Extraction and elucidation of chemical constituents from the roots of Derris Elliptic A / Tengku Muzzabfarrullah Tengku Sham

The chemical compounds form the roots of Derris elliptica were extracted and isolated by various chromatography methods. The isolated compounds were elucidated by the spectroscopic methods. Extractions of the roots of Derris elliptica (300g) were done by macerated in the chloroform. The extraction y...

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Main Author: Tengku Sham, Tengku Muzzabfarrullah
Format: Student Project
Language:English
Published: Faculty of Applied Sciences 2008
Subjects:
Online Access:https://ir.uitm.edu.my/id/eprint/23184/
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author Tengku Sham, Tengku Muzzabfarrullah
author_facet Tengku Sham, Tengku Muzzabfarrullah
author_sort Tengku Sham, Tengku Muzzabfarrullah
building UiTM Institutional Repository
collection Online Access
description The chemical compounds form the roots of Derris elliptica were extracted and isolated by various chromatography methods. The isolated compounds were elucidated by the spectroscopic methods. Extractions of the roots of Derris elliptica (300g) were done by macerated in the chloroform. The extraction yield crude extract 8.74g (0.03 % w/w) were isolated using the chromatography methods. Vacuum liquid chromatography (VLC) and Radial chromatography (RC) were used to isolate the crude extract. Thin layer chromatography (TLC) was used to identify the pure compounds. The isolated crude produce two compound were produce labeled DEI (16.7mg) and DE2 (14.1mg). The pure compound were elucidated by the spectroscopic method; Nuclear Magnetic Resonance (NMR), Gas Chromatography - Mass Spectrometry (GC-MS), UV spectroscopy and Fourier Transform Infrared (FTIR). From the comparison of the spectrums with the literature reviews, the compounds were identified. Compound DEI known as rotenone and compound DE2 known as 2\-hydroxy-r,2'-dihydrorotenone.
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spelling uitm-231842019-02-14T09:20:59Z https://ir.uitm.edu.my/id/eprint/23184/ Extraction and elucidation of chemical constituents from the roots of Derris Elliptic A / Tengku Muzzabfarrullah Tengku Sham Tengku Sham, Tengku Muzzabfarrullah Extraction (Chemistry) The chemical compounds form the roots of Derris elliptica were extracted and isolated by various chromatography methods. The isolated compounds were elucidated by the spectroscopic methods. Extractions of the roots of Derris elliptica (300g) were done by macerated in the chloroform. The extraction yield crude extract 8.74g (0.03 % w/w) were isolated using the chromatography methods. Vacuum liquid chromatography (VLC) and Radial chromatography (RC) were used to isolate the crude extract. Thin layer chromatography (TLC) was used to identify the pure compounds. The isolated crude produce two compound were produce labeled DEI (16.7mg) and DE2 (14.1mg). The pure compound were elucidated by the spectroscopic method; Nuclear Magnetic Resonance (NMR), Gas Chromatography - Mass Spectrometry (GC-MS), UV spectroscopy and Fourier Transform Infrared (FTIR). From the comparison of the spectrums with the literature reviews, the compounds were identified. Compound DEI known as rotenone and compound DE2 known as 2\-hydroxy-r,2'-dihydrorotenone. Faculty of Applied Sciences 2008 Student Project NonPeerReviewed text en https://ir.uitm.edu.my/id/eprint/23184/1/PPb_TENGKU%20MUZZABFARULLAH%20TENGKU%20SHAM%20AS%2008_5.pdf Tengku Sham, Tengku Muzzabfarrullah (2008) Extraction and elucidation of chemical constituents from the roots of Derris Elliptic A / Tengku Muzzabfarrullah Tengku Sham. (2008) [Student Project] <http://terminalib.uitm.edu.my/23184.pdf> (Unpublished)
spellingShingle Extraction (Chemistry)
Tengku Sham, Tengku Muzzabfarrullah
Extraction and elucidation of chemical constituents from the roots of Derris Elliptic A / Tengku Muzzabfarrullah Tengku Sham
title Extraction and elucidation of chemical constituents from the roots of Derris Elliptic A / Tengku Muzzabfarrullah Tengku Sham
title_full Extraction and elucidation of chemical constituents from the roots of Derris Elliptic A / Tengku Muzzabfarrullah Tengku Sham
title_fullStr Extraction and elucidation of chemical constituents from the roots of Derris Elliptic A / Tengku Muzzabfarrullah Tengku Sham
title_full_unstemmed Extraction and elucidation of chemical constituents from the roots of Derris Elliptic A / Tengku Muzzabfarrullah Tengku Sham
title_short Extraction and elucidation of chemical constituents from the roots of Derris Elliptic A / Tengku Muzzabfarrullah Tengku Sham
title_sort extraction and elucidation of chemical constituents from the roots of derris elliptic a / tengku muzzabfarrullah tengku sham
topic Extraction (Chemistry)
url https://ir.uitm.edu.my/id/eprint/23184/