Oxalate-bridged heterometallic chains with monocationic dabco derivatives

A series of bimetallic oxalate-bridged one-dimensional chains with monocationic dabco derivatives, ({R-dabco}[M(solv)2][Cr(ox)3]·n(solv)) (dabco = 1,4-diazabicyclo[2.2.2]octane, H2ox = oxalate; R = H, M = Co (1); R = H, M = Zn (2); R = Bu, M = Co (3); R = Bu, M = Zn (4)) were synthesized. All compou...

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Main Authors: Sakurai, Takahiro, Saiki, Ryo, Wei, Rong Jia, Newton, Graham, Shiga, Takuya, Oshio, Hiroki
Format: Article
Published: Royal Society of Chemistry 2016
Online Access:https://eprints.nottingham.ac.uk/37737/
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author Sakurai, Takahiro
Saiki, Ryo
Wei, Rong Jia
Newton, Graham
Shiga, Takuya
Oshio, Hiroki
author_facet Sakurai, Takahiro
Saiki, Ryo
Wei, Rong Jia
Newton, Graham
Shiga, Takuya
Oshio, Hiroki
author_sort Sakurai, Takahiro
building Nottingham Research Data Repository
collection Online Access
description A series of bimetallic oxalate-bridged one-dimensional chains with monocationic dabco derivatives, ({R-dabco}[M(solv)2][Cr(ox)3]·n(solv)) (dabco = 1,4-diazabicyclo[2.2.2]octane, H2ox = oxalate; R = H, M = Co (1); R = H, M = Zn (2); R = Bu, M = Co (3); R = Bu, M = Zn (4)) were synthesized. All compounds have one-dimensional zig-zag chain structures with R-dabco cations located between chains. Cryomagnetic studies reveal that 1 and 3 showed intrachain ferromagnetic interactions between Co(II) and Cr(III) ions and metamagnetic behaviour due to interchain antiferromagnetic interactions. Permittivity measurements on compound 4 indicate specific paraelectronic relaxation behaviour originating from the rotational motion of the dabco alkyl substituent.
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publisher Royal Society of Chemistry
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spelling nottingham-377372020-05-04T18:13:43Z https://eprints.nottingham.ac.uk/37737/ Oxalate-bridged heterometallic chains with monocationic dabco derivatives Sakurai, Takahiro Saiki, Ryo Wei, Rong Jia Newton, Graham Shiga, Takuya Oshio, Hiroki A series of bimetallic oxalate-bridged one-dimensional chains with monocationic dabco derivatives, ({R-dabco}[M(solv)2][Cr(ox)3]·n(solv)) (dabco = 1,4-diazabicyclo[2.2.2]octane, H2ox = oxalate; R = H, M = Co (1); R = H, M = Zn (2); R = Bu, M = Co (3); R = Bu, M = Zn (4)) were synthesized. All compounds have one-dimensional zig-zag chain structures with R-dabco cations located between chains. Cryomagnetic studies reveal that 1 and 3 showed intrachain ferromagnetic interactions between Co(II) and Cr(III) ions and metamagnetic behaviour due to interchain antiferromagnetic interactions. Permittivity measurements on compound 4 indicate specific paraelectronic relaxation behaviour originating from the rotational motion of the dabco alkyl substituent. Royal Society of Chemistry 2016-09-05 Article PeerReviewed Sakurai, Takahiro, Saiki, Ryo, Wei, Rong Jia, Newton, Graham, Shiga, Takuya and Oshio, Hiroki (2016) Oxalate-bridged heterometallic chains with monocationic dabco derivatives. Dalton Transactions, 45 . pp. 16182-16189. ISSN 1477-9234 http://pubs.rsc.org/is/content/articlelanding/2016/dt/c6dt02955h#!divAbstract doi:10.1039/C6DT02955H doi:10.1039/C6DT02955H
spellingShingle Sakurai, Takahiro
Saiki, Ryo
Wei, Rong Jia
Newton, Graham
Shiga, Takuya
Oshio, Hiroki
Oxalate-bridged heterometallic chains with monocationic dabco derivatives
title Oxalate-bridged heterometallic chains with monocationic dabco derivatives
title_full Oxalate-bridged heterometallic chains with monocationic dabco derivatives
title_fullStr Oxalate-bridged heterometallic chains with monocationic dabco derivatives
title_full_unstemmed Oxalate-bridged heterometallic chains with monocationic dabco derivatives
title_short Oxalate-bridged heterometallic chains with monocationic dabco derivatives
title_sort oxalate-bridged heterometallic chains with monocationic dabco derivatives
url https://eprints.nottingham.ac.uk/37737/
https://eprints.nottingham.ac.uk/37737/
https://eprints.nottingham.ac.uk/37737/