Optical properties of Fe2+ Ion doped ZnS nanoparticles synthesized using co-precipitation method
Nanoparticles of Zn1-xFexS (x = 0.0, 0.1, 0.2 and 0.3) were prepared by chemical co-precipitation method from homogenous solution of zinc and ferum salt at room temperature with controlled parameter. These nanoparticles were sterically stabilized using Sodium Hexamethaphospate (SHMP). Here, a stud...
| Main Authors: | , , |
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| Format: | Article |
| Language: | English |
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Fakulti Kejuruteraan ,UKM,Bangi.
2015
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| Online Access: | http://journalarticle.ukm.my/9512/ http://journalarticle.ukm.my/9512/1/12.pdf |
| _version_ | 1848812111945269248 |
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| author | Rahizana Mohd Ibrahim, Masturah Markom, Kamal Firdausi Abd Razak, |
| author_facet | Rahizana Mohd Ibrahim, Masturah Markom, Kamal Firdausi Abd Razak, |
| author_sort | Rahizana Mohd Ibrahim, |
| building | UKM Institutional Repository |
| collection | Online Access |
| description | Nanoparticles of Zn1-xFexS (x = 0.0, 0.1, 0.2 and 0.3) were prepared by chemical co-precipitation method from homogenous
solution of zinc and ferum salt at room temperature with controlled parameter. These nanoparticles were sterically
stabilized using Sodium Hexamethaphospate (SHMP). Here, a study of the effect of Fe doping on structure and optical
properties of nanoparticles was undertaken. Structure, elemental analysis and optical properties have been investigated
by X-ray Diffraction (XRD), Transmission Electron Microscopy (TEM), Fourier-Transform-Infrared spectroscopy (FT-IR),
X-Ray Fluorescence (XRF), UV-Visible Spectroscopy and photoluminescence (PL) spectrophotometer. FT-IR and XRF results
confi rmed the incorporation of ion dopants into ZnS crystal structure, and XRD results showed that Zn1-xFexS (x = 0.00
and 0.10) nanoparticles crystallized in a zinc blende structure without any impurity. The particle size of all of samples
ranged from 2 nm to 3 nm, as calculated by the Debye-Scherrer formula. The optical absorption spectra indicate a blue
shift of the absorption edge with increasing Fe-content. The luminescence of nanoparticles excite at about 370 nm with
an emission peak at around at 452 nm, 490 nm and 550 nm. |
| first_indexed | 2025-11-14T23:57:06Z |
| format | Article |
| id | oai:generic.eprints.org:9512 |
| institution | Universiti Kebangasaan Malaysia |
| institution_category | Local University |
| language | English |
| last_indexed | 2025-11-14T23:57:06Z |
| publishDate | 2015 |
| publisher | Fakulti Kejuruteraan ,UKM,Bangi. |
| recordtype | eprints |
| repository_type | Digital Repository |
| spelling | oai:generic.eprints.org:95122016-12-14T06:50:09Z http://journalarticle.ukm.my/9512/ Optical properties of Fe2+ Ion doped ZnS nanoparticles synthesized using co-precipitation method Rahizana Mohd Ibrahim, Masturah Markom, Kamal Firdausi Abd Razak, Nanoparticles of Zn1-xFexS (x = 0.0, 0.1, 0.2 and 0.3) were prepared by chemical co-precipitation method from homogenous solution of zinc and ferum salt at room temperature with controlled parameter. These nanoparticles were sterically stabilized using Sodium Hexamethaphospate (SHMP). Here, a study of the effect of Fe doping on structure and optical properties of nanoparticles was undertaken. Structure, elemental analysis and optical properties have been investigated by X-ray Diffraction (XRD), Transmission Electron Microscopy (TEM), Fourier-Transform-Infrared spectroscopy (FT-IR), X-Ray Fluorescence (XRF), UV-Visible Spectroscopy and photoluminescence (PL) spectrophotometer. FT-IR and XRF results confi rmed the incorporation of ion dopants into ZnS crystal structure, and XRD results showed that Zn1-xFexS (x = 0.00 and 0.10) nanoparticles crystallized in a zinc blende structure without any impurity. The particle size of all of samples ranged from 2 nm to 3 nm, as calculated by the Debye-Scherrer formula. The optical absorption spectra indicate a blue shift of the absorption edge with increasing Fe-content. The luminescence of nanoparticles excite at about 370 nm with an emission peak at around at 452 nm, 490 nm and 550 nm. Fakulti Kejuruteraan ,UKM,Bangi. 2015 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/9512/1/12.pdf Rahizana Mohd Ibrahim, and Masturah Markom, and Kamal Firdausi Abd Razak, (2015) Optical properties of Fe2+ Ion doped ZnS nanoparticles synthesized using co-precipitation method. Jurnal Kejuruteraan, 27 . pp. 87-94. ISSN 0128-0198 http://www.ukm.my/jkukm/?page_id=557 |
| spellingShingle | Rahizana Mohd Ibrahim, Masturah Markom, Kamal Firdausi Abd Razak, Optical properties of Fe2+ Ion doped ZnS nanoparticles synthesized using co-precipitation method |
| title | Optical properties of Fe2+ Ion doped ZnS nanoparticles synthesized
using co-precipitation method |
| title_full | Optical properties of Fe2+ Ion doped ZnS nanoparticles synthesized
using co-precipitation method |
| title_fullStr | Optical properties of Fe2+ Ion doped ZnS nanoparticles synthesized
using co-precipitation method |
| title_full_unstemmed | Optical properties of Fe2+ Ion doped ZnS nanoparticles synthesized
using co-precipitation method |
| title_short | Optical properties of Fe2+ Ion doped ZnS nanoparticles synthesized
using co-precipitation method |
| title_sort | optical properties of fe2+ ion doped zns nanoparticles synthesized
using co-precipitation method |
| url | http://journalarticle.ukm.my/9512/ http://journalarticle.ukm.my/9512/ http://journalarticle.ukm.my/9512/1/12.pdf |