Dual role of Magnesium as a catalyst and precursor with enriched boron in the synthesis of Magnesium diboride nanoparticles

Nano-scale powder of Magnesium (Mg) is found to play the dual role of catalyst and precursor with Boron-10 (10B) in the synthesis of Magnesium diboride nanoparticles (Mg10B2NPs) at 800 °C. Catalytically, Mg softens and melts enriched Boron at a relatively lower temperature than its actual boiling po...

Full description

Bibliographic Details
Main Authors: Ahmad, P., Khandaker, Mayeen Uddin *, Jamil, S., Rehman, F., Muhammad, N., Ullah, Z., Rauf Khan, M., Khan, G., Alotaibi, M. A., Alharthi, A. I., Din, I. U., Hussain, F., Khan, M. I., Ali, H.
Format: Article
Published: Elsevier 2020
Subjects:
Online Access:http://eprints.sunway.edu.my/1607/
_version_ 1848802098721849344
author Ahmad, P.
Khandaker, Mayeen Uddin *
Jamil, S.
Rehman, F.
Muhammad, N.
Ullah, Z.
Rauf Khan, M.
Khan, G.
Alotaibi, M. A.
Alharthi, A. I.
Din, I. U.
Hussain, F.
Khan, M. I.
Ali, H.
author_facet Ahmad, P.
Khandaker, Mayeen Uddin *
Jamil, S.
Rehman, F.
Muhammad, N.
Ullah, Z.
Rauf Khan, M.
Khan, G.
Alotaibi, M. A.
Alharthi, A. I.
Din, I. U.
Hussain, F.
Khan, M. I.
Ali, H.
author_sort Ahmad, P.
building SU Institutional Repository
collection Online Access
description Nano-scale powder of Magnesium (Mg) is found to play the dual role of catalyst and precursor with Boron-10 (10B) in the synthesis of Magnesium diboride nanoparticles (Mg10B2NPs) at 800 °C. Catalytically, Mg softens and melts enriched Boron at a relatively lower temperature than its actual boiling point. As a precursor, it reacts with enriched Boron and forms the Mg10B2 compound. The nano-size catalyst and precursors help to grow the as-formed Mg10B2 compound in the form of nanoparticles. The shape or morphology of the synthesized Mg10B2NPs is revealed via field emission scanning electron microscopy (FESEM). Energy dispersive x-ray (EDX) spectroscopy has been performed to spot the elemental composition, whereas, X-ray diffraction (XRD), and X-ray photoelectron spectroscopy (XPS) are used to verify the composition and study the phase of the synthesized particles.
first_indexed 2025-11-14T21:17:57Z
format Article
id sunway-1607
institution Sunway University
institution_category Local University
last_indexed 2025-11-14T21:17:57Z
publishDate 2020
publisher Elsevier
recordtype eprints
repository_type Digital Repository
spelling sunway-16072021-03-11T07:16:43Z http://eprints.sunway.edu.my/1607/ Dual role of Magnesium as a catalyst and precursor with enriched boron in the synthesis of Magnesium diboride nanoparticles Ahmad, P. Khandaker, Mayeen Uddin * Jamil, S. Rehman, F. Muhammad, N. Ullah, Z. Rauf Khan, M. Khan, G. Alotaibi, M. A. Alharthi, A. I. Din, I. U. Hussain, F. Khan, M. I. Ali, H. R895-920 Medical Physics/Medical Radiology Nano-scale powder of Magnesium (Mg) is found to play the dual role of catalyst and precursor with Boron-10 (10B) in the synthesis of Magnesium diboride nanoparticles (Mg10B2NPs) at 800 °C. Catalytically, Mg softens and melts enriched Boron at a relatively lower temperature than its actual boiling point. As a precursor, it reacts with enriched Boron and forms the Mg10B2 compound. The nano-size catalyst and precursors help to grow the as-formed Mg10B2 compound in the form of nanoparticles. The shape or morphology of the synthesized Mg10B2NPs is revealed via field emission scanning electron microscopy (FESEM). Energy dispersive x-ray (EDX) spectroscopy has been performed to spot the elemental composition, whereas, X-ray diffraction (XRD), and X-ray photoelectron spectroscopy (XPS) are used to verify the composition and study the phase of the synthesized particles. Elsevier 2020-12 Article PeerReviewed Ahmad, P. and Khandaker, Mayeen Uddin * and Jamil, S. and Rehman, F. and Muhammad, N. and Ullah, Z. and Rauf Khan, M. and Khan, G. and Alotaibi, M. A. and Alharthi, A. I. and Din, I. U. and Hussain, F. and Khan, M. I. and Ali, H. (2020) Dual role of Magnesium as a catalyst and precursor with enriched boron in the synthesis of Magnesium diboride nanoparticles. Ceramics International, 46 (17). pp. 26809-26812. ISSN 0272-8842 http://doi.org/10.1016/j.ceramint.2020.07.156 doi:10.1016/j.ceramint.2020.07.156
spellingShingle R895-920 Medical Physics/Medical Radiology
Ahmad, P.
Khandaker, Mayeen Uddin *
Jamil, S.
Rehman, F.
Muhammad, N.
Ullah, Z.
Rauf Khan, M.
Khan, G.
Alotaibi, M. A.
Alharthi, A. I.
Din, I. U.
Hussain, F.
Khan, M. I.
Ali, H.
Dual role of Magnesium as a catalyst and precursor with enriched boron in the synthesis of Magnesium diboride nanoparticles
title Dual role of Magnesium as a catalyst and precursor with enriched boron in the synthesis of Magnesium diboride nanoparticles
title_full Dual role of Magnesium as a catalyst and precursor with enriched boron in the synthesis of Magnesium diboride nanoparticles
title_fullStr Dual role of Magnesium as a catalyst and precursor with enriched boron in the synthesis of Magnesium diboride nanoparticles
title_full_unstemmed Dual role of Magnesium as a catalyst and precursor with enriched boron in the synthesis of Magnesium diboride nanoparticles
title_short Dual role of Magnesium as a catalyst and precursor with enriched boron in the synthesis of Magnesium diboride nanoparticles
title_sort dual role of magnesium as a catalyst and precursor with enriched boron in the synthesis of magnesium diboride nanoparticles
topic R895-920 Medical Physics/Medical Radiology
url http://eprints.sunway.edu.my/1607/
http://eprints.sunway.edu.my/1607/
http://eprints.sunway.edu.my/1607/