On hydrodynamic methods for the analysis of the sizes and shapes of polysaccharides in dilute solution: a short review

Background: Polysaccharides and their derivatives are increasingly being used by the food, cosmetic and pharmaceutical industries: physical properties like size and conformation are important contributors to their performance. Discussion: Here the use of hydrodynamic tools such as sedimentation vel...

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Main Authors: Morris, Gordon A., Adams, Gary G., Harding, Stephen E.
Format: Article
Published: Elsevier 2014
Subjects:
Online Access:https://eprints.nottingham.ac.uk/42756/
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author Morris, Gordon A.
Adams, Gary G.
Harding, Stephen E.
author_facet Morris, Gordon A.
Adams, Gary G.
Harding, Stephen E.
author_sort Morris, Gordon A.
building Nottingham Research Data Repository
collection Online Access
description Background: Polysaccharides and their derivatives are increasingly being used by the food, cosmetic and pharmaceutical industries: physical properties like size and conformation are important contributors to their performance. Discussion: Here the use of hydrodynamic tools such as sedimentation velocity, sedimentation equilibrium, size exclusion chromatography e multi-angle light scattering (SEC-MALS), and viscometry are considered highlighting some recent developments in methodology and the application of these to help better understand polysaccharide structureefunction relationships. Conclusions: The size and shape of polysaccharides in solution can be estimated in a variety of ways. Molar masses and heterogeneities can be estimated to a good precision by sedimentation velocity, sedimentation equilibrium and SEC-MALS. An approximate idea of conformation and flexibility can be obtained from power-law coefficients and the Wales van Holde parameter. More sophisticated estimates can be obtained by combining methods together to yield the persistence length.
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spelling nottingham-427562020-05-04T16:58:40Z https://eprints.nottingham.ac.uk/42756/ On hydrodynamic methods for the analysis of the sizes and shapes of polysaccharides in dilute solution: a short review Morris, Gordon A. Adams, Gary G. Harding, Stephen E. Background: Polysaccharides and their derivatives are increasingly being used by the food, cosmetic and pharmaceutical industries: physical properties like size and conformation are important contributors to their performance. Discussion: Here the use of hydrodynamic tools such as sedimentation velocity, sedimentation equilibrium, size exclusion chromatography e multi-angle light scattering (SEC-MALS), and viscometry are considered highlighting some recent developments in methodology and the application of these to help better understand polysaccharide structureefunction relationships. Conclusions: The size and shape of polysaccharides in solution can be estimated in a variety of ways. Molar masses and heterogeneities can be estimated to a good precision by sedimentation velocity, sedimentation equilibrium and SEC-MALS. An approximate idea of conformation and flexibility can be obtained from power-law coefficients and the Wales van Holde parameter. More sophisticated estimates can be obtained by combining methods together to yield the persistence length. Elsevier 2014-12-15 Article PeerReviewed Morris, Gordon A., Adams, Gary G. and Harding, Stephen E. (2014) On hydrodynamic methods for the analysis of the sizes and shapes of polysaccharides in dilute solution: a short review. Food Hydrocolloids, 42 . pp. 318-334. ISSN 0268-005X Polysaccharides ; Size ; Conformation ; Structure-function relationships http://www.sciencedirect.com/science/article/pii/S0268005X14001441 doi:10.1016/j.foodhyd.2014.04.014 doi:10.1016/j.foodhyd.2014.04.014
spellingShingle Polysaccharides ; Size ; Conformation ; Structure-function relationships
Morris, Gordon A.
Adams, Gary G.
Harding, Stephen E.
On hydrodynamic methods for the analysis of the sizes and shapes of polysaccharides in dilute solution: a short review
title On hydrodynamic methods for the analysis of the sizes and shapes of polysaccharides in dilute solution: a short review
title_full On hydrodynamic methods for the analysis of the sizes and shapes of polysaccharides in dilute solution: a short review
title_fullStr On hydrodynamic methods for the analysis of the sizes and shapes of polysaccharides in dilute solution: a short review
title_full_unstemmed On hydrodynamic methods for the analysis of the sizes and shapes of polysaccharides in dilute solution: a short review
title_short On hydrodynamic methods for the analysis of the sizes and shapes of polysaccharides in dilute solution: a short review
title_sort on hydrodynamic methods for the analysis of the sizes and shapes of polysaccharides in dilute solution: a short review
topic Polysaccharides ; Size ; Conformation ; Structure-function relationships
url https://eprints.nottingham.ac.uk/42756/
https://eprints.nottingham.ac.uk/42756/
https://eprints.nottingham.ac.uk/42756/