Effect of deep eutectic solvent in proton conduction and thermal behaviour of chitosan-based membrane

This work aims to study the effect of choline chloride (ChCl) and urea based deep eutectic solvent (DES) on the proton conduction and thermal properties of chitosan-carboxymethylcellulose (Chitosan-CMC) membrane. Chitosan-CMC biocomposites were prepared in different ratios of 5:95, 10:90, 25:75, 50:...

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Main Authors: Wong, C. Y., Wong, W. Y., Walvekar, Rashmi, Loh, K. S., Khalid, Mohammad *, Lim, K. L.
Format: Article
Published: Elsevier 2018
Subjects:
Online Access:http://eprints.sunway.edu.my/969/
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author Wong, C. Y.
Wong, W. Y.
Walvekar, Rashmi
Loh, K. S.
Khalid, Mohammad *
Lim, K. L.
author_facet Wong, C. Y.
Wong, W. Y.
Walvekar, Rashmi
Loh, K. S.
Khalid, Mohammad *
Lim, K. L.
author_sort Wong, C. Y.
building SU Institutional Repository
collection Online Access
description This work aims to study the effect of choline chloride (ChCl) and urea based deep eutectic solvent (DES) on the proton conduction and thermal properties of chitosan-carboxymethylcellulose (Chitosan-CMC) membrane. Chitosan-CMC biocomposites were prepared in different ratios of 5:95, 10:90, 25:75, 50:50 and 75:25 with DES and was characterised. This study showed a positive improvement the proton conductivity without excessive swelling using DES in comparison with those without DES, with a slight trade-off on the thermal stability. The sample corresponding to 50 wt% of chitosan showed the highest proton conductivity of 1.57 × 10−2 S/cm, which was slightly lower compared to Nafion-117 membrane (8.6 × 10−2 S/cm). The study revealed the blend film with 75 wt% of chitosan with the presence of DES has a potential for polymer electrolyte membrane (PEM) with a low but sufficient water uptake of 49.4% to avoid structural disintegration despite a lower proton conductivity obtained.
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spelling sunway-9692019-04-25T07:44:24Z http://eprints.sunway.edu.my/969/ Effect of deep eutectic solvent in proton conduction and thermal behaviour of chitosan-based membrane Wong, C. Y. Wong, W. Y. Walvekar, Rashmi Loh, K. S. Khalid, Mohammad * Lim, K. L. QC Physics QD Chemistry This work aims to study the effect of choline chloride (ChCl) and urea based deep eutectic solvent (DES) on the proton conduction and thermal properties of chitosan-carboxymethylcellulose (Chitosan-CMC) membrane. Chitosan-CMC biocomposites were prepared in different ratios of 5:95, 10:90, 25:75, 50:50 and 75:25 with DES and was characterised. This study showed a positive improvement the proton conductivity without excessive swelling using DES in comparison with those without DES, with a slight trade-off on the thermal stability. The sample corresponding to 50 wt% of chitosan showed the highest proton conductivity of 1.57 × 10−2 S/cm, which was slightly lower compared to Nafion-117 membrane (8.6 × 10−2 S/cm). The study revealed the blend film with 75 wt% of chitosan with the presence of DES has a potential for polymer electrolyte membrane (PEM) with a low but sufficient water uptake of 49.4% to avoid structural disintegration despite a lower proton conductivity obtained. Elsevier 2018-08-20 Article PeerReviewed Wong, C. Y. and Wong, W. Y. and Walvekar, Rashmi and Loh, K. S. and Khalid, Mohammad * and Lim, K. L. (2018) Effect of deep eutectic solvent in proton conduction and thermal behaviour of chitosan-based membrane. Journal of Molecular Liquids, 269. pp. 675-683. ISSN 0167-7322 http://doi.org/10.1016/j.molliq.2018.08.102 doi:10.1016/j.molliq.2018.08.102
spellingShingle QC Physics
QD Chemistry
Wong, C. Y.
Wong, W. Y.
Walvekar, Rashmi
Loh, K. S.
Khalid, Mohammad *
Lim, K. L.
Effect of deep eutectic solvent in proton conduction and thermal behaviour of chitosan-based membrane
title Effect of deep eutectic solvent in proton conduction and thermal behaviour of chitosan-based membrane
title_full Effect of deep eutectic solvent in proton conduction and thermal behaviour of chitosan-based membrane
title_fullStr Effect of deep eutectic solvent in proton conduction and thermal behaviour of chitosan-based membrane
title_full_unstemmed Effect of deep eutectic solvent in proton conduction and thermal behaviour of chitosan-based membrane
title_short Effect of deep eutectic solvent in proton conduction and thermal behaviour of chitosan-based membrane
title_sort effect of deep eutectic solvent in proton conduction and thermal behaviour of chitosan-based membrane
topic QC Physics
QD Chemistry
url http://eprints.sunway.edu.my/969/
http://eprints.sunway.edu.my/969/
http://eprints.sunway.edu.my/969/