Morphology Evaluation of ZrO2 Dip Coating on Mild Steel and its Corrosion Performance in NaOH Solution
In this work, the morphology of ZrO2 thin film from dip coating process on mild steel has been investigated. Mild steel was dip-coated on solution made of zirconium butoxide as a precursor, ethanol as solvent, acetylacetone as chelating agent and water for hydrolysis. Number of dipping was adjusted...
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| Format: | Conference or Workshop Item |
| Language: | English |
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IOP Publishing
2017
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| Online Access: | http://umpir.ump.edu.my/id/eprint/19654/ http://umpir.ump.edu.my/id/eprint/19654/1/Morphology%20evaluation%20of%20ZrO2%20dip%20coating%20on%20mild%20steel%20and%20its%20corrosion%20performance%20in%20NaOH%20solution.pdf |
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| author | M. A., Anwar Kurniawan, Tedi Asmara, Y. P. W. S., Wan Harun Oumar, A. N. Nandyanto, A. B. D. |
| author_facet | M. A., Anwar Kurniawan, Tedi Asmara, Y. P. W. S., Wan Harun Oumar, A. N. Nandyanto, A. B. D. |
| author_sort | M. A., Anwar |
| building | UMP Institutional Repository |
| collection | Online Access |
| description | In this work, the morphology of ZrO2 thin film from dip coating process on mild steel has been investigated. Mild steel was dip-coated on solution made of zirconium butoxide as a precursor, ethanol as solvent, acetylacetone as chelating agent and water for hydrolysis. Number of dipping was adjusted at 3, 5 and 7 times. The dipped sample then annealed at 350°C for two hours by adjusting the heating rate at 1°C/min respectively. The optical microscope showed that micro-cracks were observed on the surface of the coating with its concentration reduced as dipping sequence increased. The XRD result showed that annealing process can produce polycrystalline tetragonal-ZrO2. Meanwhile, SEM image showed that the thicknesses of the ZrO2 coatings were in between 400-600 nm. The corrosion resistance of uncoated and coated substrates was studied by polarization test through potentio-dynamic polarization curve at 1mV/s immersed in with 3.5% NaCl. The coating efficiency was improved as the number of layer dip coated increased, which showed improvement in corrosion protection. |
| first_indexed | 2025-11-15T02:17:16Z |
| format | Conference or Workshop Item |
| id | ump-19654 |
| institution | Universiti Malaysia Pahang |
| institution_category | Local University |
| language | English |
| last_indexed | 2025-11-15T02:17:16Z |
| publishDate | 2017 |
| publisher | IOP Publishing |
| recordtype | eprints |
| repository_type | Digital Repository |
| spelling | ump-196542018-04-11T03:00:53Z http://umpir.ump.edu.my/id/eprint/19654/ Morphology Evaluation of ZrO2 Dip Coating on Mild Steel and its Corrosion Performance in NaOH Solution M. A., Anwar Kurniawan, Tedi Asmara, Y. P. W. S., Wan Harun Oumar, A. N. Nandyanto, A. B. D. Q Science (General) TJ Mechanical engineering and machinery In this work, the morphology of ZrO2 thin film from dip coating process on mild steel has been investigated. Mild steel was dip-coated on solution made of zirconium butoxide as a precursor, ethanol as solvent, acetylacetone as chelating agent and water for hydrolysis. Number of dipping was adjusted at 3, 5 and 7 times. The dipped sample then annealed at 350°C for two hours by adjusting the heating rate at 1°C/min respectively. The optical microscope showed that micro-cracks were observed on the surface of the coating with its concentration reduced as dipping sequence increased. The XRD result showed that annealing process can produce polycrystalline tetragonal-ZrO2. Meanwhile, SEM image showed that the thicknesses of the ZrO2 coatings were in between 400-600 nm. The corrosion resistance of uncoated and coated substrates was studied by polarization test through potentio-dynamic polarization curve at 1mV/s immersed in with 3.5% NaCl. The coating efficiency was improved as the number of layer dip coated increased, which showed improvement in corrosion protection. IOP Publishing 2017 Conference or Workshop Item PeerReviewed application/pdf en cc_by http://umpir.ump.edu.my/id/eprint/19654/1/Morphology%20evaluation%20of%20ZrO2%20dip%20coating%20on%20mild%20steel%20and%20its%20corrosion%20performance%20in%20NaOH%20solution.pdf M. A., Anwar and Kurniawan, Tedi and Asmara, Y. P. and W. S., Wan Harun and Oumar, A. N. and Nandyanto, A. B. D. (2017) Morphology Evaluation of ZrO2 Dip Coating on Mild Steel and its Corrosion Performance in NaOH Solution. In: IOP Conference Series: Materials Science and Engineering, 4th International Conference on Mechanical Engineering Research (ICMER2017) , 1-2 August 2017 , Kuantan, Pahang, Malaysia. pp. 1-6., 257 (012087). ISSN 1757-899X (Published) https://doi.org/10.1088/1757-899X/257/1/012087 |
| spellingShingle | Q Science (General) TJ Mechanical engineering and machinery M. A., Anwar Kurniawan, Tedi Asmara, Y. P. W. S., Wan Harun Oumar, A. N. Nandyanto, A. B. D. Morphology Evaluation of ZrO2 Dip Coating on Mild Steel and its Corrosion Performance in NaOH Solution |
| title | Morphology Evaluation of ZrO2 Dip Coating on Mild Steel and its Corrosion Performance in NaOH Solution |
| title_full | Morphology Evaluation of ZrO2 Dip Coating on Mild Steel and its Corrosion Performance in NaOH Solution |
| title_fullStr | Morphology Evaluation of ZrO2 Dip Coating on Mild Steel and its Corrosion Performance in NaOH Solution |
| title_full_unstemmed | Morphology Evaluation of ZrO2 Dip Coating on Mild Steel and its Corrosion Performance in NaOH Solution |
| title_short | Morphology Evaluation of ZrO2 Dip Coating on Mild Steel and its Corrosion Performance in NaOH Solution |
| title_sort | morphology evaluation of zro2 dip coating on mild steel and its corrosion performance in naoh solution |
| topic | Q Science (General) TJ Mechanical engineering and machinery |
| url | http://umpir.ump.edu.my/id/eprint/19654/ http://umpir.ump.edu.my/id/eprint/19654/ http://umpir.ump.edu.my/id/eprint/19654/1/Morphology%20evaluation%20of%20ZrO2%20dip%20coating%20on%20mild%20steel%20and%20its%20corrosion%20performance%20in%20NaOH%20solution.pdf |