Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin
A polystyrene (PS)-anchored Pd(II) metal complex was synthesized on cross-linked polymer by heating a mixture of chlorometylated polystyrene with phenyldithiocarbazate and carbon disulfide in the presence of potassium hydroxide (KOH) in dimethylformamide (DMF). The reaction mixture was heated at 80...
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| Format: | Article |
| Language: | English |
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Research Management Institute (RMI)
2014
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| Online Access: | https://ir.uitm.edu.my/id/eprint/12430/ |
| _version_ | 1848803154543509504 |
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| author | Che Soh, Siti Kamilah Jusoh, Siti Aminah Shamsuddin, Mustaffa |
| author_facet | Che Soh, Siti Kamilah Jusoh, Siti Aminah Shamsuddin, Mustaffa |
| author_sort | Che Soh, Siti Kamilah |
| building | UiTM Institutional Repository |
| collection | Online Access |
| description | A polystyrene (PS)-anchored Pd(II) metal complex was synthesized on cross-linked polymer by heating a mixture of chlorometylated polystyrene with phenyldithiocarbazate and carbon disulfide in the presence of potassium hydroxide (KOH) in dimethylformamide (DMF). The reaction mixture was heated at 80 °C to form the corresponding phenyldithiocarbazate-functionalized polymer. Then, it was treated with bis(benzonitrile)palladium(II) chloride. The
properties of dark colored polymer, impregnated with the metal complex was then characterized by various spectroscopic technique such as Fourier Transform Infrared (FTIR), Scanning Electron Microscopy/Energy Dispersive X-ray (SEM/EDX), CHNS elemental analysis, BET surface area, X-ray Diffraction (XRD), Thermogravimetric (TGA) and Inductively Coupled Plasma-Optical Emission (ICP-OES) spectroscopy. |
| first_indexed | 2025-11-14T21:34:44Z |
| format | Article |
| id | uitm-12430 |
| institution | Universiti Teknologi MARA |
| institution_category | Local University |
| language | English |
| last_indexed | 2025-11-14T21:34:44Z |
| publishDate | 2014 |
| publisher | Research Management Institute (RMI) |
| recordtype | eprints |
| repository_type | Digital Repository |
| spelling | uitm-124302016-05-26T02:46:51Z https://ir.uitm.edu.my/id/eprint/12430/ Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin srj Che Soh, Siti Kamilah Jusoh, Siti Aminah Shamsuddin, Mustaffa Palladium Polystyrene A polystyrene (PS)-anchored Pd(II) metal complex was synthesized on cross-linked polymer by heating a mixture of chlorometylated polystyrene with phenyldithiocarbazate and carbon disulfide in the presence of potassium hydroxide (KOH) in dimethylformamide (DMF). The reaction mixture was heated at 80 °C to form the corresponding phenyldithiocarbazate-functionalized polymer. Then, it was treated with bis(benzonitrile)palladium(II) chloride. The properties of dark colored polymer, impregnated with the metal complex was then characterized by various spectroscopic technique such as Fourier Transform Infrared (FTIR), Scanning Electron Microscopy/Energy Dispersive X-ray (SEM/EDX), CHNS elemental analysis, BET surface area, X-ray Diffraction (XRD), Thermogravimetric (TGA) and Inductively Coupled Plasma-Optical Emission (ICP-OES) spectroscopy. Research Management Institute (RMI) 2014 Article PeerReviewed text en https://ir.uitm.edu.my/id/eprint/12430/1/AJ_SITI%20KAMILAH%20CHE%20SOH%20SRJ%2014%201.pdf Che Soh, Siti Kamilah and Jusoh, Siti Aminah and Shamsuddin, Mustaffa (2014) Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin. (2014) Scientific Research Journal <https://ir.uitm.edu.my/view/publication/Scientific_Research_Journal.html>, 11 (2). pp. 1-10. ISSN 1675-7009 https://srj.uitm.edu.my/ |
| spellingShingle | Palladium Polystyrene Che Soh, Siti Kamilah Jusoh, Siti Aminah Shamsuddin, Mustaffa Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin |
| title | Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin |
| title_full | Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin |
| title_fullStr | Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin |
| title_full_unstemmed | Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin |
| title_short | Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin |
| title_sort | synthesis and physicochemical analysis of polystyrene-anchored pd(ii) metal complex / siti kamilah che soh, siti aminah jusoh and mustaffa shamsuddin |
| topic | Palladium Polystyrene |
| url | https://ir.uitm.edu.my/id/eprint/12430/ https://ir.uitm.edu.my/id/eprint/12430/ |