Melt-processed PLA/HA platelet nanoparticle composites produced using tailored dispersants

Hydroxyapatite (HA) nanoparticles, similar to those seen in the structure of human bone, have been produced via hydrothermal synthesisand used to produce nanocomposite materials via melt blending with poly(lactic acid)(PLA). Both of these processes are scalable and commercially relevant. Tailored di...

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Main Authors: Parsons, Andrew J., Walton, Kirsty, Hild, Frederic, Ilchev, Alex, Gimeno-Fabra, Miquel, Tomczynska, Magdelena M., Ward, Michael, Canciani, Alessia, Choong, Gabriel Y.H., De Focatiis, Davide S.A., Lester, Edward, Grant, David M., Irvine, Derek J.
Format: Conference or Workshop Item
Published: 2016
Subjects:
Online Access:https://eprints.nottingham.ac.uk/35681/
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author Parsons, Andrew J.
Walton, Kirsty
Hild, Frederic
Ilchev, Alex
Gimeno-Fabra, Miquel
Tomczynska, Magdelena M.
Ward, Michael
Canciani, Alessia
Choong, Gabriel Y.H.
De Focatiis, Davide S.A.
Lester, Edward
Grant, David M.
Irvine, Derek J.
author_facet Parsons, Andrew J.
Walton, Kirsty
Hild, Frederic
Ilchev, Alex
Gimeno-Fabra, Miquel
Tomczynska, Magdelena M.
Ward, Michael
Canciani, Alessia
Choong, Gabriel Y.H.
De Focatiis, Davide S.A.
Lester, Edward
Grant, David M.
Irvine, Derek J.
author_sort Parsons, Andrew J.
building Nottingham Research Data Repository
collection Online Access
description Hydroxyapatite (HA) nanoparticles, similar to those seen in the structure of human bone, have been produced via hydrothermal synthesisand used to produce nanocomposite materials via melt blending with poly(lactic acid)(PLA). Both of these processes are scalable and commercially relevant. Tailored dispersants were developed and used to improve the dispersion of the HA. Modest improvements in flexural properties were observed (max increases 30% of dry modulus, 13% of wet strength). Rheometry is not suggestive of achieving percolation,so there is potential to improve mechanical properties further. It was established that very dry processing conditions are essential to maintaining the molecular weight of the PLA during processing and that the use of the tailored dispersants can also help to mitigateprocess-induced degradation.MicroCT has proved to be a useful quality control tool to support TEM analysis.
first_indexed 2025-11-14T19:27:18Z
format Conference or Workshop Item
id nottingham-35681
institution University of Nottingham Malaysia Campus
institution_category Local University
last_indexed 2025-11-14T19:27:18Z
publishDate 2016
recordtype eprints
repository_type Digital Repository
spelling nottingham-356812020-05-04T17:52:38Z https://eprints.nottingham.ac.uk/35681/ Melt-processed PLA/HA platelet nanoparticle composites produced using tailored dispersants Parsons, Andrew J. Walton, Kirsty Hild, Frederic Ilchev, Alex Gimeno-Fabra, Miquel Tomczynska, Magdelena M. Ward, Michael Canciani, Alessia Choong, Gabriel Y.H. De Focatiis, Davide S.A. Lester, Edward Grant, David M. Irvine, Derek J. Hydroxyapatite (HA) nanoparticles, similar to those seen in the structure of human bone, have been produced via hydrothermal synthesisand used to produce nanocomposite materials via melt blending with poly(lactic acid)(PLA). Both of these processes are scalable and commercially relevant. Tailored dispersants were developed and used to improve the dispersion of the HA. Modest improvements in flexural properties were observed (max increases 30% of dry modulus, 13% of wet strength). Rheometry is not suggestive of achieving percolation,so there is potential to improve mechanical properties further. It was established that very dry processing conditions are essential to maintaining the molecular weight of the PLA during processing and that the use of the tailored dispersants can also help to mitigateprocess-induced degradation.MicroCT has proved to be a useful quality control tool to support TEM analysis. 2016-05-09 Conference or Workshop Item PeerReviewed Parsons, Andrew J., Walton, Kirsty, Hild, Frederic, Ilchev, Alex, Gimeno-Fabra, Miquel, Tomczynska, Magdelena M., Ward, Michael, Canciani, Alessia, Choong, Gabriel Y.H., De Focatiis, Davide S.A., Lester, Edward, Grant, David M. and Irvine, Derek J. (2016) Melt-processed PLA/HA platelet nanoparticle composites produced using tailored dispersants. In: The 5th International Conference of Bionic Engineering, 21 - 24 June 2016, Ningbo, China. (Unpublished) Nanocomposite; hydroxyapatite; polylactic acid
spellingShingle Nanocomposite; hydroxyapatite; polylactic acid
Parsons, Andrew J.
Walton, Kirsty
Hild, Frederic
Ilchev, Alex
Gimeno-Fabra, Miquel
Tomczynska, Magdelena M.
Ward, Michael
Canciani, Alessia
Choong, Gabriel Y.H.
De Focatiis, Davide S.A.
Lester, Edward
Grant, David M.
Irvine, Derek J.
Melt-processed PLA/HA platelet nanoparticle composites produced using tailored dispersants
title Melt-processed PLA/HA platelet nanoparticle composites produced using tailored dispersants
title_full Melt-processed PLA/HA platelet nanoparticle composites produced using tailored dispersants
title_fullStr Melt-processed PLA/HA platelet nanoparticle composites produced using tailored dispersants
title_full_unstemmed Melt-processed PLA/HA platelet nanoparticle composites produced using tailored dispersants
title_short Melt-processed PLA/HA platelet nanoparticle composites produced using tailored dispersants
title_sort melt-processed pla/ha platelet nanoparticle composites produced using tailored dispersants
topic Nanocomposite; hydroxyapatite; polylactic acid
url https://eprints.nottingham.ac.uk/35681/