An antiferromagnetically coupled heterometal Cu6Fe wheel

A heterometal Cu6Fe wheel molecule, [CuII6FeIII(HL)6- (OH)2(OCH3)4](NO3)3¢6H2O (1¢6H2O) (H2L = 1-(2-pyridine) 3-(2-pyrrole)acetylacetone) was synthesized by the one-pot reaction of H2L with copper and iron sources. X-ray structural analysis reveals that the heptanuclear wheel cluster consists of a c...

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Main Authors: Saiki, Ryo, Yoshida, Norifumi, Hoshino, Norihisa, Newton, Graham N., Shiga, Takuya, Oshio, Hiroki
Format: Article
Published: Chemical Society of Japan 2017
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Online Access:https://eprints.nottingham.ac.uk/44251/
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author Saiki, Ryo
Yoshida, Norifumi
Hoshino, Norihisa
Newton, Graham N.
Shiga, Takuya
Oshio, Hiroki
author_facet Saiki, Ryo
Yoshida, Norifumi
Hoshino, Norihisa
Newton, Graham N.
Shiga, Takuya
Oshio, Hiroki
author_sort Saiki, Ryo
building Nottingham Research Data Repository
collection Online Access
description A heterometal Cu6Fe wheel molecule, [CuII6FeIII(HL)6- (OH)2(OCH3)4](NO3)3¢6H2O (1¢6H2O) (H2L = 1-(2-pyridine) 3-(2-pyrrole)acetylacetone) was synthesized by the one-pot reaction of H2L with copper and iron sources. X-ray structural analysis reveals that the heptanuclear wheel cluster consists of a central Fe(III) ion surrounded by six Cu(II) ions, linked through methoxo- and hydroxo-bridges. Cryomagnetic studies indicate intramolecular antiferromagnetic interactions were operative.
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institution University of Nottingham Malaysia Campus
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publishDate 2017
publisher Chemical Society of Japan
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spelling nottingham-442512020-05-04T18:58:44Z https://eprints.nottingham.ac.uk/44251/ An antiferromagnetically coupled heterometal Cu6Fe wheel Saiki, Ryo Yoshida, Norifumi Hoshino, Norihisa Newton, Graham N. Shiga, Takuya Oshio, Hiroki A heterometal Cu6Fe wheel molecule, [CuII6FeIII(HL)6- (OH)2(OCH3)4](NO3)3¢6H2O (1¢6H2O) (H2L = 1-(2-pyridine) 3-(2-pyrrole)acetylacetone) was synthesized by the one-pot reaction of H2L with copper and iron sources. X-ray structural analysis reveals that the heptanuclear wheel cluster consists of a central Fe(III) ion surrounded by six Cu(II) ions, linked through methoxo- and hydroxo-bridges. Cryomagnetic studies indicate intramolecular antiferromagnetic interactions were operative. Chemical Society of Japan 2017-08-01 Article PeerReviewed Saiki, Ryo, Yoshida, Norifumi, Hoshino, Norihisa, Newton, Graham N., Shiga, Takuya and Oshio, Hiroki (2017) An antiferromagnetically coupled heterometal Cu6Fe wheel. Chemistry Letters, 46 (8). pp. 1197-1199. ISSN 0366-7022 Heterometal polynuclear complex ; Wheel complex ; Antiferromagnetic interaction http://www.journal.csj.jp/doi/abs/10.1246/cl.170365?af=R doi:10.1246/cl.170365 doi:10.1246/cl.170365
spellingShingle Heterometal polynuclear complex ; Wheel complex ; Antiferromagnetic interaction
Saiki, Ryo
Yoshida, Norifumi
Hoshino, Norihisa
Newton, Graham N.
Shiga, Takuya
Oshio, Hiroki
An antiferromagnetically coupled heterometal Cu6Fe wheel
title An antiferromagnetically coupled heterometal Cu6Fe wheel
title_full An antiferromagnetically coupled heterometal Cu6Fe wheel
title_fullStr An antiferromagnetically coupled heterometal Cu6Fe wheel
title_full_unstemmed An antiferromagnetically coupled heterometal Cu6Fe wheel
title_short An antiferromagnetically coupled heterometal Cu6Fe wheel
title_sort antiferromagnetically coupled heterometal cu6fe wheel
topic Heterometal polynuclear complex ; Wheel complex ; Antiferromagnetic interaction
url https://eprints.nottingham.ac.uk/44251/
https://eprints.nottingham.ac.uk/44251/
https://eprints.nottingham.ac.uk/44251/