1-Anilino-5-methyl-1H-1,2,3-triazole-4-carbaldehyde

The title compound, C10H10N4O, is twisted about the Nring-Namine bond with the dihedral angle between the 1,2,3-triazolyl and N-bound phenyl rings being 79.14 (9)°. The C-bound aldehyde group is coplanar with the triazolyl ring, with the N-C-C-O torsion angle being 3.5 (3)°. While coplanar, the alde...

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Bibliographic Details
Main Authors: Cunha, Anna C., Jordão, Alessandro K., Souza, Maria C. B. V. de, Ferreira, Vitor F., Almeida, Maria C. B. de, Wardell, James L., Tiekink, Edward R. T. *
Format: Article
Language:English
Published: International Union of Crystallography 2016
Subjects:
Online Access:http://eprints.sunway.edu.my/664/
http://eprints.sunway.edu.my/664/1/IUCrData%202016%201%20x160038.pdf
Description
Summary:The title compound, C10H10N4O, is twisted about the Nring-Namine bond with the dihedral angle between the 1,2,3-triazolyl and N-bound phenyl rings being 79.14 (9)°. The C-bound aldehyde group is coplanar with the triazolyl ring, with the N-C-C-O torsion angle being 3.5 (3)°. While coplanar, the aldehyde O atom is orientated in the opposite direction to the triazolyl-bound methyl group. The most prominent feature of the mol­ecular packing is the formation of zigzag chains (glide symmetry) along the b axis and mediated by amine-N-H...N(triazol­yl) hydrogen bonds. The chains are connected into supra­molecular layers by phenyl- and methyl-C-H...O(aldehyde) inter­actions, with phenyl groups projecting to either side. Layers stack along the c axis with no directional inter­actions between them.