Synthesis, characterisation and thermo-physical investigations on magnesia nanoparticles dispersed in ethylene glycol–DI water (50:50)

In the present work, magnesia nanoparticles (17 nm) were synthesised by solution combustion and characterised using X-ray diffraction and scanning electron microscopy. Nanofluid prepared by magnesia dispersion in ethylene glycol and deionised water (50:50) is characterised using Fourier transform in...

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Main Authors: Krishnan Sasidharan, Suseel Jai, KrishnaMurthy, Nagarajan Parasumanna, R., Mamat, Sathyamurthy, R.
Format: Article
Language:English
Published: The Institution of Engineering and Technology 2018
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/21063/
http://umpir.ump.edu.my/id/eprint/21063/1/Synthesis%2C%20characterisation%20and%20thermo-physical%20investigations%20on%20magnesia%20nanoparticles%20dispersed.pdf
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author Krishnan Sasidharan, Suseel Jai
KrishnaMurthy, Nagarajan Parasumanna
R., Mamat
Sathyamurthy, R.
author_facet Krishnan Sasidharan, Suseel Jai
KrishnaMurthy, Nagarajan Parasumanna
R., Mamat
Sathyamurthy, R.
author_sort Krishnan Sasidharan, Suseel Jai
building UMP Institutional Repository
collection Online Access
description In the present work, magnesia nanoparticles (17 nm) were synthesised by solution combustion and characterised using X-ray diffraction and scanning electron microscopy. Nanofluid prepared by magnesia dispersion in ethylene glycol and deionised water (50:50) is characterised using Fourier transform infrared, dynamic light scattering (DLS) and Zeta potential measurement. The -41 mV zeta potential confirms nanofluid stability. The average particle size in the nanofluid obtained by the DLS method is 33 nm, whereas the crystallite size is 17 nm as per the Scherrer relation. The nanofluid properties were determined under varying volume concentration (0.025, 0.05, 0.1, 0.2%) and temperature (25–60°C). The viscosity measured by using a rotational viscometer decreases with increase in the temperature, whereas the thermal conductivity and specific heat, measured by using a KD2 Pro analyser and a differential scanning calorimeter, respectively, increases. With the increase in volume concentration, thermal conductivity, and viscosity increases, whereas specific heat decreases. The maximum thermal conductivity enhancement and specific heat diminution was 15.6 and 20.5%, respectively, for 0.2% concentration and the minimum viscosity was 2.2% for 0.025% concentration at 60°C. Based on the measured data, new correlations have been proposed.
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language English
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publisher The Institution of Engineering and Technology
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spelling ump-210632018-08-28T08:23:25Z http://umpir.ump.edu.my/id/eprint/21063/ Synthesis, characterisation and thermo-physical investigations on magnesia nanoparticles dispersed in ethylene glycol–DI water (50:50) Krishnan Sasidharan, Suseel Jai KrishnaMurthy, Nagarajan Parasumanna R., Mamat Sathyamurthy, R. TJ Mechanical engineering and machinery In the present work, magnesia nanoparticles (17 nm) were synthesised by solution combustion and characterised using X-ray diffraction and scanning electron microscopy. Nanofluid prepared by magnesia dispersion in ethylene glycol and deionised water (50:50) is characterised using Fourier transform infrared, dynamic light scattering (DLS) and Zeta potential measurement. The -41 mV zeta potential confirms nanofluid stability. The average particle size in the nanofluid obtained by the DLS method is 33 nm, whereas the crystallite size is 17 nm as per the Scherrer relation. The nanofluid properties were determined under varying volume concentration (0.025, 0.05, 0.1, 0.2%) and temperature (25–60°C). The viscosity measured by using a rotational viscometer decreases with increase in the temperature, whereas the thermal conductivity and specific heat, measured by using a KD2 Pro analyser and a differential scanning calorimeter, respectively, increases. With the increase in volume concentration, thermal conductivity, and viscosity increases, whereas specific heat decreases. The maximum thermal conductivity enhancement and specific heat diminution was 15.6 and 20.5%, respectively, for 0.2% concentration and the minimum viscosity was 2.2% for 0.025% concentration at 60°C. Based on the measured data, new correlations have been proposed. The Institution of Engineering and Technology 2018-03 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/21063/1/Synthesis%2C%20characterisation%20and%20thermo-physical%20investigations%20on%20magnesia%20nanoparticles%20dispersed.pdf Krishnan Sasidharan, Suseel Jai and KrishnaMurthy, Nagarajan Parasumanna and R., Mamat and Sathyamurthy, R. (2018) Synthesis, characterisation and thermo-physical investigations on magnesia nanoparticles dispersed in ethylene glycol–DI water (50:50). IET Micro & Nano Letters, 13 (3). pp. 335-340. ISSN 1750-0443. (Published) https://ieeexplore.ieee.org/document/8306346/ 10.1049/mnl.2017.0484
spellingShingle TJ Mechanical engineering and machinery
Krishnan Sasidharan, Suseel Jai
KrishnaMurthy, Nagarajan Parasumanna
R., Mamat
Sathyamurthy, R.
Synthesis, characterisation and thermo-physical investigations on magnesia nanoparticles dispersed in ethylene glycol–DI water (50:50)
title Synthesis, characterisation and thermo-physical investigations on magnesia nanoparticles dispersed in ethylene glycol–DI water (50:50)
title_full Synthesis, characterisation and thermo-physical investigations on magnesia nanoparticles dispersed in ethylene glycol–DI water (50:50)
title_fullStr Synthesis, characterisation and thermo-physical investigations on magnesia nanoparticles dispersed in ethylene glycol–DI water (50:50)
title_full_unstemmed Synthesis, characterisation and thermo-physical investigations on magnesia nanoparticles dispersed in ethylene glycol–DI water (50:50)
title_short Synthesis, characterisation and thermo-physical investigations on magnesia nanoparticles dispersed in ethylene glycol–DI water (50:50)
title_sort synthesis, characterisation and thermo-physical investigations on magnesia nanoparticles dispersed in ethylene glycol–di water (50:50)
topic TJ Mechanical engineering and machinery
url http://umpir.ump.edu.my/id/eprint/21063/
http://umpir.ump.edu.my/id/eprint/21063/
http://umpir.ump.edu.my/id/eprint/21063/
http://umpir.ump.edu.my/id/eprint/21063/1/Synthesis%2C%20characterisation%20and%20thermo-physical%20investigations%20on%20magnesia%20nanoparticles%20dispersed.pdf