Design, Synthesis, and Evaluation of New P2Y2 Receptor Antagonists and Fluorescent Ligands

The P2Y2 receptor (P2Y2R) is an exciting therapeutic target for numerous diseases including atherosclerosis, idiopathic pulmonary fibrosis, and cancer. Despite this, there are a limited number of receptor antagonists available, none of which are clinically viable. The highest affinity P2Y2R antagoni...

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Main Author: Knight, Rebecca
Format: Thesis (University of Nottingham only)
Language:English
Published: 2025
Subjects:
Online Access:https://eprints.nottingham.ac.uk/80213/
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author Knight, Rebecca
author_facet Knight, Rebecca
author_sort Knight, Rebecca
building Nottingham Research Data Repository
collection Online Access
description The P2Y2 receptor (P2Y2R) is an exciting therapeutic target for numerous diseases including atherosclerosis, idiopathic pulmonary fibrosis, and cancer. Despite this, there are a limited number of receptor antagonists available, none of which are clinically viable. The highest affinity P2Y2R antagonists detailed are AR-C118925 and its thiazole-based analogues, for which physiochemical properties remain a barrier for future drug development. The work presented in this project details the design, synthesis, and evaluation of new chemotype P2Y2R antagonists and fluorescent ligands, which provide scope for future drug development projects to depart from ARC118925 and its analogues. The new chemotype P2Y2R antagonists and fluorescent ligands retained micromolar affinity for the receptor, despite the absence of the tricyclic ring system and thiouracil, with the presence of a terminal acidic group on the thiazole substituent being crucial for P2Y2R activity. The fluorescent ligand 4.09 (pKd = 5.24 ± 0.04, n = 5), which appears to bind to the P2Y2R on the intracellular side of the plasma membrane, offers exciting opportunities to target this difficult to drug receptor with new modalities that could overcome existing limitations in developing P2Y2R antagonists.
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spelling nottingham-802132025-07-31T04:40:08Z https://eprints.nottingham.ac.uk/80213/ Design, Synthesis, and Evaluation of New P2Y2 Receptor Antagonists and Fluorescent Ligands Knight, Rebecca The P2Y2 receptor (P2Y2R) is an exciting therapeutic target for numerous diseases including atherosclerosis, idiopathic pulmonary fibrosis, and cancer. Despite this, there are a limited number of receptor antagonists available, none of which are clinically viable. The highest affinity P2Y2R antagonists detailed are AR-C118925 and its thiazole-based analogues, for which physiochemical properties remain a barrier for future drug development. The work presented in this project details the design, synthesis, and evaluation of new chemotype P2Y2R antagonists and fluorescent ligands, which provide scope for future drug development projects to depart from ARC118925 and its analogues. The new chemotype P2Y2R antagonists and fluorescent ligands retained micromolar affinity for the receptor, despite the absence of the tricyclic ring system and thiouracil, with the presence of a terminal acidic group on the thiazole substituent being crucial for P2Y2R activity. The fluorescent ligand 4.09 (pKd = 5.24 ± 0.04, n = 5), which appears to bind to the P2Y2R on the intracellular side of the plasma membrane, offers exciting opportunities to target this difficult to drug receptor with new modalities that could overcome existing limitations in developing P2Y2R antagonists. 2025-07-31 Thesis (University of Nottingham only) NonPeerReviewed application/pdf en cc_by https://eprints.nottingham.ac.uk/80213/1/Knight%2C%20Rebecca%2C%2020307351%2C%20corrections.pdf Knight, Rebecca (2025) Design, Synthesis, and Evaluation of New P2Y2 Receptor Antagonists and Fluorescent Ligands. PhD thesis, University of Nottingham. antagonists fluorescent ligands P2Y2R receptor antagonists drug development
spellingShingle antagonists
fluorescent ligands
P2Y2R
receptor antagonists
drug development
Knight, Rebecca
Design, Synthesis, and Evaluation of New P2Y2 Receptor Antagonists and Fluorescent Ligands
title Design, Synthesis, and Evaluation of New P2Y2 Receptor Antagonists and Fluorescent Ligands
title_full Design, Synthesis, and Evaluation of New P2Y2 Receptor Antagonists and Fluorescent Ligands
title_fullStr Design, Synthesis, and Evaluation of New P2Y2 Receptor Antagonists and Fluorescent Ligands
title_full_unstemmed Design, Synthesis, and Evaluation of New P2Y2 Receptor Antagonists and Fluorescent Ligands
title_short Design, Synthesis, and Evaluation of New P2Y2 Receptor Antagonists and Fluorescent Ligands
title_sort design, synthesis, and evaluation of new p2y2 receptor antagonists and fluorescent ligands
topic antagonists
fluorescent ligands
P2Y2R
receptor antagonists
drug development
url https://eprints.nottingham.ac.uk/80213/