compounding process. Fiber loading was considered from 20 to 30 wt.%, whereas IM was varied from 2.0 to 5.0 wt.%. Composites were characterized by tensile test, impact test, dynamic thermal mechanical analysis (DTMA), differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), and X‐ray diffraction (XRD). Composites’ fractured surfaces were examined by scanning electron microscope (SEM). In addition, fiber size distribution was also analyzed. Result analyses showed that the fiber incorporation changed the tensile strength (TS) slightly, but the tensile modulus (TM) significantly. The TM was found to be improved by 45% at the amount of fiber loading of 30 wt.%. Moreover, the thermomechanical properties revealed that the storage modulus (SM) and loss modulus (LM) were increased due to the incorporation of MCC, which was improved further by the uses of 5.0 wt.% of VA. The MCC possess high crystallinity index and high crystallite size along with enhanced mechanical and thermal properties. Therefore, the extraordinary benefit of using MCC in PA was evaluated in terms of thermomechanical, structural, and thermal properties in the presence of the impact modifier. Wiley 2018-08-14 Article NonPeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/23873/1/Characterization%20of%20polyamide%206.10%20composites%20incorporated1.pdf Beg, M. D. H. and Islam, Muhammad Remanul and Al Mamun, Abdullah and Heim, Hans‐Peter and Feldmann, Maik and Akindoyo, John Olabode (2018) Characterization of polyamide 6.10 composites incorporated with microcrystalline cellulose fiber: Effects of fiber loading and impact modifier. Advances in Polymer Technology, 37 (8). pp. 3412-3420. ISSN 1098-2329. (Published) https://doi.org/10.1002/adv.22125 https://doi.org/10.1002/adv.22125
spellingShingle TP Chemical technology
Beg, M. D. H.
Islam, Muhammad Remanul
Al Mamun, Abdullah
Heim, Hans‐Peter
Feldmann, Maik
Akindoyo, John Olabode
Characterization of polyamide 6.10 composites incorporated with microcrystalline cellulose fiber: Effects of fiber loading and impact modifier
title Characterization of polyamide 6.10 composites incorporated with microcrystalline cellulose fiber: Effects of fiber loading and impact modifier
title_full Characterization of polyamide 6.10 composites incorporated with microcrystalline cellulose fiber: Effects of fiber loading and impact modifier
title_fullStr Characterization of polyamide 6.10 composites incorporated with microcrystalline cellulose fiber: Effects of fiber loading and impact modifier
title_full_unstemmed Characterization of polyamide 6.10 composites incorporated with microcrystalline cellulose fiber: Effects of fiber loading and impact modifier
title_short Characterization of polyamide 6.10 composites incorporated with microcrystalline cellulose fiber: Effects of fiber loading and impact modifier
title_sort characterization of polyamide 6.10 composites incorporated with microcrystalline cellulose fiber: effects of fiber loading and impact modifier
topic TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/23873/
http://umpir.ump.edu.my/id/eprint/23873/
http://umpir.ump.edu.my/id/eprint/23873/
http://umpir.ump.edu.my/id/eprint/23873/1/Characterization%20of%20polyamide%206.10%20composites%20incorporated1.pdf