Silica aerogels’ nanostructure studied using small angle neutron scattering technique

Small angle neutron scattering (SANS) technique has been widely employed in probing the microstructure of amorphous materials in the nanometer range. In aerogels system, the size range of 1 – 100 nm is of particular interest since the structural units, such as the pores and particles, often fall in...

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Main Authors: Noorddin Ibrahim, Tan, Chier Fang
Format: Article
Language:English
Published: Universiti Kebangsaan Malaysia 2010
Online Access:http://journalarticle.ukm.my/7331/
http://journalarticle.ukm.my/7331/1/01_Md_Yeaminhossain.pdf
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author Noorddin Ibrahim,
Tan, Chier Fang
author_facet Noorddin Ibrahim,
Tan, Chier Fang
author_sort Noorddin Ibrahim,
building UKM Institutional Repository
collection Online Access
description Small angle neutron scattering (SANS) technique has been widely employed in probing the microstructure of amorphous materials in the nanometer range. In aerogels system, the size range of 1 – 100 nm is of particular interest since the structural units, such as the pores and particles, often fall in this range. In a typical scattering experiment, scattered neutron intensity is measured as a function of the scattering angle. Various plots of intensity I(Q) and scattering vector, Q, can provide information about fractal dimensions, and particle and cluster sizes. In this study, SANS facilities, at Nuklear Malaysia (NM) and Badan Tenaga Atom Nasional(BATAN), Indonesia were used to analyse particle and cluster size of silica aerogels and titanium containing silica aerogels. Results from NM showed that silica aerogels have surface fractal dimension while titanium containing silica aerogels have mass fractal dimension. On the other hand, results from BATAN showed that both silica aerogels and titanium containing silica aerogels have mass fractal dimension. The particle size for silica aerogels and titanium containing silica aerogels samples obtained by NM were 11.18 ± 0.03 and 9.19 ± 0.06 nm, respectively while the respective values obtained from BATAN measurements were 11.78 ± 0.06 and 10.57 ± 0.07 nm.
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spelling oai:generic.eprints.org:73312016-12-14T06:43:46Z http://journalarticle.ukm.my/7331/ Silica aerogels’ nanostructure studied using small angle neutron scattering technique Noorddin Ibrahim, Tan, Chier Fang Small angle neutron scattering (SANS) technique has been widely employed in probing the microstructure of amorphous materials in the nanometer range. In aerogels system, the size range of 1 – 100 nm is of particular interest since the structural units, such as the pores and particles, often fall in this range. In a typical scattering experiment, scattered neutron intensity is measured as a function of the scattering angle. Various plots of intensity I(Q) and scattering vector, Q, can provide information about fractal dimensions, and particle and cluster sizes. In this study, SANS facilities, at Nuklear Malaysia (NM) and Badan Tenaga Atom Nasional(BATAN), Indonesia were used to analyse particle and cluster size of silica aerogels and titanium containing silica aerogels. Results from NM showed that silica aerogels have surface fractal dimension while titanium containing silica aerogels have mass fractal dimension. On the other hand, results from BATAN showed that both silica aerogels and titanium containing silica aerogels have mass fractal dimension. The particle size for silica aerogels and titanium containing silica aerogels samples obtained by NM were 11.18 ± 0.03 and 9.19 ± 0.06 nm, respectively while the respective values obtained from BATAN measurements were 11.78 ± 0.06 and 10.57 ± 0.07 nm. Universiti Kebangsaan Malaysia 2010-04 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/7331/1/01_Md_Yeaminhossain.pdf Noorddin Ibrahim, and Tan, Chier Fang (2010) Silica aerogels’ nanostructure studied using small angle neutron scattering technique. Sains Malaysiana, 39 (2). pp. 275-280. ISSN 0126-6039 http://www.ukm.my/jsm/english_journals/vol39num2_2010/contentsVol39num2_2010.html
spellingShingle Noorddin Ibrahim,
Tan, Chier Fang
Silica aerogels’ nanostructure studied using small angle neutron scattering technique
title Silica aerogels’ nanostructure studied using small angle neutron scattering technique
title_full Silica aerogels’ nanostructure studied using small angle neutron scattering technique
title_fullStr Silica aerogels’ nanostructure studied using small angle neutron scattering technique
title_full_unstemmed Silica aerogels’ nanostructure studied using small angle neutron scattering technique
title_short Silica aerogels’ nanostructure studied using small angle neutron scattering technique
title_sort silica aerogels’ nanostructure studied using small angle neutron scattering technique
url http://journalarticle.ukm.my/7331/
http://journalarticle.ukm.my/7331/
http://journalarticle.ukm.my/7331/1/01_Md_Yeaminhossain.pdf