A new microwave-assisted, three-component reaction of 5-aminopyrazole-4-carboxylates:selective synthesis of substituted 5-aza-9-deaza-adenines
annulation of 1,3,5-triazine ring onto 5-aminopyrazole-4-carboxylates via a one-pot,multicomponent, microwave-assisted approach. The products were obtained in good yields and high purity. This catalyst-free method was demonstrated to be scalable and highly reproducible in different microwave reacto...
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| Format: | Article |
| Language: | English |
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Elsevier
2018
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| Online Access: | http://eprints.sunway.edu.my/790/ http://eprints.sunway.edu.my/790/1/Tiekink%20E%20A%20New%20microwave%20assisted.pdf |
| _version_ | 1848801896044691456 |
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| author | Lim, Felicia Phei Lin Halcovitch, Nathan R. Tiekink, Edward R. T. * Dolzhenko, Anton V |
| author_facet | Lim, Felicia Phei Lin Halcovitch, Nathan R. Tiekink, Edward R. T. * Dolzhenko, Anton V |
| author_sort | Lim, Felicia Phei Lin |
| building | SU Institutional Repository |
| collection | Online Access |
| description | annulation of 1,3,5-triazine ring onto 5-aminopyrazole-4-carboxylates via a one-pot,multicomponent, microwave-assisted approach. The products were obtained in good yields and high purity. This catalyst-free method was demonstrated to be scalable and highly reproducible in
different microwave reactors. Some structural features of the prepared compounds were studied in details using dynamic NMR spectroscopy and X-ray crystallography. |
| first_indexed | 2025-11-14T21:14:44Z |
| format | Article |
| id | sunway-790 |
| institution | Sunway University |
| institution_category | Local University |
| language | English |
| last_indexed | 2025-11-14T21:14:44Z |
| publishDate | 2018 |
| publisher | Elsevier |
| recordtype | eprints |
| repository_type | Digital Repository |
| spelling | sunway-7902020-10-07T09:06:55Z http://eprints.sunway.edu.my/790/ A new microwave-assisted, three-component reaction of 5-aminopyrazole-4-carboxylates:selective synthesis of substituted 5-aza-9-deaza-adenines Lim, Felicia Phei Lin Halcovitch, Nathan R. Tiekink, Edward R. T. * Dolzhenko, Anton V QD Chemistry annulation of 1,3,5-triazine ring onto 5-aminopyrazole-4-carboxylates via a one-pot,multicomponent, microwave-assisted approach. The products were obtained in good yields and high purity. This catalyst-free method was demonstrated to be scalable and highly reproducible in different microwave reactors. Some structural features of the prepared compounds were studied in details using dynamic NMR spectroscopy and X-ray crystallography. Elsevier 2018-04-12 Article PeerReviewed text en http://eprints.sunway.edu.my/790/1/Tiekink%20E%20A%20New%20microwave%20assisted.pdf Lim, Felicia Phei Lin and Halcovitch, Nathan R. and Tiekink, Edward R. T. * and Dolzhenko, Anton V (2018) A new microwave-assisted, three-component reaction of 5-aminopyrazole-4-carboxylates:selective synthesis of substituted 5-aza-9-deaza-adenines. Tetrahedron, 74 (15). pp. 1868-1879. ISSN 0040-4020 |
| spellingShingle | QD Chemistry Lim, Felicia Phei Lin Halcovitch, Nathan R. Tiekink, Edward R. T. * Dolzhenko, Anton V A new microwave-assisted, three-component reaction of 5-aminopyrazole-4-carboxylates:selective synthesis of substituted 5-aza-9-deaza-adenines |
| title | A new microwave-assisted, three-component reaction of 5-aminopyrazole-4-carboxylates:selective synthesis of substituted 5-aza-9-deaza-adenines |
| title_full | A new microwave-assisted, three-component reaction of 5-aminopyrazole-4-carboxylates:selective synthesis of substituted 5-aza-9-deaza-adenines |
| title_fullStr | A new microwave-assisted, three-component reaction of 5-aminopyrazole-4-carboxylates:selective synthesis of substituted 5-aza-9-deaza-adenines |
| title_full_unstemmed | A new microwave-assisted, three-component reaction of 5-aminopyrazole-4-carboxylates:selective synthesis of substituted 5-aza-9-deaza-adenines |
| title_short | A new microwave-assisted, three-component reaction of 5-aminopyrazole-4-carboxylates:selective synthesis of substituted 5-aza-9-deaza-adenines |
| title_sort | new microwave-assisted, three-component reaction of 5-aminopyrazole-4-carboxylates:selective synthesis of substituted 5-aza-9-deaza-adenines |
| topic | QD Chemistry |
| url | http://eprints.sunway.edu.my/790/ http://eprints.sunway.edu.my/790/1/Tiekink%20E%20A%20New%20microwave%20assisted.pdf |