Synthesis and characterization of zinc-layered 2, 4, 5 trichlorophenoxybutyric acid under aqueous condition / Nur Hani Ab Rahman

The synthesis of zinc-layered 2, 4, 5-triclorophenoxybutyric acid (ZTBA) and the characterization of the nanohybrid compound by using powder x-ray diffraction (PXRD), Fourier Transform Infrared (FTIR), Thermogravimetric and Derivative Thermogravimetric Analysis (TGA/DTG) and Elemental Analysis (CHNS...

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Main Author: Ab Rahman, Nur Hani
Format: Student Project
Language:English
Published: Faculty of Applied Sciences 2016
Subjects:
Online Access:https://ir.uitm.edu.my/id/eprint/24267/
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author Ab Rahman, Nur Hani
author_facet Ab Rahman, Nur Hani
author_sort Ab Rahman, Nur Hani
building UiTM Institutional Repository
collection Online Access
description The synthesis of zinc-layered 2, 4, 5-triclorophenoxybutyric acid (ZTBA) and the characterization of the nanohybrid compound by using powder x-ray diffraction (PXRD), Fourier Transform Infrared (FTIR), Thermogravimetric and Derivative Thermogravimetric Analysis (TGA/DTG) and Elemental Analysis (CHNS) has been developed. The synthesis of the ZTBA nanohybrid compound was successfully prepared by using anion-exchange method. The pure phase and well-ordered zinc-layered 2, 4, 5-trichlorophenoxybutyric acid was synthesized at 0.1 M 2, 4, 5-trichlorophenoxybutyric acid (TBA) and with a basal spacing of 13.0 Å. The FTIR spectra show resemblance of TBA with ZnO absorption characteristics. The percentage loading of guest anions, TBA in the zinc layered hydroxide was calculated to be about 51.92 % .The total weight loss by using TGA / DTG is calculated to be at about 63.5 % in the range of 90 - 1000⁰C.
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spelling uitm-242672019-05-17T07:39:24Z https://ir.uitm.edu.my/id/eprint/24267/ Synthesis and characterization of zinc-layered 2, 4, 5 trichlorophenoxybutyric acid under aqueous condition / Nur Hani Ab Rahman Ab Rahman, Nur Hani QD Chemistry Metal complexes. Layered double hydroxides The synthesis of zinc-layered 2, 4, 5-triclorophenoxybutyric acid (ZTBA) and the characterization of the nanohybrid compound by using powder x-ray diffraction (PXRD), Fourier Transform Infrared (FTIR), Thermogravimetric and Derivative Thermogravimetric Analysis (TGA/DTG) and Elemental Analysis (CHNS) has been developed. The synthesis of the ZTBA nanohybrid compound was successfully prepared by using anion-exchange method. The pure phase and well-ordered zinc-layered 2, 4, 5-trichlorophenoxybutyric acid was synthesized at 0.1 M 2, 4, 5-trichlorophenoxybutyric acid (TBA) and with a basal spacing of 13.0 Å. The FTIR spectra show resemblance of TBA with ZnO absorption characteristics. The percentage loading of guest anions, TBA in the zinc layered hydroxide was calculated to be about 51.92 % .The total weight loss by using TGA / DTG is calculated to be at about 63.5 % in the range of 90 - 1000⁰C. Faculty of Applied Sciences 2016 Student Project NonPeerReviewed text en https://ir.uitm.edu.my/id/eprint/24267/1/PPb_NUR%20HANI%20AB%20RAHMAN%20AS%20N%2016_5.pdf Ab Rahman, Nur Hani (2016) Synthesis and characterization of zinc-layered 2, 4, 5 trichlorophenoxybutyric acid under aqueous condition / Nur Hani Ab Rahman. (2016) [Student Project] <http://terminalib.uitm.edu.my/24267.pdf> (Unpublished)
spellingShingle QD Chemistry
Metal complexes. Layered double hydroxides
Ab Rahman, Nur Hani
Synthesis and characterization of zinc-layered 2, 4, 5 trichlorophenoxybutyric acid under aqueous condition / Nur Hani Ab Rahman
title Synthesis and characterization of zinc-layered 2, 4, 5 trichlorophenoxybutyric acid under aqueous condition / Nur Hani Ab Rahman
title_full Synthesis and characterization of zinc-layered 2, 4, 5 trichlorophenoxybutyric acid under aqueous condition / Nur Hani Ab Rahman
title_fullStr Synthesis and characterization of zinc-layered 2, 4, 5 trichlorophenoxybutyric acid under aqueous condition / Nur Hani Ab Rahman
title_full_unstemmed Synthesis and characterization of zinc-layered 2, 4, 5 trichlorophenoxybutyric acid under aqueous condition / Nur Hani Ab Rahman
title_short Synthesis and characterization of zinc-layered 2, 4, 5 trichlorophenoxybutyric acid under aqueous condition / Nur Hani Ab Rahman
title_sort synthesis and characterization of zinc-layered 2, 4, 5 trichlorophenoxybutyric acid under aqueous condition / nur hani ab rahman
topic QD Chemistry
Metal complexes. Layered double hydroxides
url https://ir.uitm.edu.my/id/eprint/24267/