Supramolecular association in the triclinic (Z′ = 1) and monoclinic (Z′ = 4) polymorphs of 4-(4-acetylphenyl)piperazin-1-ium 2-amino4-nitrobenzoate
Crystallography reveals two polymorphs for the salt [4-(4- acetylphenyl)piperazin-1-ium][2-amino-4-nitrobenzoate], a monoclinic form (2; modelled as P21/n with Z' = 4) formed directly from the reaction mixture, and a triclinic form (1; Z' = 1) isolated from recrystallisation. Relatively m...
| Main Authors: | Jotani, Mukesh M., Wardell, James L., Tiekink, Edward R. T. * |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
De Gruyter for Oldenbourgh Verlag
2019
|
| Subjects: | |
| Online Access: | http://eprints.sunway.edu.my/988/ http://eprints.sunway.edu.my/988/1/Tiekink%20Supramolecular%20Z%20Kristallogr%202019%20234%2043%20final%20version.pdf |
Similar Items
Hydrazinium 2-amino-4-nitrobenzoate dihydrate: crystal structure and Hirshfeld surface analysis
by: Wardell, James L., et al.
Published: (2017)
by: Wardell, James L., et al.
Published: (2017)
4-(2-Methoxyphenyl)piperazin-1-ium 6-chloro-5-isopropyl-2,4-dioxopyrimidin-1-ide
by: A. M. Al-Omary, Fatmah, et al.
Published: (2014)
by: A. M. Al-Omary, Fatmah, et al.
Published: (2014)
Two dialkylammonium salts of 2-amino-4-nitrobenzoic acid: crystal structures and Hirshfeld surface analysis
by: Wardell, James L., et al.
Published: (2016)
by: Wardell, James L., et al.
Published: (2016)
6-Amino-3,4-dimethyl-1,2,4-triazin-1-ium 2-anilinobenzoate–3-amino-5,6-dimethyl-1,2,4-triazine (1/1)
by: Sangeetha, Ramalingam, et al.
Published: (2017)
by: Sangeetha, Ramalingam, et al.
Published: (2017)
6-Amino-3,4-dimethyl-1,2,4-triazin-1-ium
2-anilinobenzoate–3-amino-5,6-dimethyl-1,2,4-
triazine (1/1)
by: Sangeetha, Ramalingam, et al.
Published: (2017)
by: Sangeetha, Ramalingam, et al.
Published: (2017)
A monoclinic polymorph of 4-(2H-1,3-benzodioxol-5-yl)-1-(4-methylphenyl)-1H-pyrazol-5-amine
by: Jotani, Mukesh M., et al.
Published: (2015)
by: Jotani, Mukesh M., et al.
Published: (2015)
(E)-2-[4-(Diethylamino)styryl]-1-methylquinolin-
1-ium 4-chlorobenzenesulfonate
monohydrate
by: Chantrapromma, Suchada, et al.
Published: (2014)
by: Chantrapromma, Suchada, et al.
Published: (2014)
2-{[2,8-Bis(trifluoromethyl)quinolin-4-yl](hydroxy)methyl}piperidin-1-ium trichloroacetate: Crystal structure and Hirshfeld surface analysis
by: Wardell, James L., et al.
Published: (2018)
by: Wardell, James L., et al.
Published: (2018)
(4Z,6Z,12Z,14Z)-2,10-Dimethyl-2,8,10,16-tetrahydrodipyrazolo[3,4-e:3',4'-l][1,2,4,8,9,11]hexaazacyclotetradecine-4,12-diamine.
by: Dolzhenko, Anton, et al.
Published: (2009)
by: Dolzhenko, Anton, et al.
Published: (2009)
Ethyl 4-butylamino-3-nitrobenzoate
by: Narendra Babu, Shivanagere Nagojappa, et al.
Published: (2009)
by: Narendra Babu, Shivanagere Nagojappa, et al.
Published: (2009)
4-ethylamino-3-nitrobenzoic acid
by: Narendra Babu, Shivanagere Nagojappa, et al.
Published: (2009)
by: Narendra Babu, Shivanagere Nagojappa, et al.
Published: (2009)
On the influence of small chemical changes upon the supramolecular association in substituted 2-(phenoxy)-1,4-naphthoquinones
by: Tonin, Marlon D. L., et al.
Published: (2019)
by: Tonin, Marlon D. L., et al.
Published: (2019)
Ethyl 4-(2-hydroxyethylamino)-3-nitrobenzoate
by: Abdul Rahim, Aisyah Saad, et al.
Published: (2010)
by: Abdul Rahim, Aisyah Saad, et al.
Published: (2010)
4-(sec-butylamino)-3-nitrobenzoic acid
by: Narendra Babu, Shivanagere Nagojappa, et al.
Published: (2009)
by: Narendra Babu, Shivanagere Nagojappa, et al.
Published: (2009)
4-tert-Butylamino-3-nitrobenzoic acid
by: Narendra Babu, Shivanagere Nagojappa, et al.
Published: (2009)
by: Narendra Babu, Shivanagere Nagojappa, et al.
Published: (2009)
3-(Adamantan-1-yl)-4-ethyl-1-{[4-(2-methoxyphenyl)piperazin-1-yl]methyl}-1H-1,2,4-triazole-5(4H)-thione
by: El-Emam, Ali A., et al.
Published: (2014)
by: El-Emam, Ali A., et al.
Published: (2014)
Crystal structure and Hirshfeld surface analysis of 2-{[2,8-bis(trifluoromethyl)quinolin-4-yl](hydroxy)methyl}piperidin-1-ium 2-hydroxy-2-phenylacetate hemihydrate
by: Wardell, James L., et al.
Published: (2016)
by: Wardell, James L., et al.
Published: (2016)
Crystal structures of the 1:1 salts of 2-amino-4-nitrobenzoate with each of (2-hydroxyethyl)dimethylazanium, tert-butyl(2-hydroxyethyl)azanium and 1,3-dihydroxy-2-(hydroxymethyl)propan-2-aminium
by: Wardell, James L., et al.
Published: (2018)
by: Wardell, James L., et al.
Published: (2018)
Crystal structure of 1-{(Z)-[(2E)-3-(4-chlorophenyl)-1-phenylprop-2-en-1-ylidene]amino}-3-ethylthiourea
by: Tan, Ming Yueh, et al.
Published: (2015)
by: Tan, Ming Yueh, et al.
Published: (2015)
Crystal structure of 1-[(Z)-[4-(4-methoxyphenyl)butan-2-ylidene]amino]-3-phenylurea, C18H21N3O2
by: Tan, Ming Yueh, et al.
Published: (2018)
by: Tan, Ming Yueh, et al.
Published: (2018)
Crystal structure of 1-[(Z)-[4-(4-methoxyphenyl) butan-2 ylidene]amino]-3-phenylurea, C18H21N3O2
by: Tan, Ming Yueh, et al.
Published: (2018)
by: Tan, Ming Yueh, et al.
Published: (2018)
Crystal structure of 2,4-diamino-7-(hydroxymethyl)pteridin-1-ium nitrate
by: Sivajeyanthi, Palaniyappan, et al.
Published: (2015)
by: Sivajeyanthi, Palaniyappan, et al.
Published: (2015)
New monoclinic form of {O-Ethyl N-(4-nitrophenyl)thiocarbamato-κS}(tri-4-tolylphosphane-κP)gold(I): crystal structure and Hirshfeld surface analysis
by: Fong, Sheen Kuan, et al.
Published: (2017)
by: Fong, Sheen Kuan, et al.
Published: (2017)
9-Aminoacridin-10-ium 4-aminobenzoate dihydrate
by: Dhanabalan, Nallathambi, et al.
Published: (2014)
by: Dhanabalan, Nallathambi, et al.
Published: (2014)
4-Amino-3-(3-methoxybenzyl)-1H-1,2,4-triazole-5(4H)-thione
by: Hegde, Gurumurthy, et al.
Published: (2013)
by: Hegde, Gurumurthy, et al.
Published: (2013)
3-Methyl-4-{(E)-[4-(methylsulfanyl)-benzylidene]amino}-1H-1, 2,4-triazole-5(4H)-thione
by: Hegde, Gurumurthy, et al.
Published: (2013)
by: Hegde, Gurumurthy, et al.
Published: (2013)
Transcriptional analysis of the human D4Z4 and mouse Dux arrays
by: Hampson, Amanda
Published: (2012)
by: Hampson, Amanda
Published: (2012)
On the integral solutions of the diophantine equation x4 + y4 = z3
by: Ismail, S., et al.
Published: (2013)
by: Ismail, S., et al.
Published: (2013)
3-{(E)-[4-(4-Hydroxy-3-methoxyphenyl)butan-2-ylidene]amino}-1-phenylurea: crystal structure and Hirshfeld surface analysis
by: Tan, Ming Yueh, et al.
Published: (2018)
by: Tan, Ming Yueh, et al.
Published: (2018)
Supramolecular assemblies of 1,4-benzene diboronic acid on KCl(001)
by: Pawlak, R., et al.
Published: (2010)
by: Pawlak, R., et al.
Published: (2010)
Ethanol- and heat-mediated phase change from a kinetic (Z′ = 4) polymorph to a thermodynamic (Z′ = 1) polymorph for an N2,6-diaryl-1,3,5-triazine-2,4-diamine
by: Tan, Sang Loon *, et al.
Published: (2023)
by: Tan, Sang Loon *, et al.
Published: (2023)
2-({[(Pyridin-1-ium-2-ylmethyl)carbamoyl]formamido}methyl)pyridin-1-ium bis(3,5-dicarboxybenzoate): crystal structure and Hirshfeld surface analysis
by: Jotani, Mukesh M., et al.
Published: (2016)
by: Jotani, Mukesh M., et al.
Published: (2016)
Crystal structure of (2Z)-2-amino-3-[(E)-[(2,4-dihydroxyphenyl)methylidene]-amino]but-2-enedinitrile, C11H8N4O2
by: Lee, See Mun *, et al.
Published: (2020)
by: Lee, See Mun *, et al.
Published: (2020)
Crystal structure of (Z)-4-methylbenzyl 3-[1-(5-methylpyridin-2-yl)ethylidene]dithiocarbazate
by: Ravoof, Thahira Begum S. A., et al.
Published: (2015)
by: Ravoof, Thahira Begum S. A., et al.
Published: (2015)
Disentangling star formation and AGN activity in powerful infrared luminous radio galaxies at 1 < z < 4
by: Drouart, Guillaume, et al.
Published: (2016)
by: Drouart, Guillaume, et al.
Published: (2016)
A monoclinic polymorph of N-ethoxycarbonyl-N'-(3-phenyl-1H-1,2,4-triazol-5-yl)thiourea
by: Dolzhenko, Anton, et al.
Published: (2010)
by: Dolzhenko, Anton, et al.
Published: (2010)
Physical properties of z > 4 submillimeter galaxies
in the COSMOS field
by: Smolcic, V., et al.
Published: (2015)
by: Smolcic, V., et al.
Published: (2015)
Radio spectra of bright compact sources at z > 4.5
by: Coppejans, R., et al.
Published: (2017)
by: Coppejans, R., et al.
Published: (2017)
4-(4-Acetyl-5-methyl-1H-1,2,3-triazol-1-yl)benzonitrile: crystal structure and Hirshfeld surface analysis
by: Zukerman-Schpector, Julio, et al.
Published: (2018)
by: Zukerman-Schpector, Julio, et al.
Published: (2018)
Crystal Structure of 4-({(1E,2E)-3-[3-(4-fluorophenyl)-1-isopropyl-1H-indol-2-yl]allylidene}amino)1H-1,2,4-triazole-5(4H)-thione
by: Kulkarni, Ajaykumar D., et al.
Published: (2015)
by: Kulkarni, Ajaykumar D., et al.
Published: (2015)
Similar Items
-
Hydrazinium 2-amino-4-nitrobenzoate dihydrate: crystal structure and Hirshfeld surface analysis
by: Wardell, James L., et al.
Published: (2017) -
4-(2-Methoxyphenyl)piperazin-1-ium 6-chloro-5-isopropyl-2,4-dioxopyrimidin-1-ide
by: A. M. Al-Omary, Fatmah, et al.
Published: (2014) -
Two dialkylammonium salts of 2-amino-4-nitrobenzoic acid: crystal structures and Hirshfeld surface analysis
by: Wardell, James L., et al.
Published: (2016) -
6-Amino-3,4-dimethyl-1,2,4-triazin-1-ium 2-anilinobenzoate–3-amino-5,6-dimethyl-1,2,4-triazine (1/1)
by: Sangeetha, Ramalingam, et al.
Published: (2017) -
6-Amino-3,4-dimethyl-1,2,4-triazin-1-ium
2-anilinobenzoate–3-amino-5,6-dimethyl-1,2,4-
triazine (1/1)
by: Sangeetha, Ramalingam, et al.
Published: (2017)