Persistence of C–H⋯π(chelate ring) interactions in the crystal structures of Pd(S2COR)2. The utility of Pd(S2COR)2 as precursors for palladium sulphide materials

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Persistence of C–H⋯π(chelate ring) interactions in the crystal structures of Pd(S2COR)2. The utility of Pd(S2COR)2 as precursors for palladium sulphide materials

The crystallographic structures of 12 palladium xanthates, PdĲS2COR)2 (R = alkyl) show a uniform adoption of square-planar PdS4 geometries. Supramolecular aggregation in 1 (R = Me), 2 (Et) and 3 (n-Pr) is based on secondary Pd⋯S interactions, which are “turned off” when the bulk of R increases. In...

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Bibliographic Details
Main Authors:	Tan, Yee Seng , Siti Nadiah Abdul Halim, Molloy, Kieran C., Sudlow, Anna L., Otero-de-la-Roza, Alberto, Tiekink, Edward R. T.
Format:	Article
Published:	Royal Society of Chemistry 2016
Subjects:	QD Chemistry
Online Access:	http://eprints.sunway.edu.my/615/

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