Synthesis of Nanofiltration Membrane Developed from Triethanolamine (TEOA) and Trimesoyl Chloride (TMC) for Separation of Xylose from Glucose

Synthesis of thin film composite (TFC) nanofilt ration (NF) membrane has experienced tremendous development since the concept of interfacial polymerisation (IP) was first introduced. One of its new application is on the separation of xylose from glucos e in...

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Main Authors: Nurul Fatihah, Mahamad Roli, Wan Mohd Hafizuddin, Wan Yussof, Syed Mohd Saufi, Tuan Chik, Mazrul Nizam, Abu Seman, Abdul W., Mohammad
Format: Article
Language:English
Published: AIDIC Servizi 2017
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/19799/
http://umpir.ump.edu.my/id/eprint/19799/1/fkksa-2017-fatiha-Synthesis%20of%20Nanofiltration%20Membrane%20Developed.pdf
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author Nurul Fatihah, Mahamad Roli
Wan Mohd Hafizuddin, Wan Yussof
Syed Mohd Saufi, Tuan Chik
Mazrul Nizam, Abu Seman
Abdul W., Mohammad
author_facet Nurul Fatihah, Mahamad Roli
Wan Mohd Hafizuddin, Wan Yussof
Syed Mohd Saufi, Tuan Chik
Mazrul Nizam, Abu Seman
Abdul W., Mohammad
author_sort Nurul Fatihah, Mahamad Roli
building UMP Institutional Repository
collection Online Access
description Synthesis of thin film composite (TFC) nanofilt ration (NF) membrane has experienced tremendous development since the concept of interfacial polymerisation (IP) was first introduced. One of its new application is on the separation of xylose from glucos e in biomass hydrolysate. In this present study, NF TFC membrane has been produced through interfacial poly merisation by manipulation the concentration of triethanolamine (TEOA) at 35 min reaction time with 0. 15 % w/v of trimesoyl chloride (TMC). The membrane was then characterised in term of their chemical and physical properties, and separation performance between xylose and glucose. The growth of thin layer f ilm depends on concentration of TEOA as the monomer and reaction time. As concentration of TEOA and re action time increased, the layer of the TFC becomes thicker thus decreases the permeability of the membrane. Contradicted to this study, the lowest and the highest permeability were recorded at 4 % w/v of TEOA and 8 % w/v of TEOA at reaction time of 35-min in TMC. The TFC membrane prepared with 4 % w/v TEOA has high in permeate flux, resultant in high xylose separation of 1.3. Low permeate flux but moderate xylose separation factor of 0.93 was obtained for the TFC membrane prepared with 8 % w/v TEOA.
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publisher AIDIC Servizi
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spelling ump-197992019-10-30T07:47:01Z http://umpir.ump.edu.my/id/eprint/19799/ Synthesis of Nanofiltration Membrane Developed from Triethanolamine (TEOA) and Trimesoyl Chloride (TMC) for Separation of Xylose from Glucose Nurul Fatihah, Mahamad Roli Wan Mohd Hafizuddin, Wan Yussof Syed Mohd Saufi, Tuan Chik Mazrul Nizam, Abu Seman Abdul W., Mohammad TP Chemical technology Synthesis of thin film composite (TFC) nanofilt ration (NF) membrane has experienced tremendous development since the concept of interfacial polymerisation (IP) was first introduced. One of its new application is on the separation of xylose from glucos e in biomass hydrolysate. In this present study, NF TFC membrane has been produced through interfacial poly merisation by manipulation the concentration of triethanolamine (TEOA) at 35 min reaction time with 0. 15 % w/v of trimesoyl chloride (TMC). The membrane was then characterised in term of their chemical and physical properties, and separation performance between xylose and glucose. The growth of thin layer f ilm depends on concentration of TEOA as the monomer and reaction time. As concentration of TEOA and re action time increased, the layer of the TFC becomes thicker thus decreases the permeability of the membrane. Contradicted to this study, the lowest and the highest permeability were recorded at 4 % w/v of TEOA and 8 % w/v of TEOA at reaction time of 35-min in TMC. The TFC membrane prepared with 4 % w/v TEOA has high in permeate flux, resultant in high xylose separation of 1.3. Low permeate flux but moderate xylose separation factor of 0.93 was obtained for the TFC membrane prepared with 8 % w/v TEOA. AIDIC Servizi 2017 Article PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/19799/1/fkksa-2017-fatiha-Synthesis%20of%20Nanofiltration%20Membrane%20Developed.pdf Nurul Fatihah, Mahamad Roli and Wan Mohd Hafizuddin, Wan Yussof and Syed Mohd Saufi, Tuan Chik and Mazrul Nizam, Abu Seman and Abdul W., Mohammad (2017) Synthesis of Nanofiltration Membrane Developed from Triethanolamine (TEOA) and Trimesoyl Chloride (TMC) for Separation of Xylose from Glucose. Chemical Engineering Transactions, 56. pp. 1507-1512. ISSN 2283-9216. (Published) http://www.aidic.it/cet/17/56/252.pdf DOI: 10.3303/CET1756252
spellingShingle TP Chemical technology
Nurul Fatihah, Mahamad Roli
Wan Mohd Hafizuddin, Wan Yussof
Syed Mohd Saufi, Tuan Chik
Mazrul Nizam, Abu Seman
Abdul W., Mohammad
Synthesis of Nanofiltration Membrane Developed from Triethanolamine (TEOA) and Trimesoyl Chloride (TMC) for Separation of Xylose from Glucose
title Synthesis of Nanofiltration Membrane Developed from Triethanolamine (TEOA) and Trimesoyl Chloride (TMC) for Separation of Xylose from Glucose
title_full Synthesis of Nanofiltration Membrane Developed from Triethanolamine (TEOA) and Trimesoyl Chloride (TMC) for Separation of Xylose from Glucose
title_fullStr Synthesis of Nanofiltration Membrane Developed from Triethanolamine (TEOA) and Trimesoyl Chloride (TMC) for Separation of Xylose from Glucose
title_full_unstemmed Synthesis of Nanofiltration Membrane Developed from Triethanolamine (TEOA) and Trimesoyl Chloride (TMC) for Separation of Xylose from Glucose
title_short Synthesis of Nanofiltration Membrane Developed from Triethanolamine (TEOA) and Trimesoyl Chloride (TMC) for Separation of Xylose from Glucose
title_sort synthesis of nanofiltration membrane developed from triethanolamine (teoa) and trimesoyl chloride (tmc) for separation of xylose from glucose
topic TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/19799/
http://umpir.ump.edu.my/id/eprint/19799/
http://umpir.ump.edu.my/id/eprint/19799/
http://umpir.ump.edu.my/id/eprint/19799/1/fkksa-2017-fatiha-Synthesis%20of%20Nanofiltration%20Membrane%20Developed.pdf