Essential Oil from Cinnamomum Cassia Bark Through Hydrodistillation and Advanced Microwave Assisted Hydrodistillation

The increasing demand for essential oil necessitates the use of advanced techniques for its extraction. In this study, volatile oils were extracted from Cinnamomum cassia bark through microwave assisted hydrodistillation (MAHD) and conventional hydrodistillation (HD) methods. Effects of pre-treatmen...

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Main Authors: Nitthiyah, Jeyaratnam, Nour, A. H., K., Ramesh, Azhari, H. Nour, A. R., Yuvaraj, Akindoyo, John Olabode
Format: Article
Language:English
Published: Elsevier Ltd 2016
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/14116/
http://umpir.ump.edu.my/id/eprint/14116/1/Essential%20Oil%20from%20Cinnamomum%20Cassia%20Bark%20Through%20Hydrodistillation%20and%20Advanced%20Microwave%20Assisted%20Hydrodistillation.pdf
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author Nitthiyah, Jeyaratnam
Nour, A. H.
K., Ramesh
Azhari, H. Nour
A. R., Yuvaraj
Akindoyo, John Olabode
author_facet Nitthiyah, Jeyaratnam
Nour, A. H.
K., Ramesh
Azhari, H. Nour
A. R., Yuvaraj
Akindoyo, John Olabode
author_sort Nitthiyah, Jeyaratnam
building UMP Institutional Repository
collection Online Access
description The increasing demand for essential oil necessitates the use of advanced techniques for its extraction. In this study, volatile oils were extracted from Cinnamomum cassia bark through microwave assisted hydrodistillation (MAHD) and conventional hydrodistillation (HD) methods. Effects of pre-treatment and morphological changes to cinnamon bark powder before and after extraction were observed through Scanning Electron Microscopy (SEM). After extraction, Fourier Transform Infrared Spectroscopy (FTIR) analysis revealed close similarities in compounds of the oil extracted through HD and MAHD. Gas Chromatography–Mass Spectrometry (GC–MS) revealed that MAHD produced 9% higher oxygenated compounds than HD. Furthermore, MAHD was found to be more energy saving and environmental friendly, reducing the overall carbon dioxide emission from HD by 59%. In addition, cytotoxicity studies revealed that essential oil obtained through MAHD showed lower lethal concentration 50 (LC50) value of 51.2 mg/L compared with HD (68.9 mg/L). Therefore, MAHD technique is very suitable for obtaining volatile oils from C. cassia bark and the oil obtained can offer great pharmaceutical benefits.
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publishDate 2016
publisher Elsevier Ltd
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spelling ump-141162019-09-10T03:00:18Z http://umpir.ump.edu.my/id/eprint/14116/ Essential Oil from Cinnamomum Cassia Bark Through Hydrodistillation and Advanced Microwave Assisted Hydrodistillation Nitthiyah, Jeyaratnam Nour, A. H. K., Ramesh Azhari, H. Nour A. R., Yuvaraj Akindoyo, John Olabode Q Science (General) TP Chemical technology The increasing demand for essential oil necessitates the use of advanced techniques for its extraction. In this study, volatile oils were extracted from Cinnamomum cassia bark through microwave assisted hydrodistillation (MAHD) and conventional hydrodistillation (HD) methods. Effects of pre-treatment and morphological changes to cinnamon bark powder before and after extraction were observed through Scanning Electron Microscopy (SEM). After extraction, Fourier Transform Infrared Spectroscopy (FTIR) analysis revealed close similarities in compounds of the oil extracted through HD and MAHD. Gas Chromatography–Mass Spectrometry (GC–MS) revealed that MAHD produced 9% higher oxygenated compounds than HD. Furthermore, MAHD was found to be more energy saving and environmental friendly, reducing the overall carbon dioxide emission from HD by 59%. In addition, cytotoxicity studies revealed that essential oil obtained through MAHD showed lower lethal concentration 50 (LC50) value of 51.2 mg/L compared with HD (68.9 mg/L). Therefore, MAHD technique is very suitable for obtaining volatile oils from C. cassia bark and the oil obtained can offer great pharmaceutical benefits. Elsevier Ltd 2016 Article PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/14116/1/Essential%20Oil%20from%20Cinnamomum%20Cassia%20Bark%20Through%20Hydrodistillation%20and%20Advanced%20Microwave%20Assisted%20Hydrodistillation.pdf Nitthiyah, Jeyaratnam and Nour, A. H. and K., Ramesh and Azhari, H. Nour and A. R., Yuvaraj and Akindoyo, John Olabode (2016) Essential Oil from Cinnamomum Cassia Bark Through Hydrodistillation and Advanced Microwave Assisted Hydrodistillation. Industrial Crops and Products, 92. pp. 57-66. ISSN 0926-6690. (Published) http://dx.doi.org/10.1016/j.indcrop.2016.07.049 DOI: 10.1016/j.indcrop.2016.07.049
spellingShingle Q Science (General)
TP Chemical technology
Nitthiyah, Jeyaratnam
Nour, A. H.
K., Ramesh
Azhari, H. Nour
A. R., Yuvaraj
Akindoyo, John Olabode
Essential Oil from Cinnamomum Cassia Bark Through Hydrodistillation and Advanced Microwave Assisted Hydrodistillation
title Essential Oil from Cinnamomum Cassia Bark Through Hydrodistillation and Advanced Microwave Assisted Hydrodistillation
title_full Essential Oil from Cinnamomum Cassia Bark Through Hydrodistillation and Advanced Microwave Assisted Hydrodistillation
title_fullStr Essential Oil from Cinnamomum Cassia Bark Through Hydrodistillation and Advanced Microwave Assisted Hydrodistillation
title_full_unstemmed Essential Oil from Cinnamomum Cassia Bark Through Hydrodistillation and Advanced Microwave Assisted Hydrodistillation
title_short Essential Oil from Cinnamomum Cassia Bark Through Hydrodistillation and Advanced Microwave Assisted Hydrodistillation
title_sort essential oil from cinnamomum cassia bark through hydrodistillation and advanced microwave assisted hydrodistillation
topic Q Science (General)
TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/14116/
http://umpir.ump.edu.my/id/eprint/14116/
http://umpir.ump.edu.my/id/eprint/14116/
http://umpir.ump.edu.my/id/eprint/14116/1/Essential%20Oil%20from%20Cinnamomum%20Cassia%20Bark%20Through%20Hydrodistillation%20and%20Advanced%20Microwave%20Assisted%20Hydrodistillation.pdf