Orbital engineering: photoactivation of an organofunctionalized polyoxotungstate

Tungsten-based polyoxometalates (POMs) are employed as UV-driven photo-catalysts for a range of organic transformations. Their photoactivity is dependent on electronic transitions between frontier orbitals, and thus manipulation of orbital energy levels provides a promising means of extending their...

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Main Authors: Newton, Graham, Oshio, Hiroki, Cameron, Jamie, Fujimoto, Satomi, Kastner, Katharina, Wei, Rong Jia, Robinson, David, Sans, Victor
Format: Article
Published: Wiley 2017
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Online Access:https://eprints.nottingham.ac.uk/38667/
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author Newton, Graham
Oshio, Hiroki
Cameron, Jamie
Fujimoto, Satomi
Kastner, Katharina
Wei, Rong Jia
Robinson, David
Sans, Victor
author_facet Newton, Graham
Oshio, Hiroki
Cameron, Jamie
Fujimoto, Satomi
Kastner, Katharina
Wei, Rong Jia
Robinson, David
Sans, Victor
author_sort Newton, Graham
building Nottingham Research Data Repository
collection Online Access
description Tungsten-based polyoxometalates (POMs) are employed as UV-driven photo-catalysts for a range of organic transformations. Their photoactivity is dependent on electronic transitions between frontier orbitals, and thus manipulation of orbital energy levels provides a promising means of extending their utility into the visible regime. Here, an organic-inorganic hybrid polyoxometalate, K₆[P₂2W₁₇O₅₇(PO₅H₅C₇)₂]·6C₄H₉NO, was found to exhibit enhanced redox behavior and photochemistry compared to its purely inorganic counterparts. Hybridization with electron withdrawing moieties was shown to modify the frontier orbital energy levels and reduce the HOMO-LUMO gap, leading to direct visible-light photoactivation of the hybrid, and establishing a simple, cheap and effective approach to the generation of visible-light-activated hybrid nanomaterials
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spelling nottingham-386672020-05-04T18:23:08Z https://eprints.nottingham.ac.uk/38667/ Orbital engineering: photoactivation of an organofunctionalized polyoxotungstate Newton, Graham Oshio, Hiroki Cameron, Jamie Fujimoto, Satomi Kastner, Katharina Wei, Rong Jia Robinson, David Sans, Victor Tungsten-based polyoxometalates (POMs) are employed as UV-driven photo-catalysts for a range of organic transformations. Their photoactivity is dependent on electronic transitions between frontier orbitals, and thus manipulation of orbital energy levels provides a promising means of extending their utility into the visible regime. Here, an organic-inorganic hybrid polyoxometalate, K₆[P₂2W₁₇O₅₇(PO₅H₅C₇)₂]·6C₄H₉NO, was found to exhibit enhanced redox behavior and photochemistry compared to its purely inorganic counterparts. Hybridization with electron withdrawing moieties was shown to modify the frontier orbital energy levels and reduce the HOMO-LUMO gap, leading to direct visible-light photoactivation of the hybrid, and establishing a simple, cheap and effective approach to the generation of visible-light-activated hybrid nanomaterials Wiley 2017-01-01 Article PeerReviewed Newton, Graham, Oshio, Hiroki, Cameron, Jamie, Fujimoto, Satomi, Kastner, Katharina, Wei, Rong Jia, Robinson, David and Sans, Victor (2017) Orbital engineering: photoactivation of an organofunctionalized polyoxotungstate. Chemistry - a European Journal, 23 (1). pp. 47-50. ISSN 1521-3765 Polyoxometalates; Photochemistry; Visible-light; Catalysis; Electrochemistry http://onlinelibrary.wiley.com/doi/10.1002/chem.201605021/abstract doi:10.1002/chem.201605021 doi:10.1002/chem.201605021
spellingShingle Polyoxometalates; Photochemistry; Visible-light; Catalysis; Electrochemistry
Newton, Graham
Oshio, Hiroki
Cameron, Jamie
Fujimoto, Satomi
Kastner, Katharina
Wei, Rong Jia
Robinson, David
Sans, Victor
Orbital engineering: photoactivation of an organofunctionalized polyoxotungstate
title Orbital engineering: photoactivation of an organofunctionalized polyoxotungstate
title_full Orbital engineering: photoactivation of an organofunctionalized polyoxotungstate
title_fullStr Orbital engineering: photoactivation of an organofunctionalized polyoxotungstate
title_full_unstemmed Orbital engineering: photoactivation of an organofunctionalized polyoxotungstate
title_short Orbital engineering: photoactivation of an organofunctionalized polyoxotungstate
title_sort orbital engineering: photoactivation of an organofunctionalized polyoxotungstate
topic Polyoxometalates; Photochemistry; Visible-light; Catalysis; Electrochemistry
url https://eprints.nottingham.ac.uk/38667/
https://eprints.nottingham.ac.uk/38667/
https://eprints.nottingham.ac.uk/38667/