Novel magnetic micro-structured porous materials for biomedical applications

Novel, porous and dense, ceramic (Fe3O4 & Ca2Fe2O5) and glass-ceramic (phosphate-based glass matrix with magnetic domains) magnetic microspheres have been manufactured for the first time via a rapid, single-stage, flame spheroidisation process. Morphological, structural, and compositional invest...

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Main Author: Molinar Diaz, Jesus
Format: Thesis (University of Nottingham only)
Language:English
Published: 2023
Subjects:
Online Access:https://eprints.nottingham.ac.uk/73616/
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author Molinar Diaz, Jesus
author_facet Molinar Diaz, Jesus
author_sort Molinar Diaz, Jesus
building Nottingham Research Data Repository
collection Online Access
description Novel, porous and dense, ceramic (Fe3O4 & Ca2Fe2O5) and glass-ceramic (phosphate-based glass matrix with magnetic domains) magnetic microspheres have been manufactured for the first time via a rapid, single-stage, flame spheroidisation process. Morphological, structural, and compositional investigations provide evidence into the microsphere formation mechanisms, as a function of Fe3O4 precursor particle size, precursor-to-porogen mass ratio, and gas flow settings. Optimised conditions for the flame spheroidisation processing of these ceramic and glass-ceramic, porous and dense magnetic microspheres are identified. The magnetic properties of the materials provided for controlled induction heating to a constant level (40 – 45 °C), making these microspheres highly appropriate for localised magnetic hyperthermia applications. Complementary, cytocompatibility investigations confirmed the suitability of porous microspheres for biomedical applications. It is suggested that the flame-spheroidised materials developed opens up new opportunities for the rapid manufacture of innovative synergistic biomaterials, towards magnetic hyperthermia applications.
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spelling nottingham-736162023-07-21T04:40:22Z https://eprints.nottingham.ac.uk/73616/ Novel magnetic micro-structured porous materials for biomedical applications Molinar Diaz, Jesus Novel, porous and dense, ceramic (Fe3O4 & Ca2Fe2O5) and glass-ceramic (phosphate-based glass matrix with magnetic domains) magnetic microspheres have been manufactured for the first time via a rapid, single-stage, flame spheroidisation process. Morphological, structural, and compositional investigations provide evidence into the microsphere formation mechanisms, as a function of Fe3O4 precursor particle size, precursor-to-porogen mass ratio, and gas flow settings. Optimised conditions for the flame spheroidisation processing of these ceramic and glass-ceramic, porous and dense magnetic microspheres are identified. The magnetic properties of the materials provided for controlled induction heating to a constant level (40 – 45 °C), making these microspheres highly appropriate for localised magnetic hyperthermia applications. Complementary, cytocompatibility investigations confirmed the suitability of porous microspheres for biomedical applications. It is suggested that the flame-spheroidised materials developed opens up new opportunities for the rapid manufacture of innovative synergistic biomaterials, towards magnetic hyperthermia applications. 2023-07-21 Thesis (University of Nottingham only) NonPeerReviewed application/pdf en cc_by https://eprints.nottingham.ac.uk/73616/1/PhD%20Thesis_Jesus%20Molinar%20Diaz_final.pdf Molinar Diaz, Jesus (2023) Novel magnetic micro-structured porous materials for biomedical applications. PhD thesis, University of Nottingham. Magnetic nanoparticle hyperthermia; Microspheres (Pharmacy); Porous materials; Biomedical materials
spellingShingle Magnetic nanoparticle hyperthermia; Microspheres (Pharmacy); Porous materials; Biomedical materials
Molinar Diaz, Jesus
Novel magnetic micro-structured porous materials for biomedical applications
title Novel magnetic micro-structured porous materials for biomedical applications
title_full Novel magnetic micro-structured porous materials for biomedical applications
title_fullStr Novel magnetic micro-structured porous materials for biomedical applications
title_full_unstemmed Novel magnetic micro-structured porous materials for biomedical applications
title_short Novel magnetic micro-structured porous materials for biomedical applications
title_sort novel magnetic micro-structured porous materials for biomedical applications
topic Magnetic nanoparticle hyperthermia; Microspheres (Pharmacy); Porous materials; Biomedical materials
url https://eprints.nottingham.ac.uk/73616/