Profiling of volatile compounds in beef, rat, and wild boar meat using SPME-GC/ MS

The high beef price triggers adulteration of beef and other non-halal animal meat, such as wild boar and rats. An appropriate and effective analytical method is needed to differentiate halal and non-halal animal meat. The SPME/ GC-MS method could authenticate meat based on specific volatile compo...

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Main Authors: Lia Amalia, Kusnandar, Feri, Nancy Dewi Yuliana, Purwantiningsih Sugita
Format: Article
Language:English
Published: Penerbit Universiti Kebangsaan Malaysia 2022
Online Access:http://journalarticle.ukm.my/20645/
http://journalarticle.ukm.my/20645/1/13.pdf
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author Lia Amalia,
Kusnandar, Feri
Nancy Dewi Yuliana,
Purwantiningsih Sugita,
author_facet Lia Amalia,
Kusnandar, Feri
Nancy Dewi Yuliana,
Purwantiningsih Sugita,
author_sort Lia Amalia,
building UKM Institutional Repository
collection Online Access
description The high beef price triggers adulteration of beef and other non-halal animal meat, such as wild boar and rats. An appropriate and effective analytical method is needed to differentiate halal and non-halal animal meat. The SPME/ GC-MS method could authenticate meat based on specific volatile compounds in each meat. The objective of this study was to characterize volatile compounds and determine the volatile marker in raw beef, rat, wild boar meat, and their mixtures using SPME/GC-MS. The chemometrics of principal component analysis (PCA) and orthogonal projection to latent structure-discriminant analysis (OPLS-DA) classified raw beef, rat, wild boar, and their mixture. Correlation coefficients and VIP values were used to determine the volatile marker compounds for each meat in the OPLS-DA classes. The OPLS-DA results that the most robust marker in the beef class was dimethylfulvene, benzyl alcohol in the rat class, and 1,3,5-cycloheptatriene in the wild boar class. Furthermore, the most robust marker in the mixture of beef and rat class was benzaldehyde, 3-ethyl-, while 2,6-dimethyldecane was dominant in the mixture of beef and wild boar class. However, further study using larger number of samples which include commercial meat is required to confirm these results.
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spelling oai:generic.eprints.org:206452022-12-06T09:20:41Z http://journalarticle.ukm.my/20645/ Profiling of volatile compounds in beef, rat, and wild boar meat using SPME-GC/ MS Lia Amalia, Kusnandar, Feri Nancy Dewi Yuliana, Purwantiningsih Sugita, The high beef price triggers adulteration of beef and other non-halal animal meat, such as wild boar and rats. An appropriate and effective analytical method is needed to differentiate halal and non-halal animal meat. The SPME/ GC-MS method could authenticate meat based on specific volatile compounds in each meat. The objective of this study was to characterize volatile compounds and determine the volatile marker in raw beef, rat, wild boar meat, and their mixtures using SPME/GC-MS. The chemometrics of principal component analysis (PCA) and orthogonal projection to latent structure-discriminant analysis (OPLS-DA) classified raw beef, rat, wild boar, and their mixture. Correlation coefficients and VIP values were used to determine the volatile marker compounds for each meat in the OPLS-DA classes. The OPLS-DA results that the most robust marker in the beef class was dimethylfulvene, benzyl alcohol in the rat class, and 1,3,5-cycloheptatriene in the wild boar class. Furthermore, the most robust marker in the mixture of beef and rat class was benzaldehyde, 3-ethyl-, while 2,6-dimethyldecane was dominant in the mixture of beef and wild boar class. However, further study using larger number of samples which include commercial meat is required to confirm these results. Penerbit Universiti Kebangsaan Malaysia 2022-09 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/20645/1/13.pdf Lia Amalia, and Kusnandar, Feri and Nancy Dewi Yuliana, and Purwantiningsih Sugita, (2022) Profiling of volatile compounds in beef, rat, and wild boar meat using SPME-GC/ MS. Sains Malaysiana, 51 (9). pp. 2897-2911. ISSN 0126-6039 https://www.ukm.my/jsm/malay_journals/jilid51bil9_2022/KandunganJilid51Bil9_2022.html
spellingShingle Lia Amalia,
Kusnandar, Feri
Nancy Dewi Yuliana,
Purwantiningsih Sugita,
Profiling of volatile compounds in beef, rat, and wild boar meat using SPME-GC/ MS
title Profiling of volatile compounds in beef, rat, and wild boar meat using SPME-GC/ MS
title_full Profiling of volatile compounds in beef, rat, and wild boar meat using SPME-GC/ MS
title_fullStr Profiling of volatile compounds in beef, rat, and wild boar meat using SPME-GC/ MS
title_full_unstemmed Profiling of volatile compounds in beef, rat, and wild boar meat using SPME-GC/ MS
title_short Profiling of volatile compounds in beef, rat, and wild boar meat using SPME-GC/ MS
title_sort profiling of volatile compounds in beef, rat, and wild boar meat using spme-gc/ ms
url http://journalarticle.ukm.my/20645/
http://journalarticle.ukm.my/20645/
http://journalarticle.ukm.my/20645/1/13.pdf