Epitaxial hetero-structure of CdSe/TiO2 nanotube arrays with PEDOT as hole transfer layer for photoelectrochemical hydrogen evolution

The photocatalytic decomposition of water is believed to be able to help mitigate the crisis of fossil fuel depletion. However, the photocatalytic hydrogen production remains challenge to obtain high and stable photoconversion efficiency. Here we report an epitaxial hetero-structure of CdSe/TiO2 nan...

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Main Authors: Chong, Baohe, Zhu, Wen, Hou, Xianghui
Format: Article
Published: Royal Society of Chemistry 2017
Online Access:https://eprints.nottingham.ac.uk/41019/
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author Chong, Baohe
Zhu, Wen
Hou, Xianghui
author_facet Chong, Baohe
Zhu, Wen
Hou, Xianghui
author_sort Chong, Baohe
building Nottingham Research Data Repository
collection Online Access
description The photocatalytic decomposition of water is believed to be able to help mitigate the crisis of fossil fuel depletion. However, the photocatalytic hydrogen production remains challenge to obtain high and stable photoconversion efficiency. Here we report an epitaxial hetero-structure of CdSe/TiO2 nanotube arrays as efficient photo-anodes via simple room-temperature, low-cost electrochemical deposition. With the help of the similar d spacing with TiO2, CdSe sensitization layer is epitaxially grown on the tube wall of the TiO2 nanotubes, resulting in an ideal coherent grain boundary and single crystal growth. The resultant photo-anode produces 30% more photocurrent than those samples without coherent grain boundary. Notably, the especial epitaxial hetero-structure is beneficial to decrease the recombination site and accelerate the separation of photogenerated electron-hole pairs. Furthermore, an ultrathin PEDOT surface layer was developed on the epitaxial hetero-structure of CdSe/TiO2 nano-tube arrays in which it functions as both a physical passivation barrier and a hole transfer layer. As a result, significantly enhanced photocurrent density and substantially better stability have been achieved. This methodology may be providing a new pathway of epitaxial growth for preparing the heterogeneous junction materials which have similar d spacing.
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spelling nottingham-410192020-05-04T18:33:52Z https://eprints.nottingham.ac.uk/41019/ Epitaxial hetero-structure of CdSe/TiO2 nanotube arrays with PEDOT as hole transfer layer for photoelectrochemical hydrogen evolution Chong, Baohe Zhu, Wen Hou, Xianghui The photocatalytic decomposition of water is believed to be able to help mitigate the crisis of fossil fuel depletion. However, the photocatalytic hydrogen production remains challenge to obtain high and stable photoconversion efficiency. Here we report an epitaxial hetero-structure of CdSe/TiO2 nanotube arrays as efficient photo-anodes via simple room-temperature, low-cost electrochemical deposition. With the help of the similar d spacing with TiO2, CdSe sensitization layer is epitaxially grown on the tube wall of the TiO2 nanotubes, resulting in an ideal coherent grain boundary and single crystal growth. The resultant photo-anode produces 30% more photocurrent than those samples without coherent grain boundary. Notably, the especial epitaxial hetero-structure is beneficial to decrease the recombination site and accelerate the separation of photogenerated electron-hole pairs. Furthermore, an ultrathin PEDOT surface layer was developed on the epitaxial hetero-structure of CdSe/TiO2 nano-tube arrays in which it functions as both a physical passivation barrier and a hole transfer layer. As a result, significantly enhanced photocurrent density and substantially better stability have been achieved. This methodology may be providing a new pathway of epitaxial growth for preparing the heterogeneous junction materials which have similar d spacing. Royal Society of Chemistry 2017-02-22 Article PeerReviewed Chong, Baohe, Zhu, Wen and Hou, Xianghui (2017) Epitaxial hetero-structure of CdSe/TiO2 nanotube arrays with PEDOT as hole transfer layer for photoelectrochemical hydrogen evolution. Journal of Materials Chemistry A . ISSN 2050-7496 http://pubs.rsc.org/en/Content/ArticleLanding/2017/TA/C6TA10202F#!divAbstract doi:10.1039/C6TA10202F doi:10.1039/C6TA10202F
spellingShingle Chong, Baohe
Zhu, Wen
Hou, Xianghui
Epitaxial hetero-structure of CdSe/TiO2 nanotube arrays with PEDOT as hole transfer layer for photoelectrochemical hydrogen evolution
title Epitaxial hetero-structure of CdSe/TiO2 nanotube arrays with PEDOT as hole transfer layer for photoelectrochemical hydrogen evolution
title_full Epitaxial hetero-structure of CdSe/TiO2 nanotube arrays with PEDOT as hole transfer layer for photoelectrochemical hydrogen evolution
title_fullStr Epitaxial hetero-structure of CdSe/TiO2 nanotube arrays with PEDOT as hole transfer layer for photoelectrochemical hydrogen evolution
title_full_unstemmed Epitaxial hetero-structure of CdSe/TiO2 nanotube arrays with PEDOT as hole transfer layer for photoelectrochemical hydrogen evolution
title_short Epitaxial hetero-structure of CdSe/TiO2 nanotube arrays with PEDOT as hole transfer layer for photoelectrochemical hydrogen evolution
title_sort epitaxial hetero-structure of cdse/tio2 nanotube arrays with pedot as hole transfer layer for photoelectrochemical hydrogen evolution
url https://eprints.nottingham.ac.uk/41019/
https://eprints.nottingham.ac.uk/41019/
https://eprints.nottingham.ac.uk/41019/