Extraction and characterization of pectin from dragon fruit (Hylocereus polyrhizus) using various extraction conditions. (Pengekstrakan dan pencirian pektin daripada buah naga (hylocereus polyrhizus)menggunakan pelbagai keadaan pengekstrakan)

The extraction of pectin from dragon fruit (Hylocereus polyrhizus) peels under three different extraction conditions was identified as an alternative source of commercial pectin. In this work, dried alcohol-insoluble residues (AIR) of dragon fruit peels were treated separately with 0.25% ammonium ox...

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Main Authors: Norazelina Sah Mohd. Ismail, Nazaruddin Ramli, Norziah Mohd. Hani, Zainudin Meon
Format: Article
Language:English
Published: Universiti Kebangsaan Malaysia 2012
Online Access:http://journalarticle.ukm.my/3228/
http://journalarticle.ukm.my/3228/1/05_Norazelina.pdf
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author Norazelina Sah Mohd. Ismail,
Nazaruddin Ramli,
Norziah Mohd. Hani,
Zainudin Meon,
author_facet Norazelina Sah Mohd. Ismail,
Nazaruddin Ramli,
Norziah Mohd. Hani,
Zainudin Meon,
author_sort Norazelina Sah Mohd. Ismail,
building UKM Institutional Repository
collection Online Access
description The extraction of pectin from dragon fruit (Hylocereus polyrhizus) peels under three different extraction conditions was identified as an alternative source of commercial pectin. In this work, dried alcohol-insoluble residues (AIR) of dragon fruit peels were treated separately with 0.25% ammonium oxalate/oxalic acid at a pH of 4.6 at 85oC; 0.03 M HCl at a pH of 1.5 at 85oC; and de-ionized water at 75oC. The pectin obtained from these methods was compared in terms of yield, physicochemical properties and chemical structure. Fourier Transform Infrared Spectroscopy (FTIR) was used in the identification of dragon fruit pectins. The results showed that the pectin yield (14.96-20.14% based on dry weight), moisture content (11.13-11.33%), ash content (6.88-11.55%), equivalent weight (475.64-713.99), methoxyl content (2.98-4.34%), anhydrouronic acid (45.25-52.45%) and the degree of esterification (31.05-46.96%) varied significantly (p < 0.05) with the various extraction conditions used. Pectin extracted with ammonium oxalate gave the highest yield of pectin, with high purity and low ash content. Based on the value of methoxyl content and the degree of esterification, dragon fruit pectin can be categorized as low-methoxyl pectin.
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spelling oai:generic.eprints.org:32282016-12-14T06:34:00Z http://journalarticle.ukm.my/3228/ Extraction and characterization of pectin from dragon fruit (Hylocereus polyrhizus) using various extraction conditions. (Pengekstrakan dan pencirian pektin daripada buah naga (hylocereus polyrhizus)menggunakan pelbagai keadaan pengekstrakan) Norazelina Sah Mohd. Ismail, Nazaruddin Ramli, Norziah Mohd. Hani, Zainudin Meon, The extraction of pectin from dragon fruit (Hylocereus polyrhizus) peels under three different extraction conditions was identified as an alternative source of commercial pectin. In this work, dried alcohol-insoluble residues (AIR) of dragon fruit peels were treated separately with 0.25% ammonium oxalate/oxalic acid at a pH of 4.6 at 85oC; 0.03 M HCl at a pH of 1.5 at 85oC; and de-ionized water at 75oC. The pectin obtained from these methods was compared in terms of yield, physicochemical properties and chemical structure. Fourier Transform Infrared Spectroscopy (FTIR) was used in the identification of dragon fruit pectins. The results showed that the pectin yield (14.96-20.14% based on dry weight), moisture content (11.13-11.33%), ash content (6.88-11.55%), equivalent weight (475.64-713.99), methoxyl content (2.98-4.34%), anhydrouronic acid (45.25-52.45%) and the degree of esterification (31.05-46.96%) varied significantly (p < 0.05) with the various extraction conditions used. Pectin extracted with ammonium oxalate gave the highest yield of pectin, with high purity and low ash content. Based on the value of methoxyl content and the degree of esterification, dragon fruit pectin can be categorized as low-methoxyl pectin. Universiti Kebangsaan Malaysia 2012-01 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/3228/1/05_Norazelina.pdf Norazelina Sah Mohd. Ismail, and Nazaruddin Ramli, and Norziah Mohd. Hani, and Zainudin Meon, (2012) Extraction and characterization of pectin from dragon fruit (Hylocereus polyrhizus) using various extraction conditions. (Pengekstrakan dan pencirian pektin daripada buah naga (hylocereus polyrhizus)menggunakan pelbagai keadaan pengekstrakan). Sains Malaysiana, 41 (1). pp. 41-45. ISSN 0126-6039 http://www.ukm.my/jsm/contents.html
spellingShingle Norazelina Sah Mohd. Ismail,
Nazaruddin Ramli,
Norziah Mohd. Hani,
Zainudin Meon,
Extraction and characterization of pectin from dragon fruit (Hylocereus polyrhizus) using various extraction conditions. (Pengekstrakan dan pencirian pektin daripada buah naga (hylocereus polyrhizus)menggunakan pelbagai keadaan pengekstrakan)
title Extraction and characterization of pectin from dragon fruit (Hylocereus polyrhizus) using various extraction conditions. (Pengekstrakan dan pencirian pektin daripada buah naga (hylocereus polyrhizus)menggunakan pelbagai keadaan pengekstrakan)
title_full Extraction and characterization of pectin from dragon fruit (Hylocereus polyrhizus) using various extraction conditions. (Pengekstrakan dan pencirian pektin daripada buah naga (hylocereus polyrhizus)menggunakan pelbagai keadaan pengekstrakan)
title_fullStr Extraction and characterization of pectin from dragon fruit (Hylocereus polyrhizus) using various extraction conditions. (Pengekstrakan dan pencirian pektin daripada buah naga (hylocereus polyrhizus)menggunakan pelbagai keadaan pengekstrakan)
title_full_unstemmed Extraction and characterization of pectin from dragon fruit (Hylocereus polyrhizus) using various extraction conditions. (Pengekstrakan dan pencirian pektin daripada buah naga (hylocereus polyrhizus)menggunakan pelbagai keadaan pengekstrakan)
title_short Extraction and characterization of pectin from dragon fruit (Hylocereus polyrhizus) using various extraction conditions. (Pengekstrakan dan pencirian pektin daripada buah naga (hylocereus polyrhizus)menggunakan pelbagai keadaan pengekstrakan)
title_sort extraction and characterization of pectin from dragon fruit (hylocereus polyrhizus) using various extraction conditions. (pengekstrakan dan pencirian pektin daripada buah naga (hylocereus polyrhizus)menggunakan pelbagai keadaan pengekstrakan)
url http://journalarticle.ukm.my/3228/
http://journalarticle.ukm.my/3228/
http://journalarticle.ukm.my/3228/1/05_Norazelina.pdf