Nickel(II) metal-organic frameworks with N,N’-di(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide ligands: influence of secondary building unit geometry on dimensionality and framework dimensions

When Ni(NO3)2∙6H2O and N,N’-di(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide (DPNDI) are reacted, a one-dimensional coordination polymer (1) is formed. However, reaction with either terephthalic acid (2) or 2,6-naphthalenedicarboxylic acid (3) affords two-dimensional, pillared metal-organic fram...

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Main Authors: Pfeiffer, Constance R., Biggins, Naomi H., Lewis, William, Champness, Neil R.
Format: Article
Published: Royal Society of Chemistry 2017
Subjects:
Online Access:https://eprints.nottingham.ac.uk/46944/
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author Pfeiffer, Constance R.
Biggins, Naomi H.
Lewis, William
Champness, Neil R.
author_facet Pfeiffer, Constance R.
Biggins, Naomi H.
Lewis, William
Champness, Neil R.
author_sort Pfeiffer, Constance R.
building Nottingham Research Data Repository
collection Online Access
description When Ni(NO3)2∙6H2O and N,N’-di(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide (DPNDI) are reacted, a one-dimensional coordination polymer (1) is formed. However, reaction with either terephthalic acid (2) or 2,6-naphthalenedicarboxylic acid (3) affords two-dimensional, pillared metal-organic frameworks. 2 and 3 containing rectangular voids of different dimensions which are dictated by the carboxylate ligand and the arrangement of the [M(k2-O2NO)]2(μ2-O2CR)2] secondary building unit (SBU) that forms the nodes of the framework. The role of SBU geometry, intermolecular face-to-face π–π and lone pair–π interactions involving the DPNDI ligands are discussed.
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spelling nottingham-469442020-05-04T19:04:36Z https://eprints.nottingham.ac.uk/46944/ Nickel(II) metal-organic frameworks with N,N’-di(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide ligands: influence of secondary building unit geometry on dimensionality and framework dimensions Pfeiffer, Constance R. Biggins, Naomi H. Lewis, William Champness, Neil R. When Ni(NO3)2∙6H2O and N,N’-di(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide (DPNDI) are reacted, a one-dimensional coordination polymer (1) is formed. However, reaction with either terephthalic acid (2) or 2,6-naphthalenedicarboxylic acid (3) affords two-dimensional, pillared metal-organic frameworks. 2 and 3 containing rectangular voids of different dimensions which are dictated by the carboxylate ligand and the arrangement of the [M(k2-O2NO)]2(μ2-O2CR)2] secondary building unit (SBU) that forms the nodes of the framework. The role of SBU geometry, intermolecular face-to-face π–π and lone pair–π interactions involving the DPNDI ligands are discussed. Royal Society of Chemistry 2017-09-05 Article PeerReviewed Pfeiffer, Constance R., Biggins, Naomi H., Lewis, William and Champness, Neil R. (2017) Nickel(II) metal-organic frameworks with N,N’-di(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide ligands: influence of secondary building unit geometry on dimensionality and framework dimensions. CrystEngComm, 19 . pp. 5559-5564. ISSN 1466-8033 Metal-organic frameworks N N’-di(4-pyridyl)-1 4 5 8-naphthalenetetracarboxydiimide nickel (II) frameworks pillared frameworks http://pubs.rsc.org/en/content/articlelanding/2017/ce/c7ce00956a#!divAbstract doi:10.1039/C7CE00956A doi:10.1039/C7CE00956A
spellingShingle Metal-organic frameworks
N
N’-di(4-pyridyl)-1
4
5
8-naphthalenetetracarboxydiimide
nickel (II) frameworks
pillared frameworks
Pfeiffer, Constance R.
Biggins, Naomi H.
Lewis, William
Champness, Neil R.
Nickel(II) metal-organic frameworks with N,N’-di(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide ligands: influence of secondary building unit geometry on dimensionality and framework dimensions
title Nickel(II) metal-organic frameworks with N,N’-di(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide ligands: influence of secondary building unit geometry on dimensionality and framework dimensions
title_full Nickel(II) metal-organic frameworks with N,N’-di(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide ligands: influence of secondary building unit geometry on dimensionality and framework dimensions
title_fullStr Nickel(II) metal-organic frameworks with N,N’-di(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide ligands: influence of secondary building unit geometry on dimensionality and framework dimensions
title_full_unstemmed Nickel(II) metal-organic frameworks with N,N’-di(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide ligands: influence of secondary building unit geometry on dimensionality and framework dimensions
title_short Nickel(II) metal-organic frameworks with N,N’-di(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide ligands: influence of secondary building unit geometry on dimensionality and framework dimensions
title_sort nickel(ii) metal-organic frameworks with n,n’-di(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide ligands: influence of secondary building unit geometry on dimensionality and framework dimensions
topic Metal-organic frameworks
N
N’-di(4-pyridyl)-1
4
5
8-naphthalenetetracarboxydiimide
nickel (II) frameworks
pillared frameworks
url https://eprints.nottingham.ac.uk/46944/
https://eprints.nottingham.ac.uk/46944/
https://eprints.nottingham.ac.uk/46944/