Structural and photoluminescence properties of nanostructured zinc oxide synthesized by immersion method / Azlinda Ab. Aziz

In this present work, Zinc oxide (ZnO) nanostructures on gold-coated silicon (Si) substrate were prepared from zinc nitrate hexahydrate (Zn(N03)2.6HO) and urea (CH4N2O) using a low-temperature solution-immersion method. High hierarchical structure of ZnO with high surface area were successfully synt...

Full description

Bibliographic Details
Main Author: Ab. Aziz, Azlinda
Format: Thesis
Language:English
Published: 2016
Online Access:https://ir.uitm.edu.my/id/eprint/18184/
_version_ 1848804463354052608
author Ab. Aziz, Azlinda
author_facet Ab. Aziz, Azlinda
author_sort Ab. Aziz, Azlinda
building UiTM Institutional Repository
collection Online Access
description In this present work, Zinc oxide (ZnO) nanostructures on gold-coated silicon (Si) substrate were prepared from zinc nitrate hexahydrate (Zn(N03)2.6HO) and urea (CH4N2O) using a low-temperature solution-immersion method. High hierarchical structure of ZnO with high surface area were successfully synthesised by the immersion method through optimization of the reaction parameters, such as different substrate surface, alignment of substrate, concentration of precursor, ratio of stabiliser in solution, and different heat temperature. FESEM, EDX, XRD, AFM and PL were the selected characterization tools to analyse the morphological, structural, surface analysis and optical properties of ZnO nanostructures. FESEM images revealed that ZnO flowerlike microspheres consist of nanosheets was the dominant structure growth along synthesis parameter. The results give evidence that the smallest diameter -11-13 |um of ZnO micro-flowers was successfully formed on gold-coated Si substrate, and gold served as a nucleation sites for the growth of ZnO micro-flowers. Low average surface roughness of ZnO nanostructures had shown the uniformity of particles size on gold-coated Si surface.
first_indexed 2025-11-14T21:55:32Z
format Thesis
id uitm-18184
institution Universiti Teknologi MARA
institution_category Local University
language English
last_indexed 2025-11-14T21:55:32Z
publishDate 2016
recordtype eprints
repository_type Digital Repository
spelling uitm-181842025-04-30T07:23:31Z https://ir.uitm.edu.my/id/eprint/18184/ Structural and photoluminescence properties of nanostructured zinc oxide synthesized by immersion method / Azlinda Ab. Aziz Ab. Aziz, Azlinda In this present work, Zinc oxide (ZnO) nanostructures on gold-coated silicon (Si) substrate were prepared from zinc nitrate hexahydrate (Zn(N03)2.6HO) and urea (CH4N2O) using a low-temperature solution-immersion method. High hierarchical structure of ZnO with high surface area were successfully synthesised by the immersion method through optimization of the reaction parameters, such as different substrate surface, alignment of substrate, concentration of precursor, ratio of stabiliser in solution, and different heat temperature. FESEM, EDX, XRD, AFM and PL were the selected characterization tools to analyse the morphological, structural, surface analysis and optical properties of ZnO nanostructures. FESEM images revealed that ZnO flowerlike microspheres consist of nanosheets was the dominant structure growth along synthesis parameter. The results give evidence that the smallest diameter -11-13 |um of ZnO micro-flowers was successfully formed on gold-coated Si substrate, and gold served as a nucleation sites for the growth of ZnO micro-flowers. Low average surface roughness of ZnO nanostructures had shown the uniformity of particles size on gold-coated Si surface. 2016 Thesis NonPeerReviewed text en https://ir.uitm.edu.my/id/eprint/18184/2/TM_AZLINDA%20AB.%20AZIZ%20AS%2016_5.pdf Ab. Aziz, Azlinda (2016) Structural and photoluminescence properties of nanostructured zinc oxide synthesized by immersion method / Azlinda Ab. Aziz. (2016) Masters thesis, thesis, Universiti Teknologi MARA. <http://terminalib.uitm.edu.my/18184.pdf>
spellingShingle Ab. Aziz, Azlinda
Structural and photoluminescence properties of nanostructured zinc oxide synthesized by immersion method / Azlinda Ab. Aziz
title Structural and photoluminescence properties of nanostructured zinc oxide synthesized by immersion method / Azlinda Ab. Aziz
title_full Structural and photoluminescence properties of nanostructured zinc oxide synthesized by immersion method / Azlinda Ab. Aziz
title_fullStr Structural and photoluminescence properties of nanostructured zinc oxide synthesized by immersion method / Azlinda Ab. Aziz
title_full_unstemmed Structural and photoluminescence properties of nanostructured zinc oxide synthesized by immersion method / Azlinda Ab. Aziz
title_short Structural and photoluminescence properties of nanostructured zinc oxide synthesized by immersion method / Azlinda Ab. Aziz
title_sort structural and photoluminescence properties of nanostructured zinc oxide synthesized by immersion method / azlinda ab. aziz
url https://ir.uitm.edu.my/id/eprint/18184/