Synthesis of alumina-CaO-KI catalyst for the production of biodiesel from rubber seed oil [Sintesis mangkin alumina-CaO-KI untuk penghasilan biodiesel daripada minyak biji getah]

In this research, biodiesel was produced by transesterification of rubber seed oil with methanol catalyzed by three types of alumina-supported catalyst. The catalysts were Al2O3 -CaO, Al2O3 -KI, and Al2O3 -CaO-KI. The catalysts were prepared by heating a mixture of alumina and the corresponding salt...

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Main Authors: Abdul Razak, Zainal Kifli, Shahida Hanum, Kamarullah, Siti Norhafiza, Mohd Khazaai, Gaanty Pragas, Maniam
Format: Article
Language:English
Published: Universiti Kebangsaan Malaysia 2018
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/21626/
http://umpir.ump.edu.my/id/eprint/21626/1/Synthesis%20of%20alumina-cao-ki%20catalyst%20for%20the%20production%20of%20biodiesel%20from%20rubber%20seed%20oil.pdf
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author Abdul Razak, Zainal Kifli
Shahida Hanum, Kamarullah
Siti Norhafiza, Mohd Khazaai
Gaanty Pragas, Maniam
author_facet Abdul Razak, Zainal Kifli
Shahida Hanum, Kamarullah
Siti Norhafiza, Mohd Khazaai
Gaanty Pragas, Maniam
author_sort Abdul Razak, Zainal Kifli
building UMP Institutional Repository
collection Online Access
description In this research, biodiesel was produced by transesterification of rubber seed oil with methanol catalyzed by three types of alumina-supported catalyst. The catalysts were Al2O3 -CaO, Al2O3 -KI, and Al2O3 -CaO-KI. The catalysts were prepared by heating a mixture of alumina and the corresponding salt in a furnace at 700 oC. Transesterification reactions were carried out at 65 °C using a mixture of rubber seed oil: methanol of mass ratio 1:9 with different catalyst loadings between 0 and 3.5%. The optimum catalyst loading was at 2.0% for all types of catalyst and Al2O3 -CaO-KI gave the highest yield (91.6%) followed by Al2O3 -KI (90.7%) and Al2O3 -CaO (63.5%). The catalyst Al2O3 -CaO-KI also gave high biodiesel yields over a wider range of catalyst loadings compared to the other two catalysts. Reactions were also carried out at different temperatures (25, 40 and 65°C). It was observed that the yield increased drastically with increasing reaction temperature. At all temperatures the Al2O3 -CaO-KI catalyst gave the highest yield. Therefore, the study showed that among these three catalysts the most productive was Al2O3 -CaO-KI, (100:30:35).
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format Article
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institution Universiti Malaysia Pahang
institution_category Local University
language English
last_indexed 2025-11-15T02:24:39Z
publishDate 2018
publisher Universiti Kebangsaan Malaysia
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spelling ump-216262018-09-14T04:23:46Z http://umpir.ump.edu.my/id/eprint/21626/ Synthesis of alumina-CaO-KI catalyst for the production of biodiesel from rubber seed oil [Sintesis mangkin alumina-CaO-KI untuk penghasilan biodiesel daripada minyak biji getah] Abdul Razak, Zainal Kifli Shahida Hanum, Kamarullah Siti Norhafiza, Mohd Khazaai Gaanty Pragas, Maniam Q Science (General) In this research, biodiesel was produced by transesterification of rubber seed oil with methanol catalyzed by three types of alumina-supported catalyst. The catalysts were Al2O3 -CaO, Al2O3 -KI, and Al2O3 -CaO-KI. The catalysts were prepared by heating a mixture of alumina and the corresponding salt in a furnace at 700 oC. Transesterification reactions were carried out at 65 °C using a mixture of rubber seed oil: methanol of mass ratio 1:9 with different catalyst loadings between 0 and 3.5%. The optimum catalyst loading was at 2.0% for all types of catalyst and Al2O3 -CaO-KI gave the highest yield (91.6%) followed by Al2O3 -KI (90.7%) and Al2O3 -CaO (63.5%). The catalyst Al2O3 -CaO-KI also gave high biodiesel yields over a wider range of catalyst loadings compared to the other two catalysts. Reactions were also carried out at different temperatures (25, 40 and 65°C). It was observed that the yield increased drastically with increasing reaction temperature. At all temperatures the Al2O3 -CaO-KI catalyst gave the highest yield. Therefore, the study showed that among these three catalysts the most productive was Al2O3 -CaO-KI, (100:30:35). Universiti Kebangsaan Malaysia 2018-04 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/21626/1/Synthesis%20of%20alumina-cao-ki%20catalyst%20for%20the%20production%20of%20biodiesel%20from%20rubber%20seed%20oil.pdf Abdul Razak, Zainal Kifli and Shahida Hanum, Kamarullah and Siti Norhafiza, Mohd Khazaai and Gaanty Pragas, Maniam (2018) Synthesis of alumina-CaO-KI catalyst for the production of biodiesel from rubber seed oil [Sintesis mangkin alumina-CaO-KI untuk penghasilan biodiesel daripada minyak biji getah]. Malaysian Journal of Analytical Sciences, 22 (2). pp. 279-285. ISSN 1394-2506. (Published) http://www.ukm.my/mjas/v22_n2/pdf/ZainalKifli_22_2_13.pdf 10.17576/mjas-2018-2202-13
spellingShingle Q Science (General)
Abdul Razak, Zainal Kifli
Shahida Hanum, Kamarullah
Siti Norhafiza, Mohd Khazaai
Gaanty Pragas, Maniam
Synthesis of alumina-CaO-KI catalyst for the production of biodiesel from rubber seed oil [Sintesis mangkin alumina-CaO-KI untuk penghasilan biodiesel daripada minyak biji getah]
title Synthesis of alumina-CaO-KI catalyst for the production of biodiesel from rubber seed oil [Sintesis mangkin alumina-CaO-KI untuk penghasilan biodiesel daripada minyak biji getah]
title_full Synthesis of alumina-CaO-KI catalyst for the production of biodiesel from rubber seed oil [Sintesis mangkin alumina-CaO-KI untuk penghasilan biodiesel daripada minyak biji getah]
title_fullStr Synthesis of alumina-CaO-KI catalyst for the production of biodiesel from rubber seed oil [Sintesis mangkin alumina-CaO-KI untuk penghasilan biodiesel daripada minyak biji getah]
title_full_unstemmed Synthesis of alumina-CaO-KI catalyst for the production of biodiesel from rubber seed oil [Sintesis mangkin alumina-CaO-KI untuk penghasilan biodiesel daripada minyak biji getah]
title_short Synthesis of alumina-CaO-KI catalyst for the production of biodiesel from rubber seed oil [Sintesis mangkin alumina-CaO-KI untuk penghasilan biodiesel daripada minyak biji getah]
title_sort synthesis of alumina-cao-ki catalyst for the production of biodiesel from rubber seed oil [sintesis mangkin alumina-cao-ki untuk penghasilan biodiesel daripada minyak biji getah]
topic Q Science (General)
url http://umpir.ump.edu.my/id/eprint/21626/
http://umpir.ump.edu.my/id/eprint/21626/
http://umpir.ump.edu.my/id/eprint/21626/
http://umpir.ump.edu.my/id/eprint/21626/1/Synthesis%20of%20alumina-cao-ki%20catalyst%20for%20the%20production%20of%20biodiesel%20from%20rubber%20seed%20oil.pdf