Preparation and characterization of Fe3O4/regenerated cellulose membrane

In this study, magnetic cellulose membranes (MCM) have been prepared by using cotton linter as cellulose source and NaOH/urea as cellulose solvent at different magnetite content. Cellulose was dissolved in pre-cooled NaOH/urea solvent at -13°C to form cellulose solution. The cellulose solution then...

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Main Authors: Hatika Kaco, Khairunnisa Waznah Baharin, Sarani Zakaria, Chin, Hua Chia, Mohd Shaiful Sajab, Sharifah Nabihah Syed Jaafar, Sin, Yee Gan
Format: Article
Language:English
Published: Penerbit Universiti Kebangsaan Malaysia 2017
Online Access:http://journalarticle.ukm.my/11040/
http://journalarticle.ukm.my/11040/1/15%20Hatika%20Kaco.pdf
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author Hatika Kaco,
Khairunnisa Waznah Baharin,
Sarani Zakaria,
Chin, Hua Chia
Mohd Shaiful Sajab,
Sharifah Nabihah Syed Jaafar,
Sin, Yee Gan
author_facet Hatika Kaco,
Khairunnisa Waznah Baharin,
Sarani Zakaria,
Chin, Hua Chia
Mohd Shaiful Sajab,
Sharifah Nabihah Syed Jaafar,
Sin, Yee Gan
author_sort Hatika Kaco,
building UKM Institutional Repository
collection Online Access
description In this study, magnetic cellulose membranes (MCM) have been prepared by using cotton linter as cellulose source and NaOH/urea as cellulose solvent at different magnetite content. Cellulose was dissolved in pre-cooled NaOH/urea solvent at -13°C to form cellulose solution. The cellulose solution then was mix with magnetite (Fe3O4) nanoparticles synthesized via co-precipitation method of Fe2+ and Fe3+ in the presence of sodium hydroxide (NaOH) to form MCM. The MCMs formed at different percentage of Fe3O4 i.e., 10, 20 and 30%. Analysis from vibrating sample magnetometer (VSM) shows that the saturation magnetization of the MCM increase as the percentages of Fe3O4 nanoparticles increased. However, the addition of Fe3O4 nanoparticles in the regenerated cellulose membrane has decreased the crystallinity index of MCM. The surface morphology of the MCM showed that the Fe3O4 nanoparticles were dispersed in the pore of the membrane. Tensile test showed decreasing in the tensile strength of the cellulose membrane with the addition of Fe3O4 nanoparticle.
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spelling oai:generic.eprints.org:110402017-11-27T15:57:56Z http://journalarticle.ukm.my/11040/ Preparation and characterization of Fe3O4/regenerated cellulose membrane Hatika Kaco, Khairunnisa Waznah Baharin, Sarani Zakaria, Chin, Hua Chia Mohd Shaiful Sajab, Sharifah Nabihah Syed Jaafar, Sin, Yee Gan In this study, magnetic cellulose membranes (MCM) have been prepared by using cotton linter as cellulose source and NaOH/urea as cellulose solvent at different magnetite content. Cellulose was dissolved in pre-cooled NaOH/urea solvent at -13°C to form cellulose solution. The cellulose solution then was mix with magnetite (Fe3O4) nanoparticles synthesized via co-precipitation method of Fe2+ and Fe3+ in the presence of sodium hydroxide (NaOH) to form MCM. The MCMs formed at different percentage of Fe3O4 i.e., 10, 20 and 30%. Analysis from vibrating sample magnetometer (VSM) shows that the saturation magnetization of the MCM increase as the percentages of Fe3O4 nanoparticles increased. However, the addition of Fe3O4 nanoparticles in the regenerated cellulose membrane has decreased the crystallinity index of MCM. The surface morphology of the MCM showed that the Fe3O4 nanoparticles were dispersed in the pore of the membrane. Tensile test showed decreasing in the tensile strength of the cellulose membrane with the addition of Fe3O4 nanoparticle. Penerbit Universiti Kebangsaan Malaysia 2017-04 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/11040/1/15%20Hatika%20Kaco.pdf Hatika Kaco, and Khairunnisa Waznah Baharin, and Sarani Zakaria, and Chin, Hua Chia and Mohd Shaiful Sajab, and Sharifah Nabihah Syed Jaafar, and Sin, Yee Gan (2017) Preparation and characterization of Fe3O4/regenerated cellulose membrane. Sains Malaysiana, 46 (4). pp. 623-628. ISSN 0126-6039 http://www.ukm.my/jsm/english_journals/vol46num4_2017/contentsVol46num4_2017.html
spellingShingle Hatika Kaco,
Khairunnisa Waznah Baharin,
Sarani Zakaria,
Chin, Hua Chia
Mohd Shaiful Sajab,
Sharifah Nabihah Syed Jaafar,
Sin, Yee Gan
Preparation and characterization of Fe3O4/regenerated cellulose membrane
title Preparation and characterization of Fe3O4/regenerated cellulose membrane
title_full Preparation and characterization of Fe3O4/regenerated cellulose membrane
title_fullStr Preparation and characterization of Fe3O4/regenerated cellulose membrane
title_full_unstemmed Preparation and characterization of Fe3O4/regenerated cellulose membrane
title_short Preparation and characterization of Fe3O4/regenerated cellulose membrane
title_sort preparation and characterization of fe3o4/regenerated cellulose membrane
url http://journalarticle.ukm.my/11040/
http://journalarticle.ukm.my/11040/
http://journalarticle.ukm.my/11040/1/15%20Hatika%20Kaco.pdf