Surface modification of mild steel using a combination of laser and electrochemical processes

Traditional methods for achieving hierarchical surface structures include highly specified, deterministic approaches to create features to meet design intention. In this study microstructural alteration was undertaken using laser apparatus and secondary texturing was achieved via succeeding electroc...

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Main Authors: Speidel, Alistair, Lutey, Adrian Hugh Alexander, Mitchell-Smith, Jonathon, Rance, Graham A., Liverani, Erica, Ascari, Alessandro, Fortunato, Alessandro, Clare, Adam T.
Format: Article
Published: Elsevier 2016
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Online Access:https://eprints.nottingham.ac.uk/37893/
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author Speidel, Alistair
Lutey, Adrian Hugh Alexander
Mitchell-Smith, Jonathon
Rance, Graham A.
Liverani, Erica
Ascari, Alessandro
Fortunato, Alessandro
Clare, Adam T.
author_facet Speidel, Alistair
Lutey, Adrian Hugh Alexander
Mitchell-Smith, Jonathon
Rance, Graham A.
Liverani, Erica
Ascari, Alessandro
Fortunato, Alessandro
Clare, Adam T.
author_sort Speidel, Alistair
building Nottingham Research Data Repository
collection Online Access
description Traditional methods for achieving hierarchical surface structures include highly specified, deterministic approaches to create features to meet design intention. In this study microstructural alteration was undertaken using laser apparatus and secondary texturing was achieved via succeeding electrochemical processes. Electrochemical jet machining (EJM) was performed on mild steel subjected to laser pre-treatment using power densities of 4167 and 5556 W/cm2 with pulse durations from 0.3 - 1.5 seconds. Results show that in combination, laser pre-treatment and EJM can alter the exposed surface textures and chemistries. Here, machined surface roughness (Sa) was shown to increase from approximately 0.45 µm for untreated surfaces to approximately 18 µm for surfaces subjected to extreme laser pretreatments. After pre-treatments materials were characterised to appraise microstructural changes, shown to be martensite formation, reinforced by complementary simulation data, and significant increases in observable hardness from approximately 261 HV for the asreceived material to over 700 HV after pre-treatment. The greater hardness was retained after EJM. Exposed martensitic lath structures at machined surfaces are shown to be partially responsible for surface roughness increases. The surfaces were explored with energy dispersive X-ray spectroscopy (EDS) and Raman spectroscopy demonstrating changes in apparent surface chemistry. This analysis revealed increasing oxide formation at the surface of the pre-treated EJM surface, a further contributory factor to surface roughness increases. This new process chain will be of interest to manufacturers seeking to control surface morphology for applications including micro-injection mould/die manufacture. While demonstrated here for steel similar mechanisms are exploitable in other material systems. A new technique has been demonstrated, resulting from the models and processes presented to couple laser and electrolyte jet processing for complex surface preparation.
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spelling nottingham-378932020-05-04T18:25:52Z https://eprints.nottingham.ac.uk/37893/ Surface modification of mild steel using a combination of laser and electrochemical processes Speidel, Alistair Lutey, Adrian Hugh Alexander Mitchell-Smith, Jonathon Rance, Graham A. Liverani, Erica Ascari, Alessandro Fortunato, Alessandro Clare, Adam T. Traditional methods for achieving hierarchical surface structures include highly specified, deterministic approaches to create features to meet design intention. In this study microstructural alteration was undertaken using laser apparatus and secondary texturing was achieved via succeeding electrochemical processes. Electrochemical jet machining (EJM) was performed on mild steel subjected to laser pre-treatment using power densities of 4167 and 5556 W/cm2 with pulse durations from 0.3 - 1.5 seconds. Results show that in combination, laser pre-treatment and EJM can alter the exposed surface textures and chemistries. Here, machined surface roughness (Sa) was shown to increase from approximately 0.45 µm for untreated surfaces to approximately 18 µm for surfaces subjected to extreme laser pretreatments. After pre-treatments materials were characterised to appraise microstructural changes, shown to be martensite formation, reinforced by complementary simulation data, and significant increases in observable hardness from approximately 261 HV for the asreceived material to over 700 HV after pre-treatment. The greater hardness was retained after EJM. Exposed martensitic lath structures at machined surfaces are shown to be partially responsible for surface roughness increases. The surfaces were explored with energy dispersive X-ray spectroscopy (EDS) and Raman spectroscopy demonstrating changes in apparent surface chemistry. This analysis revealed increasing oxide formation at the surface of the pre-treated EJM surface, a further contributory factor to surface roughness increases. This new process chain will be of interest to manufacturers seeking to control surface morphology for applications including micro-injection mould/die manufacture. While demonstrated here for steel similar mechanisms are exploitable in other material systems. A new technique has been demonstrated, resulting from the models and processes presented to couple laser and electrolyte jet processing for complex surface preparation. Elsevier 2016-12-15 Article PeerReviewed Speidel, Alistair, Lutey, Adrian Hugh Alexander, Mitchell-Smith, Jonathon, Rance, Graham A., Liverani, Erica, Ascari, Alessandro, Fortunato, Alessandro and Clare, Adam T. (2016) Surface modification of mild steel using a combination of laser and electrochemical processes. Surface and Coatings Technology, 307 (A). pp. 849-860. ISSN 1879-3347 Surface texturing ECM EJM hybrid processing laser processing http://www.sciencedirect.com/science/article/pii/S0257897216309598 doi:10.1016/j.surfcoat.2016.09.077 doi:10.1016/j.surfcoat.2016.09.077
spellingShingle Surface texturing
ECM
EJM
hybrid processing
laser processing
Speidel, Alistair
Lutey, Adrian Hugh Alexander
Mitchell-Smith, Jonathon
Rance, Graham A.
Liverani, Erica
Ascari, Alessandro
Fortunato, Alessandro
Clare, Adam T.
Surface modification of mild steel using a combination of laser and electrochemical processes
title Surface modification of mild steel using a combination of laser and electrochemical processes
title_full Surface modification of mild steel using a combination of laser and electrochemical processes
title_fullStr Surface modification of mild steel using a combination of laser and electrochemical processes
title_full_unstemmed Surface modification of mild steel using a combination of laser and electrochemical processes
title_short Surface modification of mild steel using a combination of laser and electrochemical processes
title_sort surface modification of mild steel using a combination of laser and electrochemical processes
topic Surface texturing
ECM
EJM
hybrid processing
laser processing
url https://eprints.nottingham.ac.uk/37893/
https://eprints.nottingham.ac.uk/37893/
https://eprints.nottingham.ac.uk/37893/