Preparation and characterization of impregnated magnetic particles on oil palm frond activated carbon for metal ions removal

The magnetic adsorbents i.e. oil palm frond-magnetic particles (OPF-MP) and oil palm frond activated carbon-magnetic particles (OPFAC-MP) have been prepared by impregnation of iron oxide via co-precipitation method. The magnetic adsorbents and their parent materials were characterized using Fourier...

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Main Authors: Muzakkir Mohammad Zainol, Nor Aishah Saidina Amin, Mohd Asmadi
Format: Article
Language:English
Published: Penerbit Universiti Kebangsaan Malaysia 2017
Online Access:http://journalarticle.ukm.my/11067/
http://journalarticle.ukm.my/11067/1/12%20Muzakkir%20Mohammad%20Zainol.pdf
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author Muzakkir Mohammad Zainol,
Nor Aishah Saidina Amin,
Mohd Asmadi,
author_facet Muzakkir Mohammad Zainol,
Nor Aishah Saidina Amin,
Mohd Asmadi,
author_sort Muzakkir Mohammad Zainol,
building UKM Institutional Repository
collection Online Access
description The magnetic adsorbents i.e. oil palm frond-magnetic particles (OPF-MP) and oil palm frond activated carbon-magnetic particles (OPFAC-MP) have been prepared by impregnation of iron oxide via co-precipitation method. The magnetic adsorbents and their parent materials were characterized using Fourier transform infrared (FTIR), thermogravimetric analysis (TGA), field emission scanning electron microscopy (FESEM), Brunauer Emmett Teller (BET), Barrett, Joyner & Halenda (BJH) and t-plot method, x-ray diffraction (XRD) and also using vibrating sample magnetometry (VSM) to study their properties and surface chemistry. The activated carbon magnetic adsorbent confers high surface area of 700 m2/g with amorphous structure and magnetic properties of 2.76 emu/g. The OPF-MP and OPFAC-MP were then applied in adsorption study for ions removal of Pb(II), Zn(II) and Cu(II). OPFAC-MP has shown high removal efficiency of 100 % with adsorption capacity up to 15 mg/g of Pb(II), Zn(II) and Cu(II) ions compared to OPF-MP. In addition, the magnetic adsorbents were also compared with their parent materials to observe the effect of magnetic particles. Accordingly, the impregnation of magnetic particles enhances the metal ions adsorption comparing to their parent materials.
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spelling oai:generic.eprints.org:110672017-12-12T05:01:10Z http://journalarticle.ukm.my/11067/ Preparation and characterization of impregnated magnetic particles on oil palm frond activated carbon for metal ions removal Muzakkir Mohammad Zainol, Nor Aishah Saidina Amin, Mohd Asmadi, The magnetic adsorbents i.e. oil palm frond-magnetic particles (OPF-MP) and oil palm frond activated carbon-magnetic particles (OPFAC-MP) have been prepared by impregnation of iron oxide via co-precipitation method. The magnetic adsorbents and their parent materials were characterized using Fourier transform infrared (FTIR), thermogravimetric analysis (TGA), field emission scanning electron microscopy (FESEM), Brunauer Emmett Teller (BET), Barrett, Joyner & Halenda (BJH) and t-plot method, x-ray diffraction (XRD) and also using vibrating sample magnetometry (VSM) to study their properties and surface chemistry. The activated carbon magnetic adsorbent confers high surface area of 700 m2/g with amorphous structure and magnetic properties of 2.76 emu/g. The OPF-MP and OPFAC-MP were then applied in adsorption study for ions removal of Pb(II), Zn(II) and Cu(II). OPFAC-MP has shown high removal efficiency of 100 % with adsorption capacity up to 15 mg/g of Pb(II), Zn(II) and Cu(II) ions compared to OPF-MP. In addition, the magnetic adsorbents were also compared with their parent materials to observe the effect of magnetic particles. Accordingly, the impregnation of magnetic particles enhances the metal ions adsorption comparing to their parent materials. Penerbit Universiti Kebangsaan Malaysia 2017-05 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/11067/1/12%20Muzakkir%20Mohammad%20Zainol.pdf Muzakkir Mohammad Zainol, and Nor Aishah Saidina Amin, and Mohd Asmadi, (2017) Preparation and characterization of impregnated magnetic particles on oil palm frond activated carbon for metal ions removal. Sains Malaysiana, 46 (5). pp. 773-782. ISSN 0126-6039 http://www.ukm.my/jsm/english_journals/vol46num5_2017/contentsVol46num5_2017.html
spellingShingle Muzakkir Mohammad Zainol,
Nor Aishah Saidina Amin,
Mohd Asmadi,
Preparation and characterization of impregnated magnetic particles on oil palm frond activated carbon for metal ions removal
title Preparation and characterization of impregnated magnetic particles on oil palm frond activated carbon for metal ions removal
title_full Preparation and characterization of impregnated magnetic particles on oil palm frond activated carbon for metal ions removal
title_fullStr Preparation and characterization of impregnated magnetic particles on oil palm frond activated carbon for metal ions removal
title_full_unstemmed Preparation and characterization of impregnated magnetic particles on oil palm frond activated carbon for metal ions removal
title_short Preparation and characterization of impregnated magnetic particles on oil palm frond activated carbon for metal ions removal
title_sort preparation and characterization of impregnated magnetic particles on oil palm frond activated carbon for metal ions removal
url http://journalarticle.ukm.my/11067/
http://journalarticle.ukm.my/11067/
http://journalarticle.ukm.my/11067/1/12%20Muzakkir%20Mohammad%20Zainol.pdf