Synthesis and characterization zinc oxide doped graphene nanohybrid by sol-gel method / Khairul Anwar Razak

A series of pure ZnO and graphene doped ZnO nanohybrid samples were synthesized via ultrasonic assisted sol-gel method using reducing agent Hexamethylenetetramine (HMTA) at different weight percentage. The prepared sample were characterized by XRD, FTIR and UV-Visible to study the structural, fun...

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Main Author: Razak, Khairul Anwar
Format: Student Project
Language:English
Published: Faculty of Applied Sciences 2018
Subjects:
Online Access:https://ir.uitm.edu.my/id/eprint/24849/
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author Razak, Khairul Anwar
author_facet Razak, Khairul Anwar
author_sort Razak, Khairul Anwar
building UiTM Institutional Repository
collection Online Access
description A series of pure ZnO and graphene doped ZnO nanohybrid samples were synthesized via ultrasonic assisted sol-gel method using reducing agent Hexamethylenetetramine (HMTA) at different weight percentage. The prepared sample were characterized by XRD, FTIR and UV-Visible to study the structural, functional and optical properties. XRD analysis reveals that as pure ZnO, all the diffractive peaks can be indexed as the hexagonal ZnO while for ZnO/Graphene nanohybrids shows a diffraction peaks at 28 (002) = 26.42 indicating the graphene has been successfully doped. The estimated crystallite size was decreased as increased the Graphene weight % in the range of 32.94 - 40.32 nm. In UV-Vis spectra, two absorption band were observe that can be assigned to absorption of ZnO crystal with correspond absorption edge at 375 nm and the peak at about 302 nm is describe to graphene absorption. The FTIR analysis demonstrate that the functional group present in the obtained product. The ZnO/Graphene nanohybrid may be ideal candidates for photocatalyst application
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spelling uitm-248492019-07-19T01:34:45Z https://ir.uitm.edu.my/id/eprint/24849/ Synthesis and characterization zinc oxide doped graphene nanohybrid by sol-gel method / Khairul Anwar Razak Razak, Khairul Anwar Nanostructures Carbon disulfide. Graphene. Carbon A series of pure ZnO and graphene doped ZnO nanohybrid samples were synthesized via ultrasonic assisted sol-gel method using reducing agent Hexamethylenetetramine (HMTA) at different weight percentage. The prepared sample were characterized by XRD, FTIR and UV-Visible to study the structural, functional and optical properties. XRD analysis reveals that as pure ZnO, all the diffractive peaks can be indexed as the hexagonal ZnO while for ZnO/Graphene nanohybrids shows a diffraction peaks at 28 (002) = 26.42 indicating the graphene has been successfully doped. The estimated crystallite size was decreased as increased the Graphene weight % in the range of 32.94 - 40.32 nm. In UV-Vis spectra, two absorption band were observe that can be assigned to absorption of ZnO crystal with correspond absorption edge at 375 nm and the peak at about 302 nm is describe to graphene absorption. The FTIR analysis demonstrate that the functional group present in the obtained product. The ZnO/Graphene nanohybrid may be ideal candidates for photocatalyst application Faculty of Applied Sciences 2018 Student Project NonPeerReviewed text en https://ir.uitm.edu.my/id/eprint/24849/1/PPb_KHAIRUL%20ANWAR%20RAZAK%20AS%20C%2018_5.PDF Razak, Khairul Anwar (2018) Synthesis and characterization zinc oxide doped graphene nanohybrid by sol-gel method / Khairul Anwar Razak. (2018) [Student Project] <http://terminalib.uitm.edu.my/24849.pdf> (Unpublished)
spellingShingle Nanostructures
Carbon disulfide. Graphene. Carbon
Razak, Khairul Anwar
Synthesis and characterization zinc oxide doped graphene nanohybrid by sol-gel method / Khairul Anwar Razak
title Synthesis and characterization zinc oxide doped graphene nanohybrid by sol-gel method / Khairul Anwar Razak
title_full Synthesis and characterization zinc oxide doped graphene nanohybrid by sol-gel method / Khairul Anwar Razak
title_fullStr Synthesis and characterization zinc oxide doped graphene nanohybrid by sol-gel method / Khairul Anwar Razak
title_full_unstemmed Synthesis and characterization zinc oxide doped graphene nanohybrid by sol-gel method / Khairul Anwar Razak
title_short Synthesis and characterization zinc oxide doped graphene nanohybrid by sol-gel method / Khairul Anwar Razak
title_sort synthesis and characterization zinc oxide doped graphene nanohybrid by sol-gel method / khairul anwar razak
topic Nanostructures
Carbon disulfide. Graphene. Carbon
url https://ir.uitm.edu.my/id/eprint/24849/