Oxygen-rich microporous carbons with exceptional hydrogen storage capacity

Porous carbons have been extensively investigated for hydrogen storage but, to date, appear to have an upper limit to their storage capacity. Here, in an effort to circumvent this upper limit, we explore the potential of oxygen-rich activated carbons. We describe cellulose acetatederived carbons tha...

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Main Authors: Blankenship, Troy Scott, Balahmar, Norah, Mokaya, Robert
Format: Article
Published: Nature Publishing Group 2017
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Online Access:https://eprints.nottingham.ac.uk/47253/
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author Blankenship, Troy Scott
Balahmar, Norah
Mokaya, Robert
author_facet Blankenship, Troy Scott
Balahmar, Norah
Mokaya, Robert
author_sort Blankenship, Troy Scott
building Nottingham Research Data Repository
collection Online Access
description Porous carbons have been extensively investigated for hydrogen storage but, to date, appear to have an upper limit to their storage capacity. Here, in an effort to circumvent this upper limit, we explore the potential of oxygen-rich activated carbons. We describe cellulose acetatederived carbons that combine high surface area (3800 m2 g-1) and pore volume (1.8 cm3 g-1) that arise almost entirely (> 90%) from micropores, with an oxygen-rich nature. The carbons exhibit enhanced gravimetric hydrogen uptake (8.1 wt% total, and 7.0 wt% excess) at -196 ºC and 20 bar, rising to a total uptake of 8.9 wt% at 30 bar, and exceptional volumetric uptake of 44 g l-1 at 20 bar, and 48 g l-1 at 30 bar. At room temperature they store up to 0.8 wt% (excess) and 1.2 wt% (total) hydrogen at only 30 bar, and their isosteric heat of hydrogen adsorption is above 10 kJ mol-1.
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spelling nottingham-472532020-05-04T19:17:40Z https://eprints.nottingham.ac.uk/47253/ Oxygen-rich microporous carbons with exceptional hydrogen storage capacity Blankenship, Troy Scott Balahmar, Norah Mokaya, Robert Porous carbons have been extensively investigated for hydrogen storage but, to date, appear to have an upper limit to their storage capacity. Here, in an effort to circumvent this upper limit, we explore the potential of oxygen-rich activated carbons. We describe cellulose acetatederived carbons that combine high surface area (3800 m2 g-1) and pore volume (1.8 cm3 g-1) that arise almost entirely (> 90%) from micropores, with an oxygen-rich nature. The carbons exhibit enhanced gravimetric hydrogen uptake (8.1 wt% total, and 7.0 wt% excess) at -196 ºC and 20 bar, rising to a total uptake of 8.9 wt% at 30 bar, and exceptional volumetric uptake of 44 g l-1 at 20 bar, and 48 g l-1 at 30 bar. At room temperature they store up to 0.8 wt% (excess) and 1.2 wt% (total) hydrogen at only 30 bar, and their isosteric heat of hydrogen adsorption is above 10 kJ mol-1. Nature Publishing Group 2017-11-16 Article PeerReviewed Blankenship, Troy Scott, Balahmar, Norah and Mokaya, Robert (2017) Oxygen-rich microporous carbons with exceptional hydrogen storage capacity. Nature Communications, 8 . 1545/1-1545/12. ISSN 2041-1723 hydrogen storage materials; materials chemistry; porous materials https://www.nature.com/articles/s41467-017-01633-x doi:10.1038/s41467-017-01633-x doi:10.1038/s41467-017-01633-x
spellingShingle hydrogen storage materials; materials chemistry; porous materials
Blankenship, Troy Scott
Balahmar, Norah
Mokaya, Robert
Oxygen-rich microporous carbons with exceptional hydrogen storage capacity
title Oxygen-rich microporous carbons with exceptional hydrogen storage capacity
title_full Oxygen-rich microporous carbons with exceptional hydrogen storage capacity
title_fullStr Oxygen-rich microporous carbons with exceptional hydrogen storage capacity
title_full_unstemmed Oxygen-rich microporous carbons with exceptional hydrogen storage capacity
title_short Oxygen-rich microporous carbons with exceptional hydrogen storage capacity
title_sort oxygen-rich microporous carbons with exceptional hydrogen storage capacity
topic hydrogen storage materials; materials chemistry; porous materials
url https://eprints.nottingham.ac.uk/47253/
https://eprints.nottingham.ac.uk/47253/
https://eprints.nottingham.ac.uk/47253/