Formation of high aspect ratio TiO2 nanotube arrays by anodization of Ti foil in organic solution

Titanium oxide (TiO2) nanotubes were successfully formed by anodization of pure titanium foil in a standard two-electrode bath consisting of ethylene glycol solution containing 5 wt% NH4F. The pH of the solution was ∼ 7 and the anodization voltage was 60 V. It was observed that such anodization cond...

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Main Authors: Srimala Sreekantan, Roshasnorlyza Hazan, Khairul Arifah Saharudin, Lai, Chin Wei, Ishak Mat
Format: Article
Language:English
Published: Universiti Kebangsaan Malaysia 2011
Online Access:http://journalarticle.ukm.my/702/
http://journalarticle.ukm.my/702/1/06_Srimala.pdf
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author Srimala Sreekantan,
Roshasnorlyza Hazan,
Khairul Arifah Saharudin,
Lai, Chin Wei
Ishak Mat,
author_facet Srimala Sreekantan,
Roshasnorlyza Hazan,
Khairul Arifah Saharudin,
Lai, Chin Wei
Ishak Mat,
author_sort Srimala Sreekantan,
building UKM Institutional Repository
collection Online Access
description Titanium oxide (TiO2) nanotubes were successfully formed by anodization of pure titanium foil in a standard two-electrode bath consisting of ethylene glycol solution containing 5 wt% NH4F. The pH of the solution was ∼ 7 and the anodization voltage was 60 V. It was observed that such anodization condition results in ordered arrays of TiO2 nanotubes with smooth surface and a very high aspect ratio. It was observed that a minimum of 1 wt % water addition was required to form well ordered TiO2 nanotubes with length of approximately 18.5 μm. As-anodized sample, the self-organized TiO2 nanotubes have amorphous structure and annealing at 500oC of the nanotubes promote formation of anatase and rutile phase. Photocatalytic activity of well ordered TiO2 nanotubes with two different lengths was evaluated by measuring the degradation of methyl orange (MO). The elaboration of this observation is described in detail in this paper.
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spelling ukm-7022016-12-14T06:27:56Z http://journalarticle.ukm.my/702/ Formation of high aspect ratio TiO2 nanotube arrays by anodization of Ti foil in organic solution Srimala Sreekantan, Roshasnorlyza Hazan, Khairul Arifah Saharudin, Lai, Chin Wei Ishak Mat, Titanium oxide (TiO2) nanotubes were successfully formed by anodization of pure titanium foil in a standard two-electrode bath consisting of ethylene glycol solution containing 5 wt% NH4F. The pH of the solution was ∼ 7 and the anodization voltage was 60 V. It was observed that such anodization condition results in ordered arrays of TiO2 nanotubes with smooth surface and a very high aspect ratio. It was observed that a minimum of 1 wt % water addition was required to form well ordered TiO2 nanotubes with length of approximately 18.5 μm. As-anodized sample, the self-organized TiO2 nanotubes have amorphous structure and annealing at 500oC of the nanotubes promote formation of anatase and rutile phase. Photocatalytic activity of well ordered TiO2 nanotubes with two different lengths was evaluated by measuring the degradation of methyl orange (MO). The elaboration of this observation is described in detail in this paper. Universiti Kebangsaan Malaysia 2011-03 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/702/1/06_Srimala.pdf Srimala Sreekantan, and Roshasnorlyza Hazan, and Khairul Arifah Saharudin, and Lai, Chin Wei and Ishak Mat, (2011) Formation of high aspect ratio TiO2 nanotube arrays by anodization of Ti foil in organic solution. Sains Malaysiana, 40 (3). pp. 227-230. ISSN 0126-6039
spellingShingle Srimala Sreekantan,
Roshasnorlyza Hazan,
Khairul Arifah Saharudin,
Lai, Chin Wei
Ishak Mat,
Formation of high aspect ratio TiO2 nanotube arrays by anodization of Ti foil in organic solution
title Formation of high aspect ratio TiO2 nanotube arrays by anodization of Ti foil in organic solution
title_full Formation of high aspect ratio TiO2 nanotube arrays by anodization of Ti foil in organic solution
title_fullStr Formation of high aspect ratio TiO2 nanotube arrays by anodization of Ti foil in organic solution
title_full_unstemmed Formation of high aspect ratio TiO2 nanotube arrays by anodization of Ti foil in organic solution
title_short Formation of high aspect ratio TiO2 nanotube arrays by anodization of Ti foil in organic solution
title_sort formation of high aspect ratio tio2 nanotube arrays by anodization of ti foil in organic solution
url http://journalarticle.ukm.my/702/
http://journalarticle.ukm.my/702/1/06_Srimala.pdf