Hydrogen separation through pi/ncc carbon membrane: effect of stabilization environment and heating rates

separation of hydrogen with nitrogen. TCMs were fabricated by dip coating process using P84 copolyimide as a main precursor with blending of Nanocrysttaline cellulose (NCC) as an additives. Previously, it was shown that changing the time, temperature, or environment of the carbonization protocol for...

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Main Authors: Norazlianie, Sazali, K., Kadirgama, Wan Norharyati, Wan Salleh, F. E., C. Othman, N. H., Ismail, A. F., Ismail
Format: Conference or Workshop Item
Language:English
Published: 2018
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/23866/
http://umpir.ump.edu.my/id/eprint/23866/1/28.%20Hydrogen%20separation%20through%20pi-ncc%20carbon%20membrane.pdf
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author Norazlianie, Sazali
K., Kadirgama
Wan Norharyati, Wan Salleh
F. E., C. Othman
N. H., Ismail
A. F., Ismail
author_facet Norazlianie, Sazali
K., Kadirgama
Wan Norharyati, Wan Salleh
F. E., C. Othman
N. H., Ismail
A. F., Ismail
author_sort Norazlianie, Sazali
building UMP Institutional Repository
collection Online Access
description separation of hydrogen with nitrogen. TCMs were fabricated by dip coating process using P84 copolyimide as a main precursor with blending of Nanocrysttaline cellulose (NCC) as an additives. Previously, it was shown that changing the time, temperature, or environment of the carbonization protocol for a commercially available PI/NCC altered the final properties of the carbons produced. A large variety of TCMs for gas separation have been developed by simple carbonization of a PI/NCC deposited on a ceramic tubular support. In this study, heating rates (1, 3, 5, and 7 oC/min) and stabilization environment (Argon, Nitrogen, and Helium) were investigated and the effect on permeation were determined for all resultant TCMs. In recent study, the modifications on the carbonization parameters such as stabilization conditions and heating rates during fabrication of PI/NCC-based carbon membranes could affect their gas separation performance. It was observed that stabilization under Argon environment produced carbon membranes with high separation performance while heating rates of 3oC/min improved the membrane selectivity but reduced the membrane’s permeability. In literature, the rate of evolution of the volatile compounds can be determined by carbonization heating rate as it is believed could affect the microstructure of the carbon membranes [1]. The variation in carbonization heating rates have showed different gas separation results on the PI/NCC carbon membranes as represented in Table 1. The data obtained showed an average value from at least three different PI/NCC carbon membranes with small error analysis of ±10% for both selectivity and permeance value.
first_indexed 2025-11-15T02:32:47Z
format Conference or Workshop Item
id ump-23866
institution Universiti Malaysia Pahang
institution_category Local University
language English
last_indexed 2025-11-15T02:32:47Z
publishDate 2018
recordtype eprints
repository_type Digital Repository
spelling ump-238662020-04-30T01:53:41Z http://umpir.ump.edu.my/id/eprint/23866/ Hydrogen separation through pi/ncc carbon membrane: effect of stabilization environment and heating rates Norazlianie, Sazali K., Kadirgama Wan Norharyati, Wan Salleh F. E., C. Othman N. H., Ismail A. F., Ismail TP Chemical technology separation of hydrogen with nitrogen. TCMs were fabricated by dip coating process using P84 copolyimide as a main precursor with blending of Nanocrysttaline cellulose (NCC) as an additives. Previously, it was shown that changing the time, temperature, or environment of the carbonization protocol for a commercially available PI/NCC altered the final properties of the carbons produced. A large variety of TCMs for gas separation have been developed by simple carbonization of a PI/NCC deposited on a ceramic tubular support. In this study, heating rates (1, 3, 5, and 7 oC/min) and stabilization environment (Argon, Nitrogen, and Helium) were investigated and the effect on permeation were determined for all resultant TCMs. In recent study, the modifications on the carbonization parameters such as stabilization conditions and heating rates during fabrication of PI/NCC-based carbon membranes could affect their gas separation performance. It was observed that stabilization under Argon environment produced carbon membranes with high separation performance while heating rates of 3oC/min improved the membrane selectivity but reduced the membrane’s permeability. In literature, the rate of evolution of the volatile compounds can be determined by carbonization heating rate as it is believed could affect the microstructure of the carbon membranes [1]. The variation in carbonization heating rates have showed different gas separation results on the PI/NCC carbon membranes as represented in Table 1. The data obtained showed an average value from at least three different PI/NCC carbon membranes with small error analysis of ±10% for both selectivity and permeance value. 2018-08 Conference or Workshop Item PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/23866/1/28.%20Hydrogen%20separation%20through%20pi-ncc%20carbon%20membrane.pdf Norazlianie, Sazali and K., Kadirgama and Wan Norharyati, Wan Salleh and F. E., C. Othman and N. H., Ismail and A. F., Ismail (2018) Hydrogen separation through pi/ncc carbon membrane: effect of stabilization environment and heating rates. In: 4th International Conference Of Chemical Engineering And Industrial Biotechnology (ICCEIB 2018) , 1-2 Aug 2018 , Seri Pacific Hotel, Kuala Lumpur. pp. 261-262.. (Submitted) (Submitted)
spellingShingle TP Chemical technology
Norazlianie, Sazali
K., Kadirgama
Wan Norharyati, Wan Salleh
F. E., C. Othman
N. H., Ismail
A. F., Ismail
Hydrogen separation through pi/ncc carbon membrane: effect of stabilization environment and heating rates
title Hydrogen separation through pi/ncc carbon membrane: effect of stabilization environment and heating rates
title_full Hydrogen separation through pi/ncc carbon membrane: effect of stabilization environment and heating rates
title_fullStr Hydrogen separation through pi/ncc carbon membrane: effect of stabilization environment and heating rates
title_full_unstemmed Hydrogen separation through pi/ncc carbon membrane: effect of stabilization environment and heating rates
title_short Hydrogen separation through pi/ncc carbon membrane: effect of stabilization environment and heating rates
title_sort hydrogen separation through pi/ncc carbon membrane: effect of stabilization environment and heating rates
topic TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/23866/
http://umpir.ump.edu.my/id/eprint/23866/1/28.%20Hydrogen%20separation%20through%20pi-ncc%20carbon%20membrane.pdf