Synthesis and characterization of zinc oxide nanoparticles prepared via precipitation and self- combustion methods

Zinc oxide is an important chemical substance that is widely used in the production of various industrial products. However, to produce nano particle ZnO remains a challenge. This paper describes the synthesis of zinc oxide nanoparticles via precipitation and self-combustion methods. By precipitatio...

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Main Authors: N., Yahya, S.M.S.N.S., Zahari, A., Ramli, N.M., Mohamad, P., Puspitasari, N.L., Che Zul
Format: Conference or Workshop Item
Language:English
Published: 2009
Subjects:
Online Access:http://scholars.utp.edu.my/id/eprint/473/
http://scholars.utp.edu.my/id/eprint/473/1/paper.pdf
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author N., Yahya
S.M.S.N.S., Zahari
A., Ramli
N.M., Mohamad
P., Puspitasari
N.L., Che Zul
author_facet N., Yahya
S.M.S.N.S., Zahari
A., Ramli
N.M., Mohamad
P., Puspitasari
N.L., Che Zul
author_sort N., Yahya
building UTP Institutional Repository
collection Online Access
description Zinc oxide is an important chemical substance that is widely used in the production of various industrial products. However, to produce nano particle ZnO remains a challenge. This paper describes the synthesis of zinc oxide nanoparticles via precipitation and self-combustion methods. By precipitation method, the dissolved zinc nitrate solution is drop wisely into aqueous sodium hydroxide, NaOH as precipitating agent. Self-combustion technique is a new method to obtain nanoparticles by heating the materials until it combust at 110°C. Experiment has been done by dissolving Zn(NO<sub>3</sub>) <sub>2</sub>.6H<sub>2</sub>O and HNO<sub>3</sub>. The dissolved solution was then stirred for 2 and 4 days followed by heating process until 110°C. By the data analysis, it demonstrated that ZnO prepared via selfcombustion gave better morphology, which can be referred to single-phase with nanorods structure at 2θ of 13.05° with average crystallite size of 563.10 nm. Raman and XRD result for self-combustion show higher purity singlephase structure compared to those samples prepared using precipitation technique. © 2009 American Institute of Physics.
first_indexed 2025-11-13T07:23:24Z
format Conference or Workshop Item
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institution Universiti Teknologi Petronas
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language English
last_indexed 2025-11-13T07:23:24Z
publishDate 2009
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repository_type Digital Repository
spelling oai:scholars.utp.edu.my:4732017-01-19T08:25:51Z http://scholars.utp.edu.my/id/eprint/473/ Synthesis and characterization of zinc oxide nanoparticles prepared via precipitation and self- combustion methods N., Yahya S.M.S.N.S., Zahari A., Ramli N.M., Mohamad P., Puspitasari N.L., Che Zul TK Electrical engineering. Electronics Nuclear engineering Zinc oxide is an important chemical substance that is widely used in the production of various industrial products. However, to produce nano particle ZnO remains a challenge. This paper describes the synthesis of zinc oxide nanoparticles via precipitation and self-combustion methods. By precipitation method, the dissolved zinc nitrate solution is drop wisely into aqueous sodium hydroxide, NaOH as precipitating agent. Self-combustion technique is a new method to obtain nanoparticles by heating the materials until it combust at 110°C. Experiment has been done by dissolving Zn(NO<sub>3</sub>) <sub>2</sub>.6H<sub>2</sub>O and HNO<sub>3</sub>. The dissolved solution was then stirred for 2 and 4 days followed by heating process until 110°C. By the data analysis, it demonstrated that ZnO prepared via selfcombustion gave better morphology, which can be referred to single-phase with nanorods structure at 2θ of 13.05° with average crystallite size of 563.10 nm. Raman and XRD result for self-combustion show higher purity singlephase structure compared to those samples prepared using precipitation technique. © 2009 American Institute of Physics. 2009 Conference or Workshop Item NonPeerReviewed application/pdf en http://scholars.utp.edu.my/id/eprint/473/1/paper.pdf N., Yahya and S.M.S.N.S., Zahari and A., Ramli and N.M., Mohamad and P., Puspitasari and N.L., Che Zul (2009) Synthesis and characterization of zinc oxide nanoparticles prepared via precipitation and self- combustion methods. In: International Conference on Nanoscience and Nanotechnology, Nano-SciTech 2008, 18 November 2008 through 21 November 2008, Selangor. http://www.scopus.com/inward/record.url?eid=2-s2.0-70450237501&partnerID=40&md5=b7a776ab9fe008b2d03b4f0707a8903d
spellingShingle TK Electrical engineering. Electronics Nuclear engineering
N., Yahya
S.M.S.N.S., Zahari
A., Ramli
N.M., Mohamad
P., Puspitasari
N.L., Che Zul
Synthesis and characterization of zinc oxide nanoparticles prepared via precipitation and self- combustion methods
title Synthesis and characterization of zinc oxide nanoparticles prepared via precipitation and self- combustion methods
title_full Synthesis and characterization of zinc oxide nanoparticles prepared via precipitation and self- combustion methods
title_fullStr Synthesis and characterization of zinc oxide nanoparticles prepared via precipitation and self- combustion methods
title_full_unstemmed Synthesis and characterization of zinc oxide nanoparticles prepared via precipitation and self- combustion methods
title_short Synthesis and characterization of zinc oxide nanoparticles prepared via precipitation and self- combustion methods
title_sort synthesis and characterization of zinc oxide nanoparticles prepared via precipitation and self- combustion methods
topic TK Electrical engineering. Electronics Nuclear engineering
url http://scholars.utp.edu.my/id/eprint/473/
http://scholars.utp.edu.my/id/eprint/473/
http://scholars.utp.edu.my/id/eprint/473/1/paper.pdf